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1: of 10127 reflections collected, 4572 were independent and 2593 observed; 364 parameters, SHELXTL software (Version 5.03), R(F) = 0.0658, R(wF) = 0.1137 [I > 2σ(I)], 4 < 2θ ≤ 57. The data were collected on a Siemens P4 diffractometer equipped with a SMART/CCD detector. No absorption correction was required. The hydrogen atom on boron was located from the difference map, the thermal parameter was fixed and the coordinates were allowed to refine. All other hydrogen atoms were treated as idealized contributions. Crystallographic data (excluding structure factors) for the structure reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-101985. Copies of the data can be obtained free of charge on application to CCDC. 12 Union Road. Cambridge CB21EZ, UK (fax: (+44)1223-336-033: e-mail: deposit@ccdc.cam.ac.uk).
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