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Volumn 43, Issue 6, 2010, Pages 1075-1084

Development of a liquid chromatographic method for the simultaneous determination of six benzodiazepines in human plasma after solid-phase extraction

Author keywords

Benzodiazepines; HPLC DAD; Plasma; Solid phase extraction

Indexed keywords


EID: 77949328465     PISSN: 00032719     EISSN: 1532236X     Source Type: Journal    
DOI: 10.1080/00032710903492490     Document Type: Article
Times cited : (19)

References (33)
  • 1
    • 0034536665 scopus 로고    scopus 로고
    • Screening, identification and quantitation of benzodiazepines in serum by solid phase extraction on a cyanopropyl phase using high performance liquid chromatography and photodiode array detection
    • Ahrens, B., H. J. Schwandt, and H. Schutz. 2000. Screening, identification and quantitation of benzodiazepines in serum by solid phase extraction on a cyanopropyl phase using high performance liquid chromatography and photodiode array detection. Arzneim.-Forsch. 50: 1057-1062.
    • (2000) Arzneim.-forsch , vol.50 , pp. 1057-1062
    • Ahrens, B.1    Schwandt, H.J.2    Schutz, H.3
  • 2
    • 0032968129 scopus 로고    scopus 로고
    • A modified simple and rapid reversed phase liquid chromatographic method for quantification of diazepam and nordiazepam in plasma
    • Atta Politou, J., M. Parissi-Poulou, A. Dona, and A. Koutselinis. 1999. A modified simple and rapid reversed phase liquid chromatographic method for quantification of diazepam and nordiazepam in plasma. J. Pharm. Biomed. Anal. 20: 389-396.
    • (1999) J. Pharm. Biomed. Anal , vol.20 , pp. 389-396
    • Atta Politou, J.1    Parissi-Poulou, M.2    Dona, A.3    Koutselinis, A.4
  • 4
    • 0017327442 scopus 로고
    • Determination of clorazepate and its major metabolites in blood and urine by electron capture gas-liquid chromatography
    • Brooks, M. A., M. R. Hackman, R. E. Weinfeld, and T. Macasieb. 1977. Determination of clorazepate and its major metabolites in blood and urine by electron capture gas-liquid chromatography. J. Chromatogr. 135: 123-131.
    • (1977) J. Chromatogr , vol.135 , pp. 123-131
    • Brooks, M.A.1    Hackman, M.R.2    Weinfeld, R.E.3    Macasieb, T.4
  • 5
    • 2342642079 scopus 로고    scopus 로고
    • Rapid analysis of benzodiazepines in whole blood by high-performance liquid chromatography: Use of a monolithic column
    • Bugey, A., and C. Staub. 2004. Rapid analysis of benzodiazepines in whole blood by high-performance liquid chromatography: Use of a monolithic column. J. Pharm. Biomed. Anal. 35: 555-562.
    • (2004) J. Pharm. Biomed. Anal , vol.35 , pp. 555-562
    • Bugey, A.1    Staub, C.2
  • 6
    • 33748693570 scopus 로고    scopus 로고
    • A high-throughput urinalysis of abused drugs based on a SPE-LC-MS=MS method coupled with an in-house developed post-analysis data treatment system
    • Cheng, W.-C., T.-S. Yau, M.-K. Wong, L.-P. Chan, and Vk. K. Mok. 2006. A high-throughput urinalysis of abused drugs based on a SPE-LC-MS=MS method coupled with an in-house developed post-analysis data treatment system. Forensic Sci. Int. 162: 95-107.
    • (2006) Forensic Sci. Int , vol.162 , pp. 95-107
    • Cheng, W.-C.1    Yau, T.-S.2    Wong, M.-K.3    Chan, L.-P.4    Vk, M.K.5
  • 7
    • 4644363459 scopus 로고    scopus 로고
    • Determination of bromazepam, clonazepam and metabolites after a single intake in urine and hair by LC-MS=MS. Application to forensic cases of drug facilitated crimes
    • Chèze, M., M. Villain, and G. Pépin. 2004. Determination of bromazepam, clonazepam and metabolites after a single intake in urine and hair by LC-MS=MS. Application to forensic cases of drug facilitated crimes. Forensic Sci. Int. 145: 123-130.
