Location and quantification of hydroxyl in wadsleyite: New insights

American Mineralogist

Volumn 95, Issue 2-3, 2010, Pages 312-322

  Deon, Fiorenza ^a   Koch Müller, Monika ^a   Rhede, Diether ^a   Gottschalk, Matthias ^a   Wirth, Richard ^a   Thomas, Sylvia Monique ^b  

^a GFZ GERMAN RESEARCH CENTRE FOR GEOSCIENCES   (Germany)

^b NORTHWESTERN UNIVERSITY   (United States)

Author keywords

Absorption coefficient for water; FTIR spectroscopy; Protonation; Raman spectroscopy; SIMS; Wadsleyite

Indexed keywords

CRYSTAL ATOMIC STRUCTURE; ELECTRON PROBE MICROANALYSIS; MAGNESIUM METALLOGRAPHY; PROTONATION; RAMAN SPECTROSCOPY; SECONDARY ION MASS SPECTROMETRY; SINGLE CRYSTALS; WATER ABSORPTION; X RAY DIFFRACTION;

ABSORPTION CO-EFFICIENT; BROAD BANDS; FT-IR SPECTRUM; FTIR SPECTROSCOPY; HIGH PRESSURE; MULTI-ANVIL PRESS; WADSLEYITE; X-RAY REFINEMENT;

FOURIER TRANSFORM INFRARED SPECTROSCOPY;

ABSORPTION COEFFICIENT; ELECTRON DENSITY; ELECTRON PROBE ANALYSIS; FTIR SPECTROSCOPY; HIGH PRESSURE; HYDROXYL RADICAL; RAMAN SPECTROSCOPY; WADSLEYITE;

EID: 77950202991     PISSN: 0003004X     EISSN: None     Source Type: Journal    
DOI: 10.2138/am.2010.3267     Document Type: Article

References (72)

