The first isolation of a telluroketone and its reversible dimerization

Tetrahedron Letters

Volumn 38, Issue 14, 1997, Pages 2501-2504

  Minoura, Mao ^a   Kawashima, Takayuki ^a   Okazaki, Renji ^a  

^a UNIVERSITY OF TOKYO   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

KETONE DERIVATIVE; TELLURIUM DERIVATIVE;

ARTICLE; DIMERIZATION; DRUG ISOLATION; DRUG SYNTHESIS; HEATING; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; REACTION ANALYSIS;

EID: 0030895849     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(97)00377-8     Document Type: Article

References (36)

1. Present address: Hiroshima University, Department of Chemistry, Faculty of Science, 1-3-1 Kagamiyama, Higashi-Hiroshima 739, Japan.
2. Barrett, A.G.M.; Barton, D.H.R.; Read, R.W. J. Chem. Soc., Chem. Commun. 1979, 645-647.
3. Grshovich, M.Z.; Elitsov, A.V. Z. Obshch. Khim. 1969, 39, 941-942; Lerstrup, K.A.; Henriksen, L. J. Chem. Soc., Chem. Commun. 1979, 1102-1103; Lappert, M.F.; Martin, T.R.; McLaughlin, G.M. J. Chem. Soc., Chem. Commun. 1980, 635-637; Barrett, A.G.M.; Read, R.W.; Barton, D.H.R. J. Chem. Soc., Perkin Trans. 1 1980, 2191-2195; Severengiz, T.; du Mont, W.W. J. Chem. Soc., Chem. Commun. 1987, 820-821; Kato, S.; Kageyama, H.; Kanda, T.; Murai, T.; Kawamura, T. Tetrahedron Lett. 1990, 31, 3587-3590; Segi, M.; Kojima, A.; Nakajima, T.; Suga, S. Synlett 1991, 2, 105-106. Kuhn, N.; Henkel, G.; Kratz, T. Chem. Ber. 1993, 126, 2047-2049; Kawahara, Y.; Kato, S.; Kanda, T.; Murai, T.; Ebihara, M. Bull. Chem. Soc. Jpn. 1995, 68, 3507-3517; Kato, S.; Kawahara, Y.; Kageyama, H., Yamada, R.; Niyomura, O.; Murai, T.; Kanda, T. J. Am. Chem. Soc. 1996, 118, 1262-1267.
4. Grshovich, M.Z.; Elitsov, A.V. Z. Obshch. Khim. 1969, 39, 941-942; Lerstrup, K.A.; Henriksen, L. J. Chem. Soc., Chem. Commun. 1979, 1102-1103; Lappert, M.F.; Martin, T.R.; McLaughlin, G.M. J. Chem. Soc., Chem. Commun. 1980, 635-637; Barrett, A.G.M.; Read, R.W.; Barton, D.H.R. J. Chem. Soc., Perkin Trans. 1 1980, 2191-2195; Severengiz, T.; du Mont, W.W. J. Chem. Soc., Chem. Commun. 1987, 820-821; Kato, S.; Kageyama, H.; Kanda, T.; Murai, T.; Kawamura, T. Tetrahedron Lett. 1990, 31, 3587-3590; Segi, M.; Kojima, A.; Nakajima, T.; Suga, S. Synlett 1991, 2, 105-106. Kuhn, N.; Henkel, G.; Kratz, T. Chem. Ber. 1993, 126, 2047-2049; Kawahara, Y.; Kato, S.; Kanda, T.; Murai, T.; Ebihara, M. Bull. Chem. Soc. Jpn. 1995, 68, 3507-3517; Kato, S.; Kawahara, Y.; Kageyama, H., Yamada, R.; Niyomura, O.; Murai, T.; Kanda, T. J. Am. Chem. Soc. 1996, 118, 1262-1267.
