Trace determination of sulphur mustard and related compounds in water by headspace-trap gas chromatography-mass spectrometry

Journal of Chromatography A

Volumn 1217, Issue 5, 2010, Pages 761-767

  Røen, Bent T ^a,b   Unneberg, Erik ^a   Tørnes, John Aa ^a   Lundanes, Elsa ^b  

^a NORWEGIAN DEFENCE RESEARCH ESTABLISHMENT FFI   (Norway)

^b UNIVERSITY OF OSLO   (Norway)

Author keywords

Cyclic sulphur compounds; Headspace trap; Mass spectrometry; Sulphur mustard; Water

Indexed keywords

ANALYTES; CONCENTRATION RANGES; CYCLIC COMPOUNDS; DETECTION LIMITS; FACTORIAL DESIGN; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HEADSPACE-TRAP; HEADSPACES; LIMIT OF QUANTIFICATIONS; OPTIMISATIONS; RELATED COMPOUNDS; RELATIVE STANDARD DEVIATIONS; RIVER WATER; SAMPLE HANDLING; STATIC HEADSPACE; SULPHUR COMPOUNDS; SULPHUR MUSTARD; TRACE DETERMINATION; WATER SAMPLES;

ADSORPTION; CHROMATOGRAPHIC ANALYSIS; GAS CHROMATOGRAPHY; MASS SPECTROMETERS; MASS SPECTROMETRY; SEAWATER; SULFUR; TRACE ANALYSIS;

WATER ANALYSIS;

1,3 DITHIOLANE; 1,4 DITHIANE; 1,4 THIOXANE; CHEMICAL COMPOUND; MUSTARD GAS; RIVER WATER; SEA WATER; SULFUR DERIVATIVE; UNCLASSIFIED DRUG; WATER;

ACCURACY; ARTICLE; CHEMICAL ANALYSIS; CONCENTRATION (PARAMETERS); DECOMPOSITION; FACTORIAL DESIGN; HEADSPACE TRAP GAS CHROMATOGRAPHY MASS SPECTROMETRY; MASS FRAGMENTOGRAPHY; PRIORITY JOURNAL; PROCESS OPTIMIZATION; STATISTICAL ANALYSIS; TECHNIQUE; WATER SAMPLING;

ADSORPTION; FRESH WATER; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HETEROCYCLIC COMPOUNDS; MUSTARD GAS; RAIN; REPRODUCIBILITY OF RESULTS; SEAWATER; SENSITIVITY AND SPECIFICITY; SODIUM CHLORIDE; TEMPERATURE; WATER POLLUTANTS, CHEMICAL;

EID: 73249145669     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2009.12.008     Document Type: Article

References (43)