    • (2004) Forensic Sci. Int , vol.145 , pp. 123-130
    • Chèze, M.1    Villain, M.2    Pépin, G.3
  • 8
    • 0034064114 scopus 로고    scopus 로고
    • Simultaneous determination of diazepam, oxazepam and temazepam in spiked urine by HPLC
    • El-Gizawy, S. M. 2000. Simultaneous determination of diazepam, oxazepam and temazepam in spiked urine by HPLC. Anal. Letters 33: 629-638.
    • (2000) Anal. Letters , vol.33 , pp. 629-638
    • El-Gizawy, S.M.1
  • 9
    • 0034663838 scopus 로고    scopus 로고
    • Simultaneous determination of benzodiazepines in whole blood or serum by HPLC=DAD with a semi-micro column
    • El Mahjoub, A., and C. Staub. 2000. Simultaneous determination of benzodiazepines in whole blood or serum by HPLC=DAD with a semi-micro column. J. Pharm. Biomed. Anal. 23: 447-458.
    • (2000) J. Pharm. Biomed. Anal , vol.23 , pp. 447-458
    • El Mahjoub, A.1    Staub, C.2
  • 10
    • 0035543083 scopus 로고    scopus 로고
    • Determination of midazolam in human plasma by solid-phase microextraction and gas chromatography=mass spectrometry. Rapid Commun
    • Frison, G., L. Tedeschi, S. Maietti, and S. D. Ferrara. 2001. Determination of midazolam in human plasma by solid-phase microextraction and gas chromatography=mass spectrometry. Rapid Commun. Mass Spectrom. 15: 2497-2501.
    • (2001) Mass Spectrom , vol.15 , pp. 2497-2501
    • Frison, G.1    Tedeschi, L.2    Maietti, S.3    Ferrara, S.D.4
  • 11
    • 0029080277 scopus 로고
    • High-performance liquid chromato- graphy of alprazolam in postmortem blood using solid-phase extraction
    • Hall, M. A., C. A. Robinson, and R. M. Brissie. 1995. High-performance liquid chromato- graphy of alprazolam in postmortem blood using solid-phase extraction. J. Anal. Toxicol. 19: 511-513.
    • (1995) J. Anal. Toxicol , vol.19 , pp. 511-513
    • Hall, M.A.1    Robinson, C.A.2    Brissie, R.M.3
  • 12
    • 11844296022 scopus 로고    scopus 로고
    • Solid-phase extraction of methadone enantiomers and benzodiazepines in biological fluids by two polymeric cartridges for liquid chromatographic analysis
    • He, H., C. Sun, X.-R. Wang, C. Pham-Huy, N. Chikhi-Chorfi, H. Galons, M. Thevenin, J.-R. Claude, and J.-M. Warnet. 2005. Solid-phase extraction of methadone enantiomers and benzodiazepines in biological fluids by two polymeric cartridges for liquid chromatographic analysis. J. Chromatogr. B 814: 385-391.
    • (2005) J. Chromatogr. B , vol.814 , pp. 385-391
    • He, H.1    Sun, C.2    Wang, X.-R.3    Pham-Huy, C.4    Chikhi-Chorfi, N.5    Galons, H.6    Thevenin, M.7    Claude, J.-R.8    Warnet, J.-M.9
  • 13
    • 0031689081 scopus 로고    scopus 로고
    • Determination of benzodiazepines in forensic samples by HPLC with photo-diode array detection
    • He, W., N. Parissis, and T. Kiratzidis. 1998. Determination of benzodiazepines in forensic samples by HPLC with photo-diode array detection. J. Forensic Sci. 43: 1061-1067.