5. Grshovich, M.Z.; Elitsov, A.V. Z. Obshch. Khim. 1969, 39, 941-942; Lerstrup, K.A.; Henriksen, L. J. Chem. Soc., Chem. Commun. 1979, 1102-1103; Lappert, M.F.; Martin, T.R.; McLaughlin, G.M. J. Chem. Soc., Chem. Commun. 1980, 635-637; Barrett, A.G.M.; Read, R.W.; Barton, D.H.R. J. Chem. Soc., Perkin Trans. 1 1980, 2191-2195; Severengiz, T.; du Mont, W.W. J. Chem. Soc., Chem. Commun. 1987, 820-821; Kato, S.; Kageyama, H.; Kanda, T.; Murai, T.; Kawamura, T. Tetrahedron Lett. 1990, 31, 3587-3590; Segi, M.; Kojima, A.; Nakajima, T.; Suga, S. Synlett 1991, 2, 105-106. Kuhn, N.; Henkel, G.; Kratz, T. Chem. Ber. 1993, 126, 2047-2049; Kawahara, Y.; Kato, S.; Kanda, T.; Murai, T.; Ebihara, M. Bull. Chem. Soc. Jpn. 1995, 68, 3507-3517; Kato, S.; Kawahara, Y.; Kageyama, H., Yamada, R.; Niyomura, O.; Murai, T.; Kanda, T. J. Am. Chem. Soc. 1996, 118, 1262-1267.
6. Grshovich, M.Z.; Elitsov, A.V. Z. Obshch. Khim. 1969, 39, 941-942; Lerstrup, K.A.; Henriksen, L. J. Chem. Soc., Chem. Commun. 1979, 1102-1103; Lappert, M.F.; Martin, T.R.; McLaughlin, G.M. J. Chem. Soc., Chem. Commun. 1980, 635-637; Barrett, A.G.M.; Read, R.W.; Barton, D.H.R. J. Chem. Soc., Perkin Trans. 1 1980, 2191-2195; Severengiz, T.; du Mont, W.W. J. Chem. Soc., Chem. Commun. 1987, 820-821; Kato, S.; Kageyama, H.; Kanda, T.; Murai, T.; Kawamura, T. Tetrahedron Lett. 1990, 31, 3587-3590; Segi, M.; Kojima, A.; Nakajima, T.; Suga, S. Synlett 1991, 2, 105-106. Kuhn, N.; Henkel, G.; Kratz, T. Chem. Ber. 1993, 126, 2047-2049; Kawahara, Y.; Kato, S.; Kanda, T.; Murai, T.; Ebihara, M. Bull. Chem. Soc. Jpn. 1995, 68, 3507-3517; Kato, S.; Kawahara, Y.; Kageyama, H., Yamada, R.; Niyomura, O.; Murai, T.; Kanda, T. J. Am. Chem. Soc. 1996, 118, 1262-1267.
7. Grshovich, M.Z.; Elitsov, A.V. Z. Obshch. Khim. 1969, 39, 941-942; Lerstrup, K.A.; Henriksen, L. J. Chem. Soc., Chem. Commun. 1979, 1102-1103; Lappert, M.F.; Martin, T.R.; McLaughlin, G.M. J. Chem. Soc., Chem. Commun. 1980, 635-637; Barrett, A.G.M.; Read, R.W.; Barton, D.H.R. J. Chem. Soc., Perkin Trans. 1 1980, 2191-2195; Severengiz, T.; du Mont, W.W. J. Chem. Soc., Chem. Commun. 1987, 820-821; Kato, S.; Kageyama, H.; Kanda, T.; Murai, T.; Kawamura, T. Tetrahedron Lett. 1990, 31, 3587-3590; Segi, M.; Kojima, A.; Nakajima, T.; Suga, S. Synlett 1991, 2, 105-106. Kuhn, N.; Henkel, G.; Kratz, T. Chem. Ber. 1993, 126, 2047-2049; Kawahara, Y.; Kato, S.; Kanda, T.; Murai, T.; Ebihara, M. Bull. Chem. Soc. Jpn. 1995, 68, 3507-3517; Kato, S.; Kawahara, Y.; Kageyama, H., Yamada, R.; Niyomura, O.; Murai, T.; Kanda, T. J. Am. Chem. Soc. 1996, 118, 1262-1267.