1. Akaogi, M., Yusa, H., Shiraishi, K., and Suzuki, T. (1995) Thermodynamic properties of a-quartz, coesite, and stishovite and equilibrium phase relations at high pressures and high temperatures. Journal of Geophysical Research, 100, 337-347.
2. Armstrong, J.T. (1991) Quantitative elemental analysis of individual microparticles with electron beam instruments. In K.F.J. Heinrich and D.E. Newbury, Eds., Electron Probe Quantification, p. 261-315. Plenum Press, New York.
3. Balan, E., Refson, K., Blanchard, M., Delattre, S., Lazzeri, M., Ingrin, J., Mauri, F., Wright, K., and Winkler, B. (2008) Theoretical infrared absorption coefficient of OH groups in minerals. American Mineralogist, 93, 950-953.
4. Bell, D.R. and Rossman, G.R. 1992 Water in Earth's mantle: The role of nominally anhydrous minerals. Science, 255, 1931-1937.
5. Bell, D.R., Rossman, G.R., Maldener, J., Endisch, D., and Rauch, F. (2003) Hydroxide in olivine: a quantitative determination of the absolute amount and calibration of the IR spectrum. Journal of Geophysical Research, 108, 2105-2113, DOI: 10.1029/2001JB000679.
6. Bercovici, D. and Karato, S. (2003) Whole-mantle convection and the transition-zone water filter. Nature, 425, 35-44.
7. Beurskens, P.T., Admiraal, G., Beurskens, G., Bosman, W.P., De Gelder, R., Israel, R., and Smits, J.M.M. (1999) The DIRDIF-99 program system. Technical Report of the Crystallography Laboratory, University of Nijmegen, The Netherlands.
8. Blanchard, M., Balan, E., and Wright, K. (2009) Incorporation of water in iron free ringwoodite: A first-principles study. American Mineralogist, 94, 83-89.
9. Caglioti, G., Paoletti, A., and Ricci, F.P. (1958) Choice of collimators for a crystal spectrometer for neutron diffraction. Nuclear Instrument Methods, 3, 223-228.
10. Canil, D. and O'Neill, H.St.C. (1994) Distribution of ferric iron in some upper-mantle assemblages. Journal of Petrology, 37, 609-635.
11. 4 system. Geophysical Research Letters, 29, 1875, DOI: 10.1029/2001GL014429.
12. Creagh, D.C. and Hubbell, J.H. (1992) Table 4.2.4.3. In A.J.C. Wilson, Ed., International Tables for Crystallography, Vol.C, p. 200-206. Kluwer Academic Publishers, Boston.
13. Creagh, D.C. and McAuley, W.J. (1992) Table 4.2.6.8. In A.J.C. Wilson, Ed., International Tables for Crystallography, Vol.C, p. 219-222. Kluwer Academic Publishers, Boston.
14. Cromer, D.T. and Waber, J.T. (1974) International Tables for X-ray Crystallography, Vol.IV, Table 2.2 A. The Kynoch Press, Birmingham, England.
15. Cynn, H. and Hofmeister A.M. (1994) High-pressure IR spectra of lattice modes and OH vibrations in Fe-bearing wadsleyite. Journal of Geophysical Research, 99, 17717-17727.
16. Demouchy, S., Deloule, E., Frost, D.J., and Keppler, H. (2005) Temperature and pressure dependence of water solubility in Fe-free wadsleyite. American Mineralogist, 81, 1084-1091.
17. 4 from an experimentally derived electrostatic potential. American Mineralogist, 74, 1124-1129.
18. 4, 0.00 = x = 0.40. Physics and Chemistry of Minerals, 19, 361-368.
19. 2O on the 410 km discontinuity. Earth and Planetary Science Letters, 256, 182-195, DOI: 10.1016/j.epsl.2007.01.023. (Pubitemid 46359675)
20. 4 with x = 0 and 0.25. American Mineralogist, 85, 770-777.
21. 2O in nominally anhydrous minerals in the Earth upper mantle. Earth and Planetary Science Letters, 236, 167-181.
22. Huang, X., Xu, Y., and Karato, S. (2005) Water content in the transition zone from electrical conductivity of wadsleyite and ringwoodite. Nature, 434, 746-749.
23. Ibers, J.A. and Hamilton, W.C. (1964) Dispersion corrections and crystal structure refinements. Acta Crystallographica, 17, 781-782.
24. Ingrin, J. and Skogby, H. (2000) Hydrogen in nominally anhydrous minerals: Concentration levels and implications. European Journal of Mineralogy, 12, 543-570.
25. 2O to 15 GPa. Physics of the Earth and Planetary Interiors, 85, 237-263.