1. Szinicz L. Toxicology 214 (2005) 167
2. MEDEA. Ocean Dumping of Chemical Munitions: Environmental Effects in Arctic Seas (1997), MEDEA, McLean, VA, USA
3. Deng H., and Evans P.O.M. Nonprolif. Rev. 4 (1997) 101
4. Convention on the prohibition of the development, production, stockpiling and use of chemical weapons and on their destruction, 13.1.1993.
5. Malhotra R.C., Ganesan K., Sugendran K., and Swamy R.V. Def. Sci. J. 49 (1999) 97
6. J.Aa. Tørnes, Ø.A. Voie, M. Ljønes, Aa.M. Opstad, L.H. Bjerkeseth, F. Hussain, Investigation and risk assessment of ships loaded with chemical ammunition scuttled in Skagerrak, FFI-rapport 2002/04951, Norwegian Defence Research Establishment, 2002.
7. Munro N.B., Talmage S.S., Griffin G.D., Waters L.C., Watson A.P., King J.F., and Hauschild V. Environ. Health Perspect. 107 (1999) 933
8. Asbury G.R., Wu C., Siems W.F., and Hill H.H. Anal. Chim. Acta 404 (2000) 273
9. Cheicante R.L., Stuff J.R., and Durst H.D. J. Chromatogr. A 711 (1995) 347
10. Hancock J.R., D'Agostino P.A., Jackson Lepage C.L., Chenier C.L., and Wyatt H.D.M. Eight International Symposium on Protection against Chemical and Biological Warfare Agents. Gothenburg (2004)
11. D'Agostino P.A., Provost L.R., Hansen A.S., and Luoma G.A. Biomed. Environ. Mass. Spectrom. 18 (1989) 484
12. Black R.M., Clarke R.J., Cooper D.B., Read R.W., and Utley D. J. Chromatogr. 637 (1993) 71
13. D'Agostino P.A., Hancock J.R., and Chenier C.L. Eur. J. Mass Spectrom. 9 (2003) 609
14. Black R.M., Clarke R.J., Read R.W., and Reid M.T.J. J. Chromatogr. A 662 (1994) 301
15. D'Agostino P.A., and Provost L.R. Biomed. Environ. Mass. Spectrom. 15 (1988) 553
16. Kuitunen M.L. In: Mesilaakso M. (Ed). Chemical Weapons Convention Chemical Analysis (2005), John Wiley & Sons, Ltd, Chichester 163
17. Kanaujia P.K., Pardasani D., Gupta A.K., and Dubey D.K. J. Chromatogr. A 1139 (2007) 185
18. D'Agostino P.A., and Provost L.R. J. Chromatogr. 645 (1993) 283
19. Ohsawa I., Kanamori-Kataoka M., Tsuge K., and Seto Y. J. Chromatogr. A 1061 (2004) 235
20. Palit M., Pardasani D., Gupta A.K., and Dubey D.K. Anal. Chem. 77 (2005) 711
21. Dubey D.K., Pardasani D., Gupta A.K., Palit M., Kanaujia P.K., and Tak V. J. Chromatogr. A 1107 (2006) 29
22. Lee H.S.N., Basheer C., and Lee H.K. J. Chromatogr. A 1124 (2006) 91
23. F. Hussain, Determination of chemical warfare agents in water samples by solid phase microextraction and GC-FID, FFI-rapport 2007/02185, Norwegian Defence Research Establishment, 2007.
24. Read R.W., and Black R.M. J. Chromatogr. A 862 (1999) 169
25. Black R.M., and Read R.W. J. Chromatogr. A 759 (1997) 79
26. D'Agostino P.A., Provost L.R., and Hancock J.R. J. Chromatogr. A 808 (1998) 177
27. Hooijschuur E.W.J., Kientz C.E., and Brinkman U.A.Th. J. Chromatogr. A 849 (1999) 433
28. Hooijschuur E.W.J., Kientz C.E., Hulst A.G., and Brinkman U.A.Th. Anal. Chem. 72 (2000) 1199
29. Wils E.R.J., Hulst A.G., de Jong A.L., Verweij A., and Boter H.L. J. Anal. Toxicol. 9 (1985) 254
30. Wils E.R.J., Hulst A.G., and van Laar J. J. Anal. Toxicol. 12 (1988) 15
31. Kimm G.L., Hook G.L., and Smith P.A. J. Chromatogr. A 971 (2002) 185
32. A. Tipler, C. Mazza, System and method for extracting headspace vapor, International publication number WO 2004/092711, 2004.
33. Barani F., Dell'Amico N., Griffone L., Santoro M., and Tarabella C. J. Chromatogr. Sci. 44 (2006) 625
34. Griffith H. Measuring Environmental Volatile Organic Compounds by U.S. EPA Method 8260B with Headspace Trap GC/MS (2004), PerkinElmer Life and Analytical Sciences, Shelton, CT
35. Grecsek H. Lc Gc N. Am. (2005) 47
36. Liu M.M., Zeng Z.R., and Fang H.F. J. Chromatogr. A 1076 (2005) 16
37. Serrano A., and Gallego A. J. Chromatogr. A 1118 (2006) 261
38. Penton Z.E. In: Pawliszyn J. (Ed). Sampling and Sample Preparation for Field and Laboratory (2002), Elsevier Science BV, Amsterdam 279
39. Stock T. In: Kaffka A.V. (Ed). Sea-Dumped Chemical Weapons: Aspects, Problems and Solutions (1996), Kluwer Academic Publishers, Dordrecht 55
40. Voice T.C. Environ. Sci. Technol. 27 (1993) 709
41. Aa.M. Opstad, J.Aa. Tørnes, Identification and quantification by GC-MS of sulphur mustard and related compounds after long time storage in sea water, FFI-rapport 2002/03237, Norwegian Defence Research Establishment, 2004.
42. Walters F.H., Parker L.R., Morgan S.L., and Deming S.L. Sequential Simplex Optimization (1991), CRC Press LLC, Boca Raton, FL p. 65
43. Steiner W.E., Clowers B.H., Matz L.M., Siems W.F., and Hill H.H. Anal. Chem. 74 (2002) 4343