8. Grshovich, M.Z.; Elitsov, A.V. Z. Obshch. Khim. 1969, 39, 941-942; Lerstrup, K.A.; Henriksen, L. J. Chem. Soc., Chem. Commun. 1979, 1102-1103; Lappert, M.F.; Martin, T.R.; McLaughlin, G.M. J. Chem. Soc., Chem. Commun. 1980, 635-637; Barrett, A.G.M.; Read, R.W.; Barton, D.H.R. J. Chem. Soc., Perkin Trans. 1 1980, 2191-2195; Severengiz, T.; du Mont, W.W. J. Chem. Soc., Chem. Commun. 1987, 820-821; Kato, S.; Kageyama, H.; Kanda, T.; Murai, T.; Kawamura, T. Tetrahedron Lett. 1990, 31, 3587-3590; Segi, M.; Kojima, A.; Nakajima, T.; Suga, S. Synlett 1991, 2, 105-106. Kuhn, N.; Henkel, G.; Kratz, T. Chem. Ber. 1993, 126, 2047-2049; Kawahara, Y.; Kato, S.; Kanda, T.; Murai, T.; Ebihara, M. Bull. Chem. Soc. Jpn. 1995, 68, 3507-3517; Kato, S.; Kawahara, Y.; Kageyama, H., Yamada, R.; Niyomura, O.; Murai, T.; Kanda, T. J. Am. Chem. Soc. 1996, 118, 1262-1267.
9. Grshovich, M.Z.; Elitsov, A.V. Z. Obshch. Khim. 1969, 39, 941-942; Lerstrup, K.A.; Henriksen, L. J. Chem. Soc., Chem. Commun. 1979, 1102-1103; Lappert, M.F.; Martin, T.R.; McLaughlin, G.M. J. Chem. Soc., Chem. Commun. 1980, 635-637; Barrett, A.G.M.; Read, R.W.; Barton, D.H.R. J. Chem. Soc., Perkin Trans. 1 1980, 2191-2195; Severengiz, T.; du Mont, W.W. J. Chem. Soc., Chem. Commun. 1987, 820-821; Kato, S.; Kageyama, H.; Kanda, T.; Murai, T.; Kawamura, T. Tetrahedron Lett. 1990, 31, 3587-3590; Segi, M.; Kojima, A.; Nakajima, T.; Suga, S. Synlett 1991, 2, 105-106. Kuhn, N.; Henkel, G.; Kratz, T. Chem. Ber. 1993, 126, 2047-2049; Kawahara, Y.; Kato, S.; Kanda, T.; Murai, T.; Ebihara, M. Bull. Chem. Soc. Jpn. 1995, 68, 3507-3517; Kato, S.; Kawahara, Y.; Kageyama, H., Yamada, R.; Niyomura, O.; Murai, T.; Kanda, T. J. Am. Chem. Soc. 1996, 118, 1262-1267.
10. Grshovich, M.Z.; Elitsov, A.V. Z. Obshch. Khim. 1969, 39, 941-942; Lerstrup, K.A.; Henriksen, L. J. Chem. Soc., Chem. Commun. 1979, 1102-1103; Lappert, M.F.; Martin, T.R.; McLaughlin, G.M. J. Chem. Soc., Chem. Commun. 1980, 635-637; Barrett, A.G.M.; Read, R.W.; Barton, D.H.R. J. Chem. Soc., Perkin Trans. 1 1980, 2191-2195; Severengiz, T.; du Mont, W.W. J. Chem. Soc., Chem. Commun. 1987, 820-821; Kato, S.; Kageyama, H.; Kanda, T.; Murai, T.; Kawamura, T. Tetrahedron Lett. 1990, 31, 3587-3590; Segi, M.; Kojima, A.; Nakajima, T.; Suga, S. Synlett 1991, 2, 105-106. Kuhn, N.; Henkel, G.; Kratz, T. Chem. Ber. 1993, 126, 2047-2049; Kawahara, Y.; Kato, S.; Kanda, T.; Murai, T.; Ebihara, M. Bull. Chem. Soc. Jpn. 1995, 68, 3507-3517; Kato, S.; Kawahara, Y.; Kageyama, H., Yamada, R.; Niyomura, O.; Murai, T.; Kanda, T. J. Am. Chem. Soc. 1996, 118, 1262-1267.
