Quantitative phase analysis of laboratory-active belite clinkers by synchrotron powder diffraction

Journal of the American Ceramic Society

Volumn 90, Issue 10, 2007, Pages 3205-3212

  Morsli, Khadija ^a,b   De La Torre, Ángeles G ^a   Stöber, Stephan ^c   Cuberos, Antonio J M ^a   Zahir, Mohammed ^b   Aranda, Miguel A G ^a  

^a UNIVERSITY OF MÁLAGA   (Spain)

^b FACULTÉ DES SCIENCES   (Morocco)

^c MARTIN LUTHER UNIVERSITY HALLE WITTENBERG   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

CALORIMETRY; DIFFRACTION; HYDRATION; PORTLAND CEMENT; SALTS; SILICATES; STABILIZATION; SYNCHROTRONS;

ALUMINATES; CLINKERS; PHASE-ENRICHED RESIDUES; QUANTITATIVE PHASE ANALYSIS;

KILNS;

EID: 34548819931     PISSN: 00027820     EISSN: 15512916     Source Type: Journal    
DOI: 10.1111/j.1551-2916.2007.01870.x     Document Type: Article

References (54)

1. R. McCaffrey Climate Change and the Cement Industry Global Cem. Lime Mag., Environ. Spec. Issue, 15 9 (2002).
2. F. W. Locher Low Energy Clinker pp. 57 67 in Proceedings of the 8th International Congress of Cement Chemistry, Vol. I, Rio de Janeiro, Edited by Abla Grafica e Editora Ldta. 1986.
3. G. K. Moir F. P. Glasser Mineralisers, Modifiers and Activators in the Clinkering Process pp. 125 52 in Proceedings of the 9th International Congress of Cement Chemistry, Vol. 1, New Delhi, Edited by National Council for Cement and Building Materials. 1992.
4. P. K. Mehta Investigation on Energy-Saving Cements World Cem. Technol., 11 [5] 166 77 (1980).
5. A. K. Chatterjee Structure and Performance of Cements pp. 186 236 in Special Cements, Edited by J. Bensted P. Barnes. Published by Spon Spress, London, 2002.
6. P. Arjunan, M. R. Silsbee D. M. Roy Sulfoaluminate-Belite Cement from Low-Calcium Fly Ash and Sulfur-Rich and Other Industrial By-Products Cem. Concr. Res., 29 [8] 1305 11 (1999).
7. A. K. Chatterjee High Belite Cements. Present Status and Future Technological Options: Part I Cem. Concr. Res., 26 [8] 1213 25 (1996).
8. T. Sui, L. Fan, Z. Wen, J. Wang Z. Zhang Study of the Properties of High Strength Concrete Using High Belite Cement J. Adv. Concr. Technol., 2 [2] 201 6 (2004).
9. J. Stark, A. Muller, R. Seydel K. Jost Conditions of the Existence of Hydraulically Active Belite Cement pp. 306 9 in Proceedings of the 8th International Congress of Cement Chemistry, Vol. II, Rio de Janeiro, Edited by Abla Grafica e Editora Ldta. 1986.
10. 2" Cements Cem. Concr. Res., 34 [9] 1489 98 (2004).
11. C. D. Popescu, M. Muntean J. H. Sharp Industrial Trial Production of Low Energy Belite Cement Cem. Concr. Compos., 25 [7] 689 93 (2003).
12. H. F. W. Taylor Portland Cement and Its Major Constituent Phases pp. 1 28 in Cement Chemistry, 2nd edition. Thomas Telford Ltd., London, 1997.
13. S. N. Ghosh, P. B. Rao, A. K. Paul K. Raina Review. The Chemistry of Dicalcium Silicate Mineral J. Mater. Sci., 14, 1554 66 (1979).
14. I. Nettleship, K. G. Slavick, Y. J. Kim W. M. Kriven Phase Transformation in Dicalcium Silicate: I, Fabrication and Phase Stability of Fine-Grained Beta Phase J. Am. Ceram. Soc., 75 [9] 2400 6 (1992).
