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Volumn 13, Issue 2, 2010, Pages 223-226

Ligand concentration and reaction time controlled successive substitution of chloro and η6-benzene of di-μ-chlorobis{η6-benzene)dichlororuthenium(II)} with selenated Schiff base: Formation of half sandwich Ru(II) complex highly active catalyst for oxidation of alcohols

(4) Singh, Pradhumn a Das, Dipanwita a Singh, Monika a Singh, Ajai K a

a INDIAN INSTITUTE OF TECHNOLOGY DELHI (India)

Author keywords

Alcohols; Catalytic oxidation; Crystal structure; Half sandwich complex; Ruthenium(II); Selenated Schiff base

Indexed keywords

EID: 74149085841 PISSN: 13877003 EISSN: None Source Type: Journal
DOI: 10.1016/j.inoche.2009.11.011 Document Type: Article

Times cited : (13)

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- X-ray crystallography; Bruker AXS SMART Apex CCD diffractometer using Mo Kα (0.71073 Å) radiations at 298(2) K was used. Crystal data: 1: crystal system, triclinic; space group, P over(1, ̄, a, 11.445(3) Å; b, 11.967(3) Å; c, 14.921(4) Å; β, 100.77(4)°; Å3, 1954.8(9, Z, 2; F(0 0 0) 1044.0; absorption coeff, mm-1] 2.536 Independent reflections (Rint, 6890 (0.0324, data/restraints/parameters 6890/0/481; R indices (all data, R1, 0.0925; wR2, 0.1714; Largest diff. peak/hole [ye{cyrillic} Å-3] 1.421/-0.849; 2: crystal system, triclinic; space group, P over(1, ̄, a, 9.4620(16) Å; b, 10.6377(18) Å; c, 15.264(3) Å; β, 105.422(3)°; Å3, 1400.6(4, Z, 2; F(0 0 0) 788.0; absorption coeff, mm-1] 2.143 Independent reflections (Rint, 4938 0.0250, data/restraints/parame
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22
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- Selected bond angles: 1: N(1)-Ru(1)-N(2) 99.90(2), N(1)-Ru(1)-S(1) 87.62(16), N(1)-Ru(1)-S(2) 85.99(16), N(1)-Ru(1)-Se(1) 82.68(15), N(1)-Ru(1)-Se(2) 175.78(16) N(2)-Ru(1)-S(1) 85.83(15), N(2)-Ru(1)-S(2) 88.31(15), N(2)-Ru(1)-Se(1) 176.11(15), N(2)-Ru(1)-Se(2) 182.42(15), S(1)-Ru(1)-S(2) 170.46(7), S(1)-Ru(1)-Se(1) 91.39(5), S(1)-Ru(1)-S2(2) 95.75(6), S(2)-Ru(1)-Se(1) 94.80(5), S(2)-Ru(1)-Se(2) 90.98(5), Se(1)-Ru(1)-Se(2) 94.66(4); 2: Se(1)-Ru(1)-S(1) 91.36(4), Se(1)-Ru(1)-N(1) 80.29(12), N(1)-Ru(1)-S(1) 86.48(13).
- Selected bond angles: 1: N(1)-Ru(1)-N(2) 99.90(2), N(1)-Ru(1)-S(1) 87.62(16), N(1)-Ru(1)-S(2) 85.99(16), N(1)-Ru(1)-Se(1) 82.68(15), N(1)-Ru(1)-Se(2) 175.78(16) N(2)-Ru(1)-S(1) 85.83(15), N(2)-Ru(1)-S(2) 88.31(15), N(2)-Ru(1)-Se(1) 176.11(15), N(2)-Ru(1)-Se(2) 182.42(15), S(1)-Ru(1)-S(2) 170.46(7), S(1)-Ru(1)-Se(1) 91.39(5), S(1)-Ru(1)-S2(2) 95.75(6), S(2)-Ru(1)-Se(1) 94.80(5), S(2)-Ru(1)-Se(2) 90.98(5), Se(1)-Ru(1)-Se(2) 94.66(4); 2: Se(1)-Ru(1)-S(1) 91.36(4), Se(1)-Ru(1)-N(1) 80.29(12), N(1)-Ru(1)-S(1) 86.48(13).

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