11. Grshovich, M.Z.; Elitsov, A.V. Z. Obshch. Khim. 1969, 39, 941-942; Lerstrup, K.A.; Henriksen, L. J. Chem. Soc., Chem. Commun. 1979, 1102-1103; Lappert, M.F.; Martin, T.R.; McLaughlin, G.M. J. Chem. Soc., Chem. Commun. 1980, 635-637; Barrett, A.G.M.; Read, R.W.; Barton, D.H.R. J. Chem. Soc., Perkin Trans. 1 1980, 2191-2195; Severengiz, T.; du Mont, W.W. J. Chem. Soc., Chem. Commun. 1987, 820-821; Kato, S.; Kageyama, H.; Kanda, T.; Murai, T.; Kawamura, T. Tetrahedron Lett. 1990, 31, 3587-3590; Segi, M.; Kojima, A.; Nakajima, T.; Suga, S. Synlett 1991, 2, 105-106. Kuhn, N.; Henkel, G.; Kratz, T. Chem. Ber. 1993, 126, 2047-2049; Kawahara, Y.; Kato, S.; Kanda, T.; Murai, T.; Ebihara, M. Bull. Chem. Soc. Jpn. 1995, 68, 3507-3517; Kato, S.; Kawahara, Y.; Kageyama, H., Yamada, R.; Niyomura, O.; Murai, T.; Kanda, T. J. Am. Chem. Soc. 1996, 118, 1262-1267.
12. Grshovich, M.Z.; Elitsov, A.V. Z. Obshch. Khim. 1969, 39, 941-942; Lerstrup, K.A.; Henriksen, L. J. Chem. Soc., Chem. Commun. 1979, 1102-1103; Lappert, M.F.; Martin, T.R.; McLaughlin, G.M. J. Chem. Soc., Chem. Commun. 1980, 635-637; Barrett, A.G.M.; Read, R.W.; Barton, D.H.R. J. Chem. Soc., Perkin Trans. 1 1980, 2191-2195; Severengiz, T.; du Mont, W.W. J. Chem. Soc., Chem. Commun. 1987, 820-821; Kato, S.; Kageyama, H.; Kanda, T.; Murai, T.; Kawamura, T. Tetrahedron Lett. 1990, 31, 3587-3590; Segi, M.; Kojima, A.; Nakajima, T.; Suga, S. Synlett 1991, 2, 105-106. Kuhn, N.; Henkel, G.; Kratz, T. Chem. Ber. 1993, 126, 2047-2049; Kawahara, Y.; Kato, S.; Kanda, T.; Murai, T.; Ebihara, M. Bull. Chem. Soc. Jpn. 1995, 68, 3507-3517; Kato, S.; Kawahara, Y.; Kageyama, H., Yamada, R.; Niyomura, O.; Murai, T.; Kanda, T. J. Am. Chem. Soc. 1996, 118, 1262-1267.
13. Duss, F. In Comprehensive Organic Chemistry; Barton, D.H.R.; Ollis, W.D., Eds.; Pergamon: Oxford, 1979; Vol. 3, pp 373-487; Voss, J. In Houben-Weyl Methoden der Organischen Chemie; Klamann, D. Ed.: George Thieme: New York, 1985; Bd. E11, pp 188-231.
14. Duss, F. In Comprehensive Organic Chemistry; Barton, D.H.R.; Ollis, W.D., Eds.; Pergamon: Oxford, 1979; Vol. 3, pp 373-487; Voss, J. In Houben-Weyl Methoden der Organischen Chemie; Klamann, D. Ed.: George Thieme: New York, 1985; Bd. E11, pp 188-231.