26. 4: A new water reservoir in the mantle transition zone. Geophysical Research Letters, 22, 117-120.
27. Jacobsen, S.D. (2006) Effect of water on the equation of state of nominally anhydrous minerals. In H.J. Keppler and J.R. Smyth, Eds., Water in Nominally Anhydrous Minerals, 62, p. 321-342. Reviews in Mineralogy and Geochemistry, Mineralogical Society of America, Chantilly, Virginia.
28. Jacobsen, S.D., Demouchy, S., Frost, D.J., Boffa-Ballaran, T., and Kung, J. (2005) A systematic study of OH in hydrous wadsleyite from polarized FTIR spectroscopy and single-crystal X-ray diffraction: Oxygen sites for hydrogen storage in the Earth's interior. American Mineralogist, 90, 61-70.
29. Karato, S. (1990) The role of hydrogen in the electrical conductivity of the upper mantle. Nature, 347, 272-2732.
30. - (2006) Influence of hydrogen-related defects on the electrical conductivity and plastic deformation mantle minerals: A critical review. In S.D. Jacobsen, and S. van der Lee, Eds., Earth's Deep Water Cycle, 168, p. 113-129.Geophysical Monograph Series, American Geophysical Union, Washington, D.C.
31. 4). Physics and Chemistry of Minerals, 28, 232-241.
32. Kleppe, A.K., Jephcoat, A.P., and Smyth, J.R. (2005) High-pressure Raman spectroscopic study of Fo90 hydrous wadsleyite. Physics and Chemistry of Minerals, 32, 700-709.
33. Klimenkov, M., Möslang, A., and Lindau, R. (2008) EELS analysis of complex precipitates in PM (2000) steel. The European Physical Journal of Applied Physics, 42, 293-303.
34. Koch-Müller, M., Fey, Y., Hauri, E., and Liu, Z. (2001) Location and quantitative analysis of OH in coesite. Physics and Chemistry of Minerals, 28, 693-705.
35. Koch-Müller, M., Dera, P., Fei, Y., Reno, B.L., Sobolev, N.V., Hauri, E., and Wysoczanski, R. (2003) OH in synthetic and natural coesite. American Mineralogist, 88, 1436-1445.
36. Koch-Müller, M., Matsyuk, S.S., Rhede, D., Wirth, R., and Khisina, N. (2006) Hydroxyl in mantle olivine xenocrysts from Udachnaya kimberlite pipe. Physics and Chemistry of Minerals, 33, 276-287.
37. 4. Contributions to Mineralogy and Petrology, 123, 345-357.
38. 4). American Mineralogist, 87, 293-301.
39. 4. In M.H. Manghnani and T. Yagi, Eds., Properties of Earth and Planetary Materials at High Pressure and Temperature, 101, p. 517-520. Geophysical Monograph, American Geophysical Union, Washington, D.C.
40. Larson, A.B. and Von Dreele, R.B. (2000) General Structure Analysis System (GSAS). Los Alamos National Laboratory Report LAUR 86-748.
41. Lathe, C., Koch-Müller, M., Wirth, R., Van Westrenen, W., Mueller, H.J., Schilling, F.R., and Lauterjung, J. (2005) The influence of OH in coesite on the kinetics of the coesite-quartz phase transition. American Mineralogist, 90, 36-43.
42. Libowitzky, E. (1999) Correlation of O-H stretching frequencies and O-H⋯O hydrogen bond lengths in minerals. Monatshefte für Chemie, 130, 1047-1059.
43. Libowitzky, E. and Rossman G.R. (1997) An IR absorption calibration for water in minerals. American Mineralogist, 82, 1111-1115.
44. Lloyd, E.C. (1971) Editorial introduction and summary to: Accurate characterization of the high pressure environment. U.S. National Bureau Standards Special Publication, 326, 1-3.
45. Maldener, J., Hösch, A., Langer, K., and Rauch, F. (2003) Hydrogen in some natural garnets studied by nuclear reaction analysis and vibrational spectroscopy. Physics and Chemistry of Minerals, 30, 337-344.
46. Mao, H.K. and Hemley, R.J. (1998) New windows on Earth's deep interior. In R.J. Hemley, Ed., Ultrahigh-Pressure Mineralogy: Physics and Chemistry of the Earth's Deep Interior, 37, p. 1-32. Reviews in Mineralogy and Geochemistry, Mineralogical Society of America, Chantilly, Virginia.
47. Mao, H.K., Xu, J., and Bell, P.M. (1986) Calibration of the ruby pressure gauge to 800 kbar under quasi hydrostatic conditions. Journal of Geophysical Research, 91, 4673-4676.
48. 4. American Mineralogist, 76, 354-360.