15. Y. J. Kim, I. Nettleship W. M. Kriven Phase Transformation in Dicalcium Silicate: II, TEM Studies of Crystallography, Microstructure and Mechanisms J. Am. Ceram. Soc., 75 [9] 2407 19 (1992).
16. K. Fukuda S. Ito Improvement in Reactivity and Grindability of Belite-Rich Cement by Remelting Reaction J. Am. Ceram. Soc., 82 [8] 2177 80 (1999).
17. A. Gies D. Knofel Influence of Alkalies on the Composition of Belite-Rich Cement Clinkers and the Technological Properties of the Resulting Cements Cem. Concr. Res., 16 [3] 411 22 (1986).
18. A. Guerrero, S. Goñi, A. Moragues J. S. Dolado Microstructure and Mechanical Performance of Belite from High Calcium Coal Fly Ash J. Am. Ceram. Soc., 88 [7] 1845 53 (2005).
19. A. Guerrero, S. Goñi, I. Campillo A. Moragues Belite Cement Clinker from Coal Fly Ash of High Ca Content. Optimization of Synthesis Parameters Environ. Sci. Technol., 38, 3209 13 (2004).
20. F. A. Rodrigues Low-Temperature Synthesis of Cements from Rice Hull Ash Cem. Concr. Res., 33 [10] 1525 9 (2003).
21. A. K. Chatterjee High Belite Cements. Future Technological Options: Part II Cem. Concr. Res., 26 [8] 1227 37 (1996).
22. H. M. Rietveld A Profile Refinement Method for Nuclear and Magnetic Structures J. Appl. Cryst., 2 [2] 65 71 (1969).
23. 3S from Synchrotron and Neutron Powder Diffraction and Its Role in Quantitative Phase Analyses Cem. Concr. Res., 32 [9] 1347 56 (2002).
24. A. H. de Aza, A. G. de la Torre, M. A. G. Aranda S. de Aza Quantitative Rietveld Analysis of Buen Retiro Porcelains J. Am. Ceram. Soc., 87 [3] 449 54 (2004).
25. A. G. de la Torre, A. Cabeza, A. Calvente, S. Bruque M. A. G. Aranda Full Phase Analysis of Portland Clinker by Penetrating Synchrotron Powder Diffraction Anal. Chem., 73 [2] 151 6 (2001).
26. A. G. de la Torre M. A. G. Aranda Accuracy in Rietveld Quantitative Phase Analysis of Portland Cements J. Appl. Cryst., 36 [5] 1169 76 (2003).
27. L. Wadso Applications of an Eight-Channel Isothermal Conduction Calorimeter for Cement Hydration Studies Cem. Int., 3, 94 101 (2005).
28. D. Schmitt, F. Goetz-Neunhoeffer J. Neubauer Investigations on the Hydration Behaviour of Synthetic OPC-Phases Alite and Belite by Heat-Flow Calorimetry pp. 279 87, Proceedings of the 11th International Congress of Cement Chemistry, Durban, 2003.
29. R. Mueller, J. Neubauer F. Goetz-Neunhoeffer Effects of Phosphate-Rich Raw Materials on the Crystallographic and Hydraulic Properties of Dicalcium Silicate pp. 1043 52, Proceedings of the 11th International Congress of Cement Chemistry, Durban, 2003.
30. K. Fukuda, N. Wakamatsu, S. Ito H. Yoshida Acceleration of Early Hydration in Belite-Rich Cement by Remelting Reaction J. Ceram. Soc. Jpn., 107 [10] 901 6 (1999).
31. K. Fukuda, N. Wakamatsu S. Ito Improvement in Hydration Reactivity of α-Phase Belite by Remelting Reaction J. Am. Ceram. Soc., 84 [3] 639 41 (2001).
32. A. G. de la Torre, M. A. G. Aranda, A. H. de Aza, P. Pena S. de Aza Belite Portland Clinker. Synthesis and Mineralogical Analysis Bol. Soc. Esp. Ceram. Vid., 44 [3] 185 91 (2005).