15. Magnas, P.D. In Comprehensive Organic Chemistry; Barton, D.H.R.; Ollis, W.D., Eds.; Pergamon: Oxford, 1979; Vol. 3, pp 491-538; Paulmier, C. Selenium Reagents and Intermediates in Organic Synthesis; Pergamon: Oxford, 1986; pp 58-83; Guziec, F.S., Jr. In The Chemistry of Organic Selenium and Tellurium Compounds; Patai, S. Ed.; John Wiley & Sons: New York, 1987; Vol. 2, pp 215-273; Guziec, F.S. Jr.; Guziec, L.J. In Comprehensive Organic Functional Group Transformations; Pattenden, G., Ed.; Katritzky, A.R.; Meth-Cohn, O., Rees, C.W., Eds.-in-Chief; Pergamon: Oxford, 1995; Vol. 3, pp 381-401.
16. Magnas, P.D. In Comprehensive Organic Chemistry; Barton, D.H.R.; Ollis, W.D., Eds.; Pergamon: Oxford, 1979; Vol. 3, pp 491-538; Paulmier, C. Selenium Reagents and Intermediates in Organic Synthesis; Pergamon: Oxford, 1986; pp 58-83; Guziec, F.S., Jr. In The Chemistry of Organic Selenium and Tellurium Compounds; Patai, S. Ed.; John Wiley & Sons: New York, 1987; Vol. 2, pp 215-273; Guziec, F.S. Jr.; Guziec, L.J. In Comprehensive Organic Functional Group Transformations; Pattenden, G., Ed.; Katritzky, A.R.; Meth-Cohn, O., Rees, C.W., Eds.-in-Chief; Pergamon: Oxford, 1995; Vol. 3, pp 381-401.
17. Magnas, P.D. In Comprehensive Organic Chemistry; Barton, D.H.R.; Ollis, W.D., Eds.; Pergamon: Oxford, 1979; Vol. 3, pp 491-538; Paulmier, C. Selenium Reagents and Intermediates in Organic Synthesis; Pergamon: Oxford, 1986; pp 58-83; Guziec, F.S., Jr. In The Chemistry of Organic Selenium and Tellurium Compounds; Patai, S. Ed.; John Wiley & Sons: New York, 1987; Vol. 2, pp 215-273; Guziec, F.S. Jr.; Guziec, L.J. In Comprehensive Organic Functional Group Transformations; Pattenden, G., Ed.; Katritzky, A.R.; Meth-Cohn, O., Rees, C.W., Eds.-in-Chief; Pergamon: Oxford, 1995; Vol. 3, pp 381-401.
18. Magnas, P.D. In Comprehensive Organic Chemistry; Barton, D.H.R.; Ollis, W.D., Eds.; Pergamon: Oxford, 1979; Vol. 3, pp 491-538; Paulmier, C. Selenium Reagents and Intermediates in Organic Synthesis; Pergamon: Oxford, 1986; pp 58-83; Guziec, F.S., Jr. In The Chemistry of Organic Selenium and Tellurium Compounds; Patai, S. Ed.; John Wiley & Sons: New York, 1987; Vol. 2, pp 215-273; Guziec, F.S. Jr.; Guziec, L.J. In Comprehensive Organic Functional Group Transformations; Pattenden, G., Ed.; Katritzky, A.R.; Meth-Cohn, O., Rees, C.W., Eds.-in-Chief; Pergamon: Oxford, 1995; Vol. 3, pp 381-401.
19. Segi, M.; Koyama, T.; Takata, Y.; Nakajima, T.; Suga, S. J. Am. Chem. Soc. 1989, 111, 8749-8751; Back, T.G.; Dyck, B.P.; Parvez, M. J. Org. Chem. 1995, 60, 4657-4659; also see: Erker, G.; Hock, R. Angew. Chem., Int. Ed. Engl. 1989, 28, 179-180.
20. Segi, M.; Koyama, T.; Takata, Y.; Nakajima, T.; Suga, S. J. Am. Chem. Soc. 1989, 111, 8749-8751; Back, T.G.; Dyck, B.P.; Parvez, M. J. Org. Chem. 1995, 60, 4657-4659; also see: Erker, G.; Hock, R. Angew. Chem., Int. Ed. Engl. 1989, 28, 179-180.
21. Segi, M.; Koyama, T.; Takata, Y.; Nakajima, T.; Suga, S. J. Am. Chem. Soc. 1989, 111, 8749-8751; Back, T.G.; Dyck, B.P.; Parvez, M. J. Org. Chem. 1995, 60, 4657-4659; also see: Erker, G.; Hock, R. Angew. Chem., Int. Ed. Engl. 1989, 28, 179-180.
