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a) W. A. Howard, T. M. Trnka, M. Waters, G. Parkin, J. Organo-met.Chem. 1997, 528, 95;
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10
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0000596575
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1) to be prone to loss of Te°, see J. M.Fischer, W. E. Piers, T. Ziegler, L. R. MacGillivray, M. J. Zaworotko, Chem.Eur. J. 1996, 2, 1221.
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1) to be prone to loss of Te°, see J. M.Fischer, W. E. Piers, T. Ziegler, L. R. MacGillivray, M. J. Zaworotko, Chem.Eur. J. 1996, 2, 1221.
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J. M. Fischer, W. E. Piers, L. R. MacGillivray, M. J. Zaworotko, hwrg.Chem. 1995, 34, 2499.
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Fischer, J.M.1
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70349900209
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a) U. J. Kilgore, C. A. Sengelaub, M. Pink, A. R. Fout, D.J. Mindiola,Angew. Chem. 2008, 120, 3829;
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Kilgore, U.J.1
Sengelaub, C.A.2
Pink, M.3
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Mindiola, D.J.5
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14
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61849137313
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b) U. J. Kilgore, C. A. Sengelaub, H. Fan, J. Tomaszewski, M. Pink, J. A.Karty, M.-H. Baik, D. J. Mindiola, Organometallics 2009, 28, 843.
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Kilgore, U.J.1
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Karty, J.A.6
Baik, M.-H.7
Mindiola, D.J.8
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15
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85036798484
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See the Supporting Information for details
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See the Supporting Information for details.
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16
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33748408758
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a) J. Beck, A. Haas, W. Herrendorf, H. Heuduk, J. Chem. Soc. DaltonTrans. 1996, 4463;
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33746740401
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b) M. Baum, J. Beck, A. Haas, W. Herrendorf, C. Mouse, J. Chem. Soc.Dalton Trans. 2000, 11;
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Baum, M.1
Beck, J.2
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0040911139
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c) B. Solouki, H. Bock, A. Haas, M. Baum, C. Monse, Z. Havlas, Z.Anorg. Allg. Chem. 1999, 625, 1726;
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d) M. Minoura, T. Kawa-shima, R. Okazaki, Tetrahedron Lett.1997, 38, 2501;
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0342710062
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e) T. G. Back, B. P. Dyck, M. Parvez, J. Org. Chem. 1995,60, 4657;
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Back, T.G.1
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21
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0024843602
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For an example of a telluroaldehyde trapped by dienes, see
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f) For an example of a telluroaldehyde trapped by dienes, see: M. Segi,T. Koyama, Y. Takata, T. Nakajima, S. Suga, J. Am. Chem. Soc.1989, 111, 8749.
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J. Am. Chem. Soc
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Segi, M.1
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Takata, Y.3
Nakajima, T.4
Suga, S.5
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22
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0001479080
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a) M. V. Lakshmikantham, M. P. Cava, M. Albeck, L. Engman, P. Carroll, J.Bergman, F. Wudl, Tetrahedron Lett. 1981, 22, 4199;
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Lakshmikantham, M.V.1
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Engman, L.4
Carroll, P.5
Bergman, J.6
Wudl, F.7
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24
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85036779996
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int, = 0.0304,GoF = 1.055, R = 0.0209 [I>2σ(I)], wR2 = 0.0522[I>2σ(I)]. CCDC 706518, 706519, 706520, 706521, 706522(2-5 and 8) contain the supplementary crystallographic data forthis paper. These data can be obtained free of charge from The CambridgeCrystallographic Data Centre via www.ccdc.cam.ac.uk/data-request/cif.
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int, = 0.0304,GoF = 1.055, R = 0.0209 [I>2σ(I)], wR2 = 0.0522[I>2σ(I)]. CCDC 706518, 706519, 706520, 706521, 706522(2-5 and 8) contain the supplementary crystallographic data forthis paper. These data can be obtained free of charge from The CambridgeCrystallographic Data Centre via www.ccdc.cam.ac.uk/data-request/cif.
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25
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85036784901
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Crystal data for 3: C10H20Te3, M= 523.06, monoclinic, P21/n, α, 12.7214(7) Å, b, 5.9309(3)Å, c, 19.0338(11) Å, β, 96.5310(10)°, V= 1426.77(13) Å′, Z, 4, ρcalcd, 2.435 Mgm3, T= 150(2) K, Mo Kα, 0.71073 Å, absorption coefficient 6.058 mm 1, F(000, 944, 24037 reflections collected, 3230 independentreflections, Rint, 0.0195, GoF, 1.074, R, 0.0147[I>2α(I)J, wR2, 0.0319 [I>2α I
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int = 0.0195, GoF = 1.074, R = 0.0147[I>2α(I)J, wR2 = 0.0319 [I>2α (I).