33. F. Triviño M. T. Blanco-Varela Determinación de la Composición Mineralógica del Clínker por Microscopía Cuantitativa, Disolución de Fases y Difracción de rayos-X (Clinker Mineralogical Composition Analysis Using Quantitative Microscopy, Phases Dissolution and X-Ray Diffraction) Materiales de la construcción, 190 1, 103 114 (1983).
34. W. A. Gutteridge On the Dissolution of the Interstitial Phases in Portland Cement Cem. Concr. Res., 9 [3] 319 24 (1979).
35. A. C. Larson R. B. Von Dreele. General Structure Analysis System (GSAS), Los Alamos National Laboratory Report LAUR 86-748, 2000.
36. 3 J. Appl. Cryst., 20 [2] 79 83 (1987).
37. W. E. Haskell Three Factors Govern Optimum Gypsum Content of Cement Rock Prod., 62, 108 49 (1959).
38. H. J. Kuzel A Simple Heat Conducting Calorimeter with High-Sensitivity Fortschr. Mineral., 60 [1] 128 9 (1982).
39. 4 Cem. Concr. Res., 10 [2] 139 44 (1980).
40. W. G. Mumme, R. J. Hill, G. Bushnell-Wye E. R. Segnit Rietveld Structure Refinement, Crystal Chemistry and Calculated Powder Diffraction Data for the Polymorphs of Dicalcium Silicate and Related Phases N. Jb. Miner. Abh., 169 [1] 35 68 (1995).
41. L. B. McCusker, R. B. Von Dreele, D. E. Cox, D. Louer P. Scardi Rietveld Refinement Guidelines J. Appl. Cryst., 32 [1] 36 50 (1999).
42. K. Fukuda, E. Iizuka, H. Taguchi S. Ito Effect of Crystal Grain Size and Thermal Stress on Martensitic Transformation of Phosphorus-Bearing Dicalcium Silicates J. Am. Ceram. Soc., 81 [10] 2729 31 (1998).
43. 4 Sov. Phys. Crystallogr., 35 [1] 91 3 (1990).
44. C. Remy, D. Andraul M. Madon High-Temperature, High-Pressure X-Ray Investigation of Dicalcium Silicate J. Am. Ceram. Soc., 80 [4] 851 60 (1997).
45. F. Dunstetter, M.-N. de Noirfontaine M. Courtial Polymorphism of Tricalcium Silicate, the Major Compound of Portland Cement Clinker. 1. Structural Data: Review and Unified Analysis Cem. Concr. Res., 36 [1] 39 53 (2006).
46. M.-N. de Noirfontaine, F. Dunstetter, M. Courtial, G. Gasecki M. Signes-Frehel Polymorphism of Tricalcium Silicate, the Major Compound of Portland Cement Clinker 2. Modelling Alite for Rietveld Analysis, an Industrial Challenge Cem. Concr. Res., 36 [1] 54 64 (2006).
47. 3S Sov. Phys. Crystallogr., 20 [4] 441 5 (1975).
48. 5 Acta Cryst., B27 [12] 2311 5 (1971).
49. J. Neubauer, H. J. Kuzel R. Sieber Rietveld Quantitative XRD Analysis of Portland Cement: II. Quantification of Synthetic and Technical Portland Cement Clinkers pp. 100 11, Proceedings of 18th International Conference on Cement Microscopy, Houston, 1996.
50. 2O Solid-Solution Series Z. Kristallogr., 152 [3-4] 259 307 (1980).
51. 3A Polymorphs Related to Industrial Clinker Alkalies Content Cem. Concr. Res., 34 [4] 657 64 (2004).
52. J. F. Young H. S. Tong Microstructure and Strength Development of Beta-Dicalcium Silicate Pastes with and without Admixtures Cem. Concr. Res., 7 [6] 627 36 (1977).
53. R. Delhez, T. H. de Keijser, J. I. Langford, D. Louer, E. J. Mittemeijer E. J. Sonneveld Crystal Imperfection Broadening and Peak Shape in the Rietveld Method pp. 132 66 in The Rietveld Method, Edited by R. A. Young. Oxford University Press, Oxford, 1993.
54. J. I. Langford D. Louer Powder Diffraction Rep. Prog. Phys., 59, 131 234 (1996).