Aluminum-rich belite sulfoaluminate cements: Clinkering and early age hydration

Cement and Concrete Research

Volumn 40, Issue 3, 2010, Pages 359-369

  Martín Sedeño, M Carmen ^a   Cuberos, Antonio J M ^a   De la Torre, Ángeles G ^a   Álvarez Pinazo, Gema ^a   Ordónez, Luis M ^b   Gateshki, Milen ^c   Aranda, Miguel A G ^a  

^a UNIVERSITY OF MÁLAGA   (Spain)

^b AIDICO   (Spain)

^c MALVERN INSTRUMENTS LTD   (United Kingdom)

Author keywords

3CaO 3Al2O3 CaSO4 (D); Belite sulfoaluminate cement (D); Clinkerization (E); Hydration (A); Quantitative mineralogical phase analysis (B)

Indexed keywords

AMORPHOUS PHASIS; BELITE CEMENTS; BELITE SULFOALUMINATE CEMENT (D); CEMENT PASTE; CLINKERIZATION; EARLY AGE; ENVIRONMENTALLY FRIENDLY BUILDINGS; EXPERIMENTAL CONDITIONS; FREE WATER; HIGH TEMPERATURE; HYDRATION PROCESS; MINERALOGICAL COMPOSITIONS; NOMINAL COMPOSITION; ORDINARY PORTLAND CEMENT; PHASE ANALYSIS; PHASE ASSEMBLAGES; PHASE EVOLUTIONS; QUANTITATIVE PHASE ANALYSIS; RIETVELD; S-PHASE; SULFOALUMINATE; SULFOALUMINATE CEMENT; THERMOGRAVIMETRY;

ALUMINUM; BODY FLUIDS; BUILDING MATERIALS; CONSTRUCTION EQUIPMENT; DIFFRACTION; GYPSUM; HYDRATION; ISOMERS; PORTLAND CEMENT; RIETVELD METHOD; THERMOANALYSIS; X RAY POWDER DIFFRACTION;

RIETVELD ANALYSIS;

EID: 74449091886     PISSN: 00088846     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.cemconres.2009.11.003     Document Type: Article

References (73)

