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-1, KBr): 3298 (s), 3148 (m), 3130 (m), 1647 (s), 1625 (s), 1560 (w), 1520 (m), 1375 (s), 1358 (s), 1239 (m), 1110 (m), 1086 (m), 999 (m), 944 (w), 839 (m), 774 (w), 741 (w), 722 (m), 662(w).
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21
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77949539892
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note
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2 = 0.1386 [I > 2r(I)]. Structural data for 1 was collected on a Bruker Smart Apex CCD with graphitemonochromated MoKa radiation (λ = 0.71073 Å) at 293 K. Their structures were solved by direct methods and refined with the fullmatrix least-squares technique using the SHELXS-97 and SHELXL-97 programs [14]. Selected bond lengths and angles with their estimated standard deviations of 1 are listed in Table S1.
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