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77950789923
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Note
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2, and 20 mL of hexane was added to precipitate the metal complex. After filtration on Celite, the precipitate was dissolved in MeOH. Removal of volatiles in vacuo left behind a yellow bright solid (m = 182 mg, yield = 85%), which could be used without any further purification. Crystals were obtained from MeOH.
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12
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77950852618
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Note
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For crystal data, see Supporting Information. The crystal structure has been deposited at the Cambridge Crystallographic Data Centre and allocated the deposition number CCDC 685045. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge, CB2 1EZ, UK (fax (+44) 1223-336-033; e-mail: deposit@ccdc.cam.ac.uk).
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13
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3142749778
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20
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77950832121
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Note
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4, filtrated, and concentrated in vacuo. The desired products were purified by flash chromatography on silica gel. Optical purities of the products were obtained from GLC analysis (Chiraldex-GTA column) or HPLC analysis (OD-H column).
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21
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77950841706
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Note
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The ee value was determined by HPLC on chiral column (chiracel OD-H), and the absolute configuration was established by comparison of the optical rotation with the literature data.
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22
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77950807823
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Note
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DIPPAM/Pd complexes are very stable toward air and can be easily purified by chromatography on silica gel.
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23
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84987265458
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Von Matt, P.; Lloyd-Jones, G. C.; Minidis, A. B. E.; Pfaltz, A.; Macko, L.; Neuburger, M.; Zehnder, M.; Rüegger, H.; Pregosin, P. S. Helv. Chim. Acta 1995, 78, 265-284
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Von Matt, P.1
Lloyd-Jones, G.C.2
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Pfaltz, A.4
MacKo, L.5
Neuburger, M.6
Zehnder, M.7
Rüegger, H.8
Pregosin, P.S.9
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