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note
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6S (304.3): C, 55.26; H, 2.65%. Found: C, 54.90, H, 2.72%.
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19
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76149115730
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note
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2O (744.0): C, 45.20; H, 2.98%. Found: C, 45.30, H, 2.99%. Details of the crystal structure of the compound are available free of charge via Cambridge Crystallographic Data Centre under deposition number CCDC-749400.
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20
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76149085358
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note
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2O/DMSO because the solubility of these ligands in water was poor. The values in a mixture of water and organic solvent are higher than in water.
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21
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76149117065
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note
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For the electrical conductivity study, the powdered sample was compressed to approximately 0.5 mm in thickness and 2.5 mm in diameter. Both sides of the pellet were attached to gold wires with gold paste. The conductivity measurement was carried out using a Solartron 1260 impedance/gain-phase analyzer by a quasi-fourprobe method in the frequency range 10 MHz to 1Hz. Proton conductivity was calculated from the diameter of the semicircle. Samples were placed in a temperature-humidity-controlled chamber (SH221, ESPEC Corp.) during the measurement.
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