    • (1998) J. Forensic Sci , vol.43 , pp. 1061-1067
    • He, W.1    Parissis, N.2    Kiratzidis, T.3
  • 14
    • 0343878145 scopus 로고    scopus 로고
    • Screening and determination of benzodiazepines in whole blood using solid-phase extraction and gas chromatography=mass spectrometry
    • Inoue, H., Y. Maeno, M. Iwasa, R. Matoba, and M. Nagao. 2000. Screening and determination of benzodiazepines in whole blood using solid-phase extraction and gas chromatography=mass spectrometry. Forensic Sci. Int. 113: 367-373.
    • (2000) Forensic Sci. Int , vol.113 , pp. 367-373
    • Inoue, H.1    Maeno, Y.2    Iwasa, M.3    Matoba, R.4    Nagao, M.5
  • 15
    • 24144434966 scopus 로고    scopus 로고
    • Screening and confirmatory method for benzodiazepines and hypnotics in oral fluid by LC-MS=MS
    • Kintz, P., M. Villain, M. Concheiro, and V. Cirimele. 2005. Screening and confirmatory method for benzodiazepines and hypnotics in oral fluid by LC-MS=MS. Forensic Sci. Int. 150: 213-220.
    • (2005) Forensic Sci. Int , vol.150 , pp. 213-220
    • Kintz, P.1    Villain, M.2    Concheiro, M.3    Cirimele, V.4
  • 16
    • 0037605911 scopus 로고    scopus 로고
    • Evaluation of immunochemical drug screenings of whole blood samples. A retrospective optimization of cutoff levels after confirmation-analysis on GC-MS and HPLC-DAD
    • Kroener, L., F. Musshoff, and B. Madea. 2003. Evaluation of immunochemical drug screenings of whole blood samples. A retrospective optimization of cutoff levels after confirmation-analysis on GC-MS and HPLC-DAD. J. Anal. Toxicol. 27: 205-212.
    • (2003) J. Anal. Toxicol , vol.27 , pp. 205-212
    • Kroener, L.1    Musshoff, F.2    Madea, B.3
  • 17
    • 0031557147 scopus 로고    scopus 로고
    • Automated on-line solid-phase extraction-gas chromatography with nitrogen-phosphorus detection: Determination of benzodiazepines in human plasma
    • Louter, A. J. H., E. Bosma, J. C. A. Schipperen, J. J. Vreuls, and U. A. T. Brinkman. 1997. Automated on-line solid-phase extraction-gas chromatography with nitrogen-phosphorus detection: Determination of benzodiazepines in human plasma. J. Chromatogr. B 689: 35-43.
    • (1997) J. Chromatogr. B , vol.689 , pp. 35-43
    • Louter, A.J.H.1    Bosma, E.2    Schipperen, J.C.A.3    Vreuls, J.J.4    Brinkman, U.A.T.5
  • 18
    • 50949099589 scopus 로고    scopus 로고
    • Quantitation of benzodiazepines in urine, serum, plasma, and meconium by LC-MS-MS
    • Marín, S. J., R. Coles, M. Merrell, and G. A. McMillin. 2008. Quantitation of benzodiazepines in urine, serum, plasma, and meconium by LC-MS-MS. J. Anal. Toxicol. 32: 491-498.
    • (2008) J. Anal. Toxicol , vol.32 , pp. 491-498
    • Marín, S.J.1    Coles, R.2    Merrell, M.3    McMillin, G.A.4
  • 19
    • 21144443914 scopus 로고    scopus 로고
    • Simultaneous analysis of seven benzodiazepines in dietary supplements as adulterants using high performance liquid chromatography and its application to an identification system for diazepam
    • Mikami, E., T. Goto, T. Ohno, and H. Kanamori. 2005. Simultaneous analysis of seven benzodiazepines in dietary supplements as adulterants using high performance liquid chromatography and its application to an identification system for diazepam. J. Health Sci. 51: 278-283.
    • (2005) J. Health Sci , vol.51 , pp. 278-283
    • Mikami, E.1    Goto, T.2    Ohno, T.3    Kanamori, H.4
  • 20
    • 30944443337 scopus 로고    scopus 로고
    • A method for screening for various sedative-hypnotics in serum by liquid chromatography=single quadrupole mass spectrometry
    • Miyaguchi, H., K. Kuwayama, K. Tsujikawa, T. Kanamori, Y. T. Iwata, H. Inoue, and T. Kishi. 2006. A method for screening for various sedative-hypnotics in serum by liquid chromatography=single quadrupole mass spectrometry. Forensic Sci. Int. 157: 57-70.