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26
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85036777494
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A search of the Cambridge Structural Database on 10/27/08 using Conquest1.10 suggests an average Te-Te bond length of approximately 2.7 Å formolecules containing C-Te-Te-C moieties.
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A search of the Cambridge Structural Database on 10/27/08 using Conquest1.10 suggests an average Te-Te bond length of approximately 2.7 Å formolecules containing C-Te-Te-C moieties.
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28
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85036797895
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Crystal data for 4: C2H40.NP2Te 2 Mr, 734.67, monoclinic, P21I c, α =7.2758(4) Å, b, 14.7745(10) Å, c, 27.0582(18) Å, β =95.3410(10)°, V=2896.0(3) Å3′, Z, 4, ρcalod =1.685 Mgnr3, T= 150(2) K, MoKα, 0.71073 Å,absorption coefficient 2.442 mnr1, F(000, 1440, 33700 reflectionscollected, 8801 independent reflections, Rmt, 0.0337, GoF, 1.013, R= 0.0293 {I 2σ(I, wR2, 0.0609 [I2σI
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mt = 0.0337, GoF = 1.013, R= 0.0293 {I 2σ(I)}, wR2 = 0.0609 [I2σ(I)].
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29
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34948899449
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L. C. H. Gerber, L. A. Watson, S. Parkin, W. Weng, B. M. Foxman, O. V.Ozerov, Organometallics 2007, 26, 4866.
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(2007)
Organometallics
, vol.26
, pp. 4866
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-
Gerber, L.C.H.1
Watson, L.A.2
Parkin, S.3
Weng, W.4
Foxman, B.M.5
Ozerov, O.V.6
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30
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37249043770
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U. J. Kilgore, J. Tomaszewski, H. Fan, J. C. Huffman, D. J. Mindiola,Organometallics 2007, 26, 6132.
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(2007)
Organometallics
, vol.26
, pp. 6132
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Kilgore, U.J.1
Tomaszewski, J.2
Fan, H.3
Huffman, J.C.4
Mindiola, D.J.5
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31
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85036782785
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Crystal data for 5: C46H70N3P 2V-C6H12-0.5C6 H14,M r, 905.17, monoclinic, P21/c, α, 12.6324(13) Å, 6 =36.310(4) Å, c, 11.6032(13) Å, β, 101.219(2)°,V=5220. 4(10) Å3, Z, 4, ρcalcd, 1.152 Mgnr3, T=123(2) K, MoKαl, 0.71073 Å, absorption coefficient0.289 mnr1, F(000, 1972, 63610 reflections collected, 9229independent reflections, Rint, 0.0611, GoF, 1.039, R =0.0479 [I>2σ(I, wR2, 0.0988 [I>2σI
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int = 0.0611, GoF = 1.039, R =0.0479 [I>2σ(I)], wR2 = 0.0988 [I>2σ(I)].
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32
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85036792892
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Few examples of vanadium bis(imide) complexes (transient or stableentities) have been reported;
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Few examples of vanadium bis(imide) complexes (transient or stableentities) have been reported;
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33
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85178745755
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F. Preuss, H. Becker, T. Wieland, Z. Naturforsch. B1990, 45, 191;
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a) F. Preuss, H. Becker, T. Wieland, Z. Naturforsch. B1990, 45, 191;
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34
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0000790696
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b) J. DeWith, A. D. Horton, A. G. Orpen, Organometallics 1993, 12, 1493;
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(1993)
Organometallics
, vol.12
, pp. 1493
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DeWith, J.1
Horton, A.D.2
Orpen, A.G.3
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37
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2442710014
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d) Y.-C. Tsai, P.-Y. Wang, K.-M. Lin, S.-A. Chen, J.-M. Chen, Chem.Commun. 2008, 205.
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(2008)
Chem.Commun
, pp. 205
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Tsai, Y.-C.1
Wang, P.-Y.2
Lin, K.-M.3
Chen, S.-A.4
Chen, J.-M.5
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38
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85036785946
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Crystal data for 8: C4H58N3P 2Te1 (I9V, M, 880.58, monoclinic, P21/c, α =12.439(3) Å, 6, 18.092(4) Å, c, 20.004(4) Å, β =106.380(4)°, V= 4319.2(17) Å3, Z, 4, ρcak.d, 1.354MgnT3, T= 150(2) K, MoKα, 0.71073 Å,absorption coefficient 1.056 mm1 F(000, 1810, 31624 reflectionscollected, 7713 independent reflections, Rint, 0.0800, GoF, 1.047,R, 0.0574 [I>2σ(I, wR2, 0.1453 [I >2σI, The crystals of 8 were found to contain co-crystalsof complex G44H58N3Te2V in a 9:1ratio. The Te disorder was refined with a set of restraints and constraints
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2V in a 9:1ratio. The Te disorder was refined with a set of restraints and constraints.
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