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Crystal data for [Pt(1)OOMe][SbF6, C16H 16N5O2Pt](SbF6, Mr, 741.18, triclinic, P1̄ (no. 2, a, 11.9822(7, b, 13.1681(13, c, 13.7797(14) Å, α, 76.641 (9, β, 80.491(6, γ, 72.974(7)°, V= 2011.5(3) Å3, Z, 4 [2 independent molecules, ρcalcd, 2,447 gcm-3, μ(Mo Ka, 8.369mm-13 T=173 K, orange needles, Oxford Diffraction Xcalibur 3 diffractometer; 12981 independent measured reflections, F2 refinement, R, 0.043, wR2, 0.104, 10111 independent observed absorption-corrected reflections, F0| >4σ|F 0, 2θ;2mal, 65°, 701 parameters. CCDC 699504 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via
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2mal = 65°], 701 parameters. CCDC 699504 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data-request/cif.
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