    • (2006) Forensic Sci. Int , vol.157 , pp. 57-70
    • Miyaguchi, H.1    Kuwayama, K.2    Tsujikawa, K.3    Kanamori, T.4    Iwata, Y.T.5    Inoue, H.6    Kishi, T.7
  • 21
    • 0035949836 scopus 로고    scopus 로고
    • High-performance liquid chromatographic determination of diazepam in plasma of children with severe malaria
    • Muchohi, S. N., B. R. Ogutu, C. R. J. C. Newton, and G. O. Kokwaro. 2001. High-performance liquid chromatographic determination of diazepam in plasma of children with severe malaria. J. Chromatogr. B 761: 255-259.
    • (2001) J. Chromatogr. B , vol.761 , pp. 255-259
    • Muchohi, S.N.1    Ogutu, B.R.2    Newton, C.R.J.C.3    Kokwaro, G.O.4
  • 22
    • 0036827348 scopus 로고    scopus 로고
    • Bioanalytical method validation and its implications for forensic and clinical toxicology-a review
    • Peters, F. J., and H. H. Maurer. 2002. Bioanalytical method validation and its implications for forensic and clinical toxicology-a review. Accred. Qual. Assur. 7: 441-449.
    • (2002) Accred. Qual. Assur , vol.7 , pp. 441-449
    • Peters, F.J.1    Maurer, H.H.2
  • 23
    • 2942564444 scopus 로고    scopus 로고
    • Development and validation of a gas chromatography-mass spectrometry method for the simultaneous determination of buprenorphine, flunitrazepam and their metabolites in rat plasma: Application to the pharmacokinetic study
    • Pirnay, S., S. Bouchonnet, F. Hervé, D. Libong, N. Milan, P. d'Athis, F. Baud, and I. Ricordel. 2004. Development and validation of a gas chromatography-mass spectrometry method for the simultaneous determination of buprenorphine, flunitrazepam and their metabolites in rat plasma: Application to the pharmacokinetic study. J. Chromatogr. B 807: 335-342.
    • (2004) J. Chromatogr. B , vol.807 , pp. 335-342
    • Pirnay, S.1    Bouchonnet, S.2    Hervé, F.3    Libong, D.4    Milan, N.5    d'Athis, P.6    Baud, F.7    Ricordel, I.8
  • 24
    • 0344628591 scopus 로고    scopus 로고
    • Simultaneous determination of benzodiazepines in whole blood or serum by HPLC=DAD with a semimicro column
    • Pistos, C., and J. T. Stewart. 2003. Simultaneous determination of benzodiazepines in whole blood or serum by HPLC=DAD with a semimicro column. J. Pharm. Biomed. Anal. 33: 1135-1142.
    • (2003) J. Pharm. Biomed. Anal , vol.33 , pp. 1135-1142
    • Pistos, C.1    Stewart, J.T.2
  • 25
    • 24344483851 scopus 로고    scopus 로고
    • Liquid chromatography-electrospray ionisation mass spectrometry for the determination of nine selected benzodiazepines in human plasma and oral fluid
    • Quintela, O., A. Cruz, A. De Castro, M. Concheiro, and M. Lóez-Rivadulla. 2005. Liquid chromatography-electrospray ionisation mass spectrometry for the determination of nine selected benzodiazepines in human plasma and oral fluid. J. Chromatogr. B 825: 63-71.
    • (2005) J. Chromatogr. B , vol.825 , pp. 63-71
    • Quintela, O.1    Cruz, A.2    de Castro, A.3    Concheiro, M.4
  • 26
    • 34047214041 scopus 로고    scopus 로고
    • Development of a validated HPLC method for the determination of four 1,4-benzodiazepines in human biological fluids
    • Samanidou, V. F., A. P. Pechlivanidou, and I. N. Papadoyannis. 2007. Development of a validated HPLC method for the determination of four 1,4-benzodiazepines in human biological fluids. J. Sep. Sci. 30: 679-687.