1. Damtoft J.S., Lukasik J., Herfort D., Sorrentino D., and Gartner E.M. Sustainable development and climate change initiatives. Cem. Concr. Res. 38 2 (2008) 115-127
2. 2" cements. Cem. Concr. Res. 34 9 (2004) 1489-1498
3. Chatterjee A.K. High belite cements. Present status and future technological options: Part I and Part II. Cem. Concr. Res. 26 8 (1996) 1213-1237
4. De la Torre A.G., Aranda M.A.G., De Aza A.H., Pena P., and De Aza S. Belite portland clinkers. Synthesis and mineralogical analysis. Bol. Soc. Esp. Ceram. Vidr. 44 3 (2005) 185-191
5. Popescu C.D., Muntean M., and Sharp J.H. Industrial trial production of low energy belite cement. Cem. Concr. Compos. 25 7 (2003) 689-693
6. Glasser F.P., and Zhang L. High-performance cement matrices based on calcium sulfoaluminate-belite compositions. Cem. Concr. Res. 31 (2001) 1881-1886
7. Zhang L., Su M.Z., and Wang Y.M. Development of the use of sulfo- and ferro-aluminate cements in China. Adv. Cem. Res 11 (1999) 15-21
8. Stark J., Muller A., Seydel R., and Jost K. Conditions of the existence of hydraulically active belite cement. Proceedings of the 8th International Congress of Cement Chemistry, Rio de Janeiro vol. II (1986) 306-309
9. Gies A., and Knofel D. Influence of alkalies on the composition of belite-rich cement clinkers and the technological properties of the resulting cements. Cem. Concr. Res. 16 3 (1986) 411-422
10. Morsli K., de la Torre A.G., Stöber S., Cuberos A.J.M., Zahir M., and Aranda M.A.G. Quantitative phase analysis of laboratory active belite clinkers by synchrotron powder diffraction. J. Am. Ceram. Soc. 90 10 (2007) 3205-3212
11. Morsli K., de la Torre A.G., Zahir M., and Aranda M.A.G. Mineralogical phase analysis of alkali and sulfate bearing belite rich laboratory clinkers. Cem. Concr. Res. 37 (2007) 639-646
12. G.S. Li, E.M. Gartner, High-belite sulfoaluminate clinker: fabrication process and binder preparation, French patent application 04-51586 (publication 2873366), 27/01/2006.
13. Taylor H.F.W. Cement Chemistry (1997), Thomas Telford, London
14. Quillin K. Performance of belite-sulfoaluminate cements. Cem. Concr. Res. 31 (2001) 1341-1349
15. Lawrence C.D. The production of low-energy cements. In: Bensted J., and Barnes P. (Eds). Structures and performance of cements (2002), Spon Spress, London
16. 3$ content. Ceram.-Silik. 51 (2007) 74-81
17. Adolfsson D., Menad N., Viggh E., and Bjorkman B. Hydraulic properties of sulphoaluminate belite cement based on steelmaking slags. Adv. Cem. Res 19 (2007) 133-138
18. Pera J., and Ambroise J. New applications of calcium sulfoaluminate cement. Cem. Concr. Res. 34 (2004) 671-676
19. Wolter A. Belite cements and low energy clinker. Cem. Int. 3 (2005) 106-117
20. Valenti G.L., Marroccoli M., Montagnaro F., Nobili M., and Telesca A. Synthesis, hydration properties and environmental friendly features of calcium sulfoaluminate cements. Proceedings of the 12th International Congress of Cement Chemistry, Montreal (2007) W3 11.2
21. 3. Cem. Concr. Res. 9 (1979) 51-56
22. Arjunan P., Silsbee M.R., and Roy D.M. Sulfoaluminate-belite cement from low-calcium fly ash and sulfur-rich and other industrial by-products. Cem. Concr. Res. 29 (1999) 1305-1311
23. Li H., Agrawal D.K., Cheng J., and Silsbee M.R. Microwave sintering of sulphoaluminate cement with utility wastes. Cem. Concr. Res. 31 (2001) 1257-1261
24. F.P. Glasser, L. Zhang, Calculation of the chemical water demand for hydration of calcium sulfoaluminate cement, Proceedings of the 4th Beijing International Symposium on Cement and Concrete, vol. 3, International Academic Publishers, Beijing, 1998, pp. 97-108.
25. Glasser F.P., and Zhang L. Hydration of calcium sulfoaluminate cement at less than 24 h. Adv. Cem. Res 11 1 (1999) 35-41
26. Rietveld H.M. A profile refinement method for nuclear and magnetic structures. J. Appl. Crystallogr. 2 2 (1969) 65-71
27. De la Torre A.G., Cabeza A., Calvente A., Bruque S., and Aranda M.A.G. Full phase analysis of Portland clinker by penetrating synchrotron powder diffraction. Anal. Chem. 73 (2001) 151-156
28. Scarlett N.V.Y., Madsen I.C., Manias C., and Retallack D. On-line X-ray diffraction for quantitative phase analysis: Application in the Portland cement industry. Powder Diffr. 16 2 (2001) 71-80
29. De la Torre A.G., and Aranda M.A.G. Accuracy in Rietveld quantitative phase analysis of Portland cements. J. Appl. Crystallogr. 36 5 (2003) 1169-1176
30. Peterson V.K., Ray A.S., and Hunter B.A. A comparative study of Rietveld phase analysis of cement clinker using neutron, laboratory X-ray, and synchrotron data. Powder Diffr. 21 1 (2006) 12-18
31. León-Reina L., De la Torre A.G., Porras-Vázquez J.M., Cruz M., Ordonez L.M., Alcobé X., Gispert-Guirado F., Larrañaga-Varga A., Paul M., Fuellmann T., Schmidt R., and Aranda M.A.G. Round robin on Rietveld quantitative phase analysis of Portland cements. J. Appl. Crystallogr. 42 (2009) 906-916
32. De la Torre A.G., Bruque S., and Aranda M.A.G. Rietveld quantitative amorphous content analysis. J. Appl. Crystallogr. 34 (2001) 196-202
33. Scrivener K.L., Fullmann T., Gallucci E., Walenta G., and Bermejo E. Quantitative study of Portland cement hydration by X-ray diffraction/Rietveld analysis and independent methods. Cem. Concr. Res. 34 9 (2004) 1541-1547