22. Boese, R.; Haas, A.; Limberg, C. J. Chem. Soc., Chem. Commun. 1991, 1378-1379; Boese, R.; Haas, A.; Limberg, C. J. Chem. Soc., Dalton Trans. 1993, 2547-2556. Beck, J.; Haas, A.; Herrendorf, W.; Heuduk, H. J. Chem. Soc., Dalton Trans. 1996, 4463-4470. For other examples of 1,3-ditelluretanes see: Laishev, V.Z.; Petrov, M.L.; Petrov, A.A. Z. Org. Kim. 1981, 17, 2064-2071; Bender, S.L.; Haley, N.F.; Luss, H.R. Tetrahedron Lett. 1981, 22, 1495-1496; Lakshmikantham, M.V.; Cava, M.P.; Albeck, M.; Engman, L.; Carroll, P.; Bergman, J.; Wudl, F. Tetrahedraon Lett. 1981, 22, 4199-4200.
23. Boese, R.; Haas, A.; Limberg, C. J. Chem. Soc., Chem. Commun. 1991, 1378-1379; Boese, R.; Haas, A.; Limberg, C. J. Chem. Soc., Dalton Trans. 1993, 2547-2556. Beck, J.; Haas, A.; Herrendorf, W.; Heuduk, H. J. Chem. Soc., Dalton Trans. 1996, 4463-4470. For other examples of 1,3-ditelluretanes see: Laishev, V.Z.; Petrov, M.L.; Petrov, A.A. Z. Org. Kim. 1981, 17, 2064-2071; Bender, S.L.; Haley, N.F.; Luss, H.R. Tetrahedron Lett. 1981, 22, 1495-1496; Lakshmikantham, M.V.; Cava, M.P.; Albeck, M.; Engman, L.; Carroll, P.; Bergman, J.; Wudl, F. Tetrahedraon Lett. 1981, 22, 4199-4200.
24. Boese, R.; Haas, A.; Limberg, C. J. Chem. Soc., Chem. Commun. 1991, 1378-1379; Boese, R.; Haas, A.; Limberg, C. J. Chem. Soc., Dalton Trans. 1993, 2547-2556. Beck, J.; Haas, A.; Herrendorf, W.; Heuduk, H. J. Chem. Soc., Dalton Trans. 1996, 4463-4470. For other examples of 1,3-ditelluretanes see: Laishev, V.Z.; Petrov, M.L.; Petrov, A.A. Z. Org. Kim. 1981, 17, 2064-2071; Bender, S.L.; Haley, N.F.; Luss, H.R. Tetrahedron Lett. 1981, 22, 1495-1496; Lakshmikantham, M.V.; Cava, M.P.; Albeck, M.; Engman, L.; Carroll, P.; Bergman, J.; Wudl, F. Tetrahedraon Lett. 1981, 22, 4199-4200.
25. Boese, R.; Haas, A.; Limberg, C. J. Chem. Soc., Chem. Commun. 1991, 1378-1379; Boese, R.; Haas, A.; Limberg, C. J. Chem. Soc., Dalton Trans. 1993, 2547-2556. Beck, J.; Haas, A.; Herrendorf, W.; Heuduk, H. J. Chem. Soc., Dalton Trans. 1996, 4463-4470. For other examples of 1,3-ditelluretanes see: Laishev, V.Z.; Petrov, M.L.; Petrov, A.A. Z. Org. Kim. 1981, 17, 2064-2071; Bender, S.L.; Haley, N.F.; Luss, H.R. Tetrahedron Lett. 1981, 22, 1495-1496; Lakshmikantham, M.V.; Cava, M.P.; Albeck, M.; Engman, L.; Carroll, P.; Bergman, J.; Wudl, F. Tetrahedraon Lett. 1981, 22, 4199-4200.