    • (2007) J. Sep. Sci , vol.30 , pp. 679-687
    • Samanidou, V.F.1    Pechlivanidou, A.P.2    Papadoyannis, I.N.3
  • 27
    • 0035096749 scopus 로고    scopus 로고
    • Analytical methodology for the detection of benzodiazepine consumption in opioid-dependent subjects
    • Segura, M., J. Barbosa, M. Torrens, M. Farré, C. Castillo, and J. Segura. 2001. Analytical methodology for the detection of benzodiazepine consumption in opioid-dependent subjects. J. Anal. Toxicol. 25: 130-136.
    • (2001) J. Anal. Toxicol , vol.25 , pp. 130-136
    • Segura, M.1    Barbosa, J.2    Torrens, M.3    Farré, M.4    Castillo, C.5    Segura, J.6
  • 29
    • 5344229411 scopus 로고    scopus 로고
    • Quantitative analysis of 33 benzodiazepines, metabolites and benzodiazepine-like substances in whole blood by liquid chromatography-(tandem) mass spectrometry
    • Smink, B. E., J. E. Brandsma, A. Dijkhuizen, K. J. Lusthof, J. J. De Gier, A. C. G. Egberts, and D. R. A. Uges. 2004. Quantitative analysis of 33 benzodiazepines, metabolites and benzodiazepine-like substances in whole blood by liquid chromatography-(tandem) mass spectrometry. J. Chromatogr. B 811: 13-20.
    • (2004) J. Chromatogr. B , vol.811 , pp. 13-20
    • Smink, B.E.1    Brandsma, J.E.2    Dijkhuizen, A.3    Lusthof, K.J.4    de Gier, J.J.5    Egberts, A.C.G.6    Uges, D.R.A.7
  • 30
    • 0035188554 scopus 로고    scopus 로고
    • Serum and urine concentrations of flunitrazepam and metabolites, after a single oral dose, by immunoassay and GC-MS
    • Snyder, H., K. S. Schwenzer, R. Pearlman, A. J. Mcnally, M. Tsilimidos, and S. J. Salamone. 2001. Serum and urine concentrations of flunitrazepam and metabolites, after a single oral dose, by immunoassay and GC-MS. J. Anal. Toxicol. 25: 699-704.
    • (2001) J. Anal. Toxicol , vol.25 , pp. 699-704
    • Snyder, H.1    Schwenzer, K.S.2    Pearlman, R.3    McNally, A.J.4    Tsilimidos, M.5    Salamone, S.J.6
  • 31
    • 0000832772 scopus 로고    scopus 로고
    • Simultaneous determination of twelve benzodiazepines in human serum using a new reversed-phase chromatographic column on a 2-mm porous microspherical silica gel
    • Tanaka, E., M. Terada, S. Misawa, and C. Wakasugi. 1996. Simultaneous determination of twelve benzodiazepines in human serum using a new reversed-phase chromatographic column on a 2-mm porous microspherical silica gel. J. Chromatogr. B 682: 173-178.
    • (1996) J. Chromatogr. B , vol.682 , pp. 173-178
    • Tanaka, E.1    Terada, M.2    Misawa, S.3    Wakasugi, C.4
  • 32
    • 58749109242 scopus 로고    scopus 로고
    • Validation of SPE-HPLC determination of 1,4-benzodiazepines and metabolites in blood, plasma, urine, and saliva
    • Uddin, M. N., V. F. Samanidou, and I. N. Papadoyannis. 2008. Validation of SPE-HPLC determination of 1,4-benzodiazepines and metabolites in blood, plasma, urine, and saliva. J. Sep. Sci. 31: 3704-3717.
    • (2008) J. Sep. Sci , vol.31 , pp. 3704-3717
    • Uddin, M.N.1    Samanidou, V.F.2    Papadoyannis, I.N.3


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