34. Hesse C., Goetz-Neunhoeffer F., Neubauer J., Braeu M., and Gaeberlein P. Quantitative in situ X-ray diffraction analysis of early hydration of Portland cement at defined temperatures. Powder Diffr. 24 (2009) 112-115
35. Jupe A.C., Turrillas X., Barnes P., Colston S.L., Hall C., Häusermann D., and Hanfland M. Fast in situ X-ray diffraction studies of chemical reactions: a synchrotron view of the hydration of tricalcium aluminate. Phys. Rev., B 53 (1996) R14697-R14700
36. Matschei T., Lothenbach B., and Glasser F.P. The AFm phase in Portland cement. Cem. Concr. Res. 37 (2007) 118-130
37. Havlica J., and Sahu S. Mechanism of ettringite and monosulphate formation. Cem. Concr. Res. 22 (1992) 671-677
38. Meneghini C., Artioli G., Balerna A., Gualtieri A.F., and Norby P. Multipurpose imaging-plate camera for in-situ powder XRD at the GILDA beamline. J. Synchrotron Radiat. 8 (2001) 1162-1166
39. Hammersley A.P., Svensson S.O., Hanfland M., Fitch A.N., and Häusermann D. Two-dimensional detector software: from real detector to idealised image or two-theta scan. High Press. Res. 14 (1996) 235-248
40. Larson A.C., and Von Dreele R.B. General Structure Analysis System (GSAS), Los Alamos National Laboratory Report LAUR 86-748 (2000)
41. 3. J. Appl. Crystallogr. 20 2 (1987) 79-83
42. Finger L.W., Cox D.E., and Jephcoat A.P. A correction for powder diffraction peak asymmetry due to diaxial divergence. J. Appl. Crystallogr. 27 (1994) 892-900
43. Mumme W.G., Hill R.J., Bushnell-Wye G., and Segnit E.R. Rietveld structure refinement, crystal chemistry and calculated powder diffraction data for the polymorphs of dicalcium silicate and related phases. Neues Jahrb. Mineral. Abh. 169 (1995) 35-68
44. Udagawa S., Urabe K., Natsume M., and Yano T. Refinement of the crystal-structure of -Ca2SiO4. Cem. Concr. Res. 10 2 (1980) 139-144
45. 16S. J. Solid State Chem. 119 (1995) 1-7
46. Saalfeld H., and Depmeier W. Silicon-free compounds with sodalite structure. Krist. Tech. 7 (1972) 229-233
47. 4. J. Inorg. Nucl. Chem. 38 5 (1976) 983-984
48. Palacios L., De la Torre A.G., Bruque S., García Muñoz J.L., García-Granda S., Sheptyakov D., and Aranda M.A.G. Crystal structures and in-situ formation study of mayenita electrides. Inorg. Chem. 46 (2007) 4167-4176
49. 2. Kristallografiya 15 (1970) 1140-1143
50. 6. Acta Crystallogr., B 31 (1975) 689-697
51. 7. Neues Jahrb. Mineral. Abh. 144 (1982) 254-267
52. Natta G., and Passerini L. Soluzioni solide, isomorfismo e simmorfismo tra gli ossidi dei metallic bivalenti. Sistemi: CaO-CdO, CaO-MnO, CaO-CoO, CaO-NiO, CaO-MgO. Gazz. Chim. Ital. 59 (1929) 129-154
53. 4 from X-ray and neutron diffraction. Acta Crystallogr., B 36 (1980) 2881-2890
54. De la Torre A.G., López-Olmo M.G., Álvarez-Rua C., García-Granda S., and Aranda M.A.G. Structure and microstructure of gypsum and its relevance to Rietveld quantitative phase analyses. Powder Diffr. 19 (2004) 240-246
55. Goetz-Neunhoeffer F., and Neubauer J. Refined ettringite (Ca6Al2(SO4)3(OH)12 26H2O structure for quantitative X-ray diffraction analysis. Powder Diffr. 21 1 (2006) 4-11
56. 2O. Neues Jahrb. Mineral., Monatsh. (1977) 136-144
57. Guirado F., Galí S., Chinchón S., and Rius J. Crystal structure solution of hydrated high-alumina cement from X-ray powder diffraction data. Angew. Chem. Int. Ed. Commun. (1998) 72-75
58. 3, Z. Kristallogr. 139 (1974) 129-135.
59. Rinaldi R., Sacerdoti M., and Passaglia E. Straetlingite: crystal structure, chemistry, and a reexamination of its polytype vertumnite. Eur. J. Mineral. 2 (1990) 841-849
60. Sanz J., Madani A., Serratosa J.M., Moya J.S., and De Aza S. Aluminium-27 and silicon-29 magic-angle spining nuclear magnetic resonance study of the kaolinite-mullite transformation. J. Am. Ceram. Soc. 71 10 (1988) C418-C421
61. 27Al MAS-NMR investigation. J. Am. Ceram. Soc. 74 10 (1991) 2398-2403
62. 33 pseudobinary system. J. Am. Ceram. Soc. 31 (2001) 1185-1189
63. Odler I. Special Inorganic cements (2000), Taylor and Francis Publisher 69-74 Chapter 4
64. Lawrence C.D. The production of low-energy cements. Lea's chemistry of cement and concrete Chapter 9 (1998) 421-470
65. Jun-An D., Wen-Min G., Mu-Zhen S., and Xiu-Ying L. Sulfoaluminate cement series. Proceedings of the 7th International Congress of Cement Chemistry, Paris vol. V (1980) 381-386
66. Scrivener K.L., and Capmas A. Calcium Aluminate Cements. Lea's Chemistry of Cement and Concrete Chapter 13 (1998) 709-771
67. 3$ in air. Cem. Concr. Res. 38 2 (1995) 572-580
68. 3 Portland clinkers and cements I. Clinker synthesis and cement preparation. Cem. Concr. Res. 26 9 (1996) 1307-1313
69. Kacimi L., Simon-Masseron A., Ghomari A., and Derriche Z. Reduction of clinkerization temperature by using phosphogypsum. J. Hazard. Mater. B137 (2006) 129-137
70. Gartner E.M., Young J.F., Damidot D.A., and Jawed I. Hydration of Portland cement. In: Bensted J., and Barnes P. (Eds). Structures and performance of cements (2002), Spon Spress, London
71. 8. Thermochim. Acta 464 (2007) 7-15
72. Bensted J. Calcium aluminate cements. In: Bensted J., and Barnes P. (Eds). Structure and Performance of Cements (2002), Spon Spress, London
73. Cuberos A.J.M., De la Torre A.G., Martín-Sedeño M.C., Moreno-Real L., Merlini M., Ordónez L.M., and Aranda M.A.G. Phase development in conventional and active belite cement pastes by Rietveld analysis and chemicals constraints. Cem. Concr. Res. 39 10 (2009) 833-842