26. Boese, R.; Haas, A.; Limberg, C. J. Chem. Soc., Chem. Commun. 1991, 1378-1379; Boese, R.; Haas, A.; Limberg, C. J. Chem. Soc., Dalton Trans. 1993, 2547-2556. Beck, J.; Haas, A.; Herrendorf, W.; Heuduk, H. J. Chem. Soc., Dalton Trans. 1996, 4463-4470. For other examples of 1,3-ditelluretanes see: Laishev, V.Z.; Petrov, M.L.; Petrov, A.A. Z. Org. Kim. 1981, 17, 2064-2071; Bender, S.L.; Haley, N.F.; Luss, H.R. Tetrahedron Lett. 1981, 22, 1495-1496; Lakshmikantham, M.V.; Cava, M.P.; Albeck, M.; Engman, L.; Carroll, P.; Bergman, J.; Wudl, F. Tetrahedraon Lett. 1981, 22, 4199-4200.
27. Boese, R.; Haas, A.; Limberg, C. J. Chem. Soc., Chem. Commun. 1991, 1378-1379; Boese, R.; Haas, A.; Limberg, C. J. Chem. Soc., Dalton Trans. 1993, 2547-2556. Beck, J.; Haas, A.; Herrendorf, W.; Heuduk, H. J. Chem. Soc., Dalton Trans. 1996, 4463-4470. For other examples of 1,3-ditelluretanes see: Laishev, V.Z.; Petrov, M.L.; Petrov, A.A. Z. Org. Kim. 1981, 17, 2064-2071; Bender, S.L.; Haley, N.F.; Luss, H.R. Tetrahedron Lett. 1981, 22, 1495-1496; Lakshmikantham, M.V.; Cava, M.P.; Albeck, M.; Engman, L.; Carroll, P.; Bergman, J.; Wudl, F. Tetrahedraon Lett. 1981, 22, 4199-4200.
28. Minoura M., Kawashima T., Okazaki R. J. Am. Chem. Soc. 115:1993;7019-7020.
29. Minoura, M.; Kawashima, T.; Tokitoh, N.; Okazaki, R. J. Chem. Soc., Chem. Commun. 1996, 123-124.
30. In these experiments, all manipulations were performed in the dark with a subdued red lump except for cases of checking the color.
31. Okazaki, R.; Minoura, M.; Kawashima, T. Chem. Lett. 1993, 1047-1048.
32. Guziec, F.S., Jr.; SanFilippo, L.J.; Murphy, C.J.; Moustakis, C.A.; Cullen, E.R. Tetrahedron 1985, 41, 4843-4852. Also see followings. Back, T.G.; Barton, D.H.R.; Britten-Kelly, M.R.; Guziec, F.S., Jr. J. Chem. Soc., Perkin Trans. 1 1976, 2079-2089; Guziec, F.S., Jr; Murphy, C.J.; Cullen, E.R. J. Chem. Soc., Perkin Trans. 1 1985, 107-113.
33. Guziec, F.S., Jr.; SanFilippo, L.J.; Murphy, C.J.; Moustakis, C.A.; Cullen, E.R. Tetrahedron 1985, 41, 4843-4852. Also see followings. Back, T.G.; Barton, D.H.R.; Britten-Kelly, M.R.; Guziec, F.S., Jr. J. Chem. Soc., Perkin Trans. 1 1976, 2079-2089; Guziec, F.S., Jr; Murphy, C.J.; Cullen, E.R. J. Chem. Soc., Perkin Trans. 1 1985, 107-113.
34. Guziec, F.S., Jr.; SanFilippo, L.J.; Murphy, C.J.; Moustakis, C.A.; Cullen, E.R. Tetrahedron 1985, 41, 4843-4852. Also see followings. Back, T.G.; Barton, D.H.R.; Britten-Kelly, M.R.; Guziec, F.S., Jr. J. Chem. Soc., Perkin Trans. 1 1976, 2079-2089; Guziec, F.S., Jr; Murphy, C.J.; Cullen, E.R. J. Chem. Soc., Perkin Trans. 1 1985, 107-113.
35. Wiersum, U.E. Recl. Trav. Chim. Pays-Bas 1982, 101, 317-332, 365-381.
36. 2: M, 600.0594.