49. Miller, G.H., Rossman, G.R., and Harlow, G.E. (1987) The natural occurrence of hydroxide in olivine. Physics and Chemistry of Minerals, 14, 461-472.
50. 4 determined by in situ X-ray observation. Science, 26, 1202-1203.
51. Mosenfelder, J.L., Deligne, N.I., Asimow, P.D., and Rossman, G.R. (2006) Hydrogen incorporation in olivine from 2-12 GPa. American Mineralogist, 91, 285-294.
52. Nishihara, Y., Matsukage, K.N., and Karato, S. (2006) Effects of metal protection coils on thermocouple EMF in multi-anvil high-pressure experiments. American Mineralogist, 91, 114-114
53. Paterson, M. (1982) The determination of hydroxyl by infrared absorption in quartz, silicate glasses, and similar materials. Bulletin de Minéralogie, 105, 20-29.
54. Piermarini, G.J. and Block, S. (1975) Ultra high pressure diamond-anvil cell and several semiconductor phase transition pressures in relation to fixed point pressure scale. Reviews of Scientific Instruments, 46, 973-980.
55. Schmidt, M.W. and Ulmer, P. (2004) A rocking multianvil: Elimination of chemical segregation in fluid-saturated high-pressure experiments. Geochimica et Cosmochimica Acta, 68, 1889-1899.
56. 4: A potential host for water in mantle? American Mineralogist, 72, 1051-1055.
57. 4): An ocean in the Earth's interior? American Mineralogist, 79, 1021-1024.
58. - (2006) Hydrogen in high pressure silicate and oxide mineral structures. In H. Keppler, and J.R. Smyth, Eds., Water in Nominally Anhydrous Minerals, 62, p. 85-115. Reviews in Mineralogy and Geochemistry, Mineralogical Society of America, Chantilly, Virginia.
59. Smyth, J.R. and Frost, D.J. (2002) The effect of water on the 410-km discontinuity: An experimental study. Geophysical Research Letters, 292, 1485.
60. Smyth, J.R. and Jacobsen S.D. (2006) Nominally anhydrous minerals and the Earth's deep water cycle. In S.D. Jacobsen and S. van der Lee, Eds., Earth's Deep Water Cycle, 168, p. 1-11. American Geophysical Union, Geophysical Monograph Series, Washington, D.C.
61. Thomas, S.M., Thomas, R., Davidson, P., Reichart, P., Koch-Müller, M., and Dollinger, G. (2008a) Application of Raman spectroscopy to quantify trace water concentrations in glasses and garnets. American Mineralogist, 93, 1550-1557.
62. Thomas, S.M., Koch-Müller, M., Kahlenberg, V., Thomas, R., Rhede, D., Wirth, R., and Wunder, B. (2008b) Protonation in germanium equivalents of ringwoodite, anhydrous phase B, and superhydrous phase B. American Mineralogist, 93, 1282-1294.
63. 2 polymorphs. Physics and Chemistry of Minerals, 36, 489-509, DOI: 10.1007/s00269-009-0295-1.
64. Tsuchiya, J. and Tsuchiya, T. (2009) First principles investigation of the structural and elastic properties of hydrous wadsleyite under pressure. Journal of Geophysical Research, 114, B02206, DOI: 10.1029/2008JB005841.
65. 2,3-edge electron energy-loss near-edge structure spectroscopy. Physics and Chemistry of Minerals, 25, 323-327.
66. Walker, D. (1991) Lubrication, gasketing, and precision in multianvil experiments. American Mineralogist, 76, 1092-1100.
67. Walter, M., Thibault, Y., Wei, K., and Luth, R.W. (1995) Characterizing pressure and temperature conditions in multi-anvil apparatus. Canadian Journal of Physics, 73, 273-286.
68. Wilkins, R.W.T. and Sabine, W. (1973) Water content of some nominally anhydrous silicates. American Mineralogist, 58, 508-516.
69. Wirth, R. (1997) Water in minerals detectable by electron energy-loss spectroscopy EELS. Physics and Chemistry of Minerals, 24, 561-568.
70. - (2004) A novel technology for advanced application of micro- and nanoanalysis in geosciences and applied mineralogy. European Journal of Mineralogy, 16, 863-876.
71. 4 and coexisting olivine: Implications for mantle evolution and dynamics. Physics and Chemistry of Minerals, 19, 409-422.
72. 3: In situ X-ray measurements using synchrotron radiation. Geophysical Research Letters, 12, 729-732.