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Crystal Growth and Design

Volumn 9, Issue 11, 2009, Pages 4584-4587

In situ atomic force microscopy study on the crystallization of calcium carbonate modulated by poly(vinyl alcohol)s

(5) Kim, Raehyun a Kim, Chulki b Lee, Sangsoo a Kim, Junkyung a Kim, I W b

a Korea Institute of Science and Technology (South Korea)

b Soongsil University (South Korea)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 72949084573 PISSN: 15287483 EISSN: 15287505 Source Type: Journal
DOI: 10.1021/cg900721g Document Type: Article

Times cited : (13)

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- In situ AFM experiments were performed with a MFP3D-SA (Asylum research, Santa Barbara) equipped with a fluid cell. CaCl2 (aq) and NaHCO 3 (aq) solutions were prepared by dissolving CaCl2 (Aldrich) and NaHCO3 (Oriental Chemical, Seoul, Korea) into deionized water (AquaMax Basic 361, Young Lin Instrument, Anyang, Korea, Each solution was separately supplied to a Yconnector, which was connected to the inlet of the fluid cell via a Teflon tubing, to be mixed just before streaming into the fluid cell. The concentration of each solution was 5.0 mM, and the concentration after mixing was 2.5 mM (pH 8.1-8.3) because equal amount solutions were transported to the fluid cell. Also, the flow rate for each solution was 1.5 mL/min, and the total flow after mixing became 3.0 mL/min. When a polymer additive was present in the growth solution, a small amount of a polymer stock solution (ca. 1, in DI water) was added to the NaHCO3 (aq) part to m
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