메뉴 건너뛰기




Volumn 48, Issue 28, 2009, Pages 5152-5154

Germanium(II) dications stabilized by azamacrocycles and crown ethers

Author keywords

Cations; Crown compounds; Germanium; Macrocyclic ligands; Main group elements

Indexed keywords

AZA MACROCYCLES; CATIONS; CROWN COMPOUNDS; DENTICITY; DICATIONS; MACROCYCLES; MACROCYCLIC LIGANDS; MAIN-GROUP ELEMENTS; RING SIZES;

EID: 70349929330     PISSN: 14337851     EISSN: None     Source Type: Journal    
DOI: 10.1002/anie.200901247     Document Type: Article
Times cited : (68)

References (39)
  • 1
    • 84902427927 scopus 로고    scopus 로고
    • Comprehensive Coordination Chemistry II, 3 and 10 (Eds.: J. A. McCleverty, T. J. Meyer), Elsevier, Oxford, UK, 2004.
    • Comprehensive Coordination Chemistry II, Vol. 3 and Vol. 10 (Eds.: J. A. McCleverty, T. J. Meyer), Elsevier, Oxford, UK, 2004.
  • 8
    • 84902415258 scopus 로고    scopus 로고
    • Eds, J. A. McCleverty, T. J. Meyer, Elsevier, Oxford
    • a) X Parr in Comprehensive Coordination Chemistry II, Vol. 3 (Eds.: J. A. McCleverty, T. J. Meyer), Elsevier, Oxford, 2004, pp. 545-608;
    • (2004) Comprehensive Coordination Chemistry II , vol.3 , pp. 545-608
    • Parr in, X.1
  • 14
    • 0141538391 scopus 로고    scopus 로고
    • Angew. Chem. Int. Ed. 2003, 42, 4071-4074;
    • (2003) Angew. Chem. Int. Ed , vol.42 , pp. 4071-4074
  • 24
    • 0037429902 scopus 로고    scopus 로고
    • Angew. Chem. Int Ed. 2003, 42, 1143-1145.
    • (2003) Angew. Chem. Int Ed , vol.42 , pp. 1143-1145
  • 34
    • 70349942763 scopus 로고
    • German Patent DE 4214281A1
    • M. K. Denk, W. A. Herrman, German Patent DE 4214281A1, 1993;
    • (1993)
    • Denk, M.K.1    Herrman, W.A.2
  • 36
    • 70349936694 scopus 로고    scopus 로고
    • Crystal data for [Ge(Me3-tacn)]Br[GeBr3, C 9H21Br4Ge2N3, M r, 636.11, monoclinic, space group P21/c (no. 14, a, 12.6486(10, b, 8.7022(10, c, 17.446(3) Å, β, 109.520(10)°, U= 1809.9(4) Å3, Z, 4, μ= 12.14 mm-1, T, 120K, 26441 total reflections, 4146 unique reflections, Aint, 0.059, R1 (I > 2σ(I, 0.031, R1 (all data, 0.040, wR2 (I>2σ(I, 0.061, wR2 (all data, 0.064. Crystal data for [Ge(Me4-cyclam, GeCl3]2CH2Cl 2: C15H34Cl8Ge 3N4, Mr= 771.83, triclinic, space group P1 (no. 2, a, 9.5581(15, b, 10.1021(15, c, 16.563(2) Å, α, 77.10910
    • 2 were not successful, and attempts to model split-site C atom positions in the disordered crown did not lead to a statistically significant improvement in the refinement and hence were not pursued. CCDC 722697, 722698, and 722699 contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac. uk/data-request/cif.
  • 38
    • 70349962116 scopus 로고    scopus 로고
    • G.M. Sheldrick, SHELXS-97, Program for crystal structure solution, University of Göttingen, Germany, 1997.
    • G.M. Sheldrick, SHELXS-97, Program for crystal structure solution, University of Göttingen, Germany, 1997.
  • 39
    • 70349963389 scopus 로고    scopus 로고
    • G. M. Sheldrick, SHELXL-97, Program for crystal structure refinement, University of Göttingen, Germany, 1997.
    • G. M. Sheldrick, SHELXL-97, Program for crystal structure refinement, University of Göttingen, Germany, 1997.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.