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Volumn 28, Issue 18, 2009, Pages 5395-5404

13C NMR spectroscopic determination of ligand donor strengths using N-Heterocyclic carbene complexes of palladium(II)

Author keywords

[No Author keywords available]

Indexed keywords

[CARBONYL; CARBENES; CO-LIGANDS; DONOR STRENGTH; ELECTRONIC PARAMETERS; LIGAND DONORS; N-HETEROCYCLIC CARBENE COMPLEX; N-HETEROCYCLIC CARBENES; ONE POT; SINGLE CRYSTAL X-RAY DIFFRACTION ANALYSIS; SPECTROSCOPIC PROBES; SUBSTITUENT EFFECT;

EID: 70349316837     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om900667d     Document Type: Article
Times cited : (302)

References (39)
  • 8
    • 36849065859 scopus 로고    scopus 로고
    • Nolan, S. P., Ed.; Wiley-VCH: Weinheim
    • (b) N-Heterocyclic Carbenes in Synthesis; Nolan, S. P., Ed.; Wiley-VCH: Weinheim, 2006.
    • (2006) N-Heterocyclic Carbenes in Synthesis
  • 10
    • 0142227781 scopus 로고    scopus 로고
    • Alternative less common experimental methods for characterizing the donor strengths of NHCs include calorimetric see
    • Alternative less common experimental methods for characterizing the donor strengths of NHCs include calorimetric (see Hillier, A. C.; Sommer, W. J.; Yong, B. S.; Petersen, J. L.; Cavallo, L.; Nolan, S. P. Organometallics 2003,22,4322)
    • (2003) Organometallics , vol.22 , pp. 4322
    • Hillier, A.C.1    Sommer, W.J.2    Yong, B.S.3    Petersen, J.L.4    Cavallo, L.5    Nolan, S.P.6
  • 11
    • 28044469657 scopus 로고    scopus 로고
    • cyclic voltammetric studies see ref 9b and (a)
    • and cyclic voltammetric studies (see ref 9b and (a) Süssner, M.; Plenio, H. Chem. Commun. 2005, 5417.
    • (2005) Chem. Commun. , pp. 5417
    • Süssner, M.1    Plenio, H.2
  • 34
    • 70349312532 scopus 로고    scopus 로고
    • 13C spectrum of probably ∼1 s will give 1 Hz resolution, which in turn corresponds to better than 0.0025 ppm on a 400 MHz spectrometer under optimal conditions (proper shimming, etc.). The determination of the peak width at half height as the observed estimated standard deviation is probably more practical and realistic.
    • 13C spectrum of probably ∼1 s will give 1 Hz resolution, which in turn corresponds to better than 0.0025 ppm on a 400 MHz spectrometer under optimal conditions (proper shimming, etc.). The determination of the peak width at half height as the observed estimated standard deviation is probably more practical and realistic.
  • 36
    • 70349303319 scopus 로고    scopus 로고
    • Bruker AXS Inc.: Madison, WI
    • SMART version 5.628; Bruker AXS Inc.: Madison, WI, 2001.
    • (2001) SMART Version 5. , vol.628
  • 37
    • 70349327560 scopus 로고    scopus 로고
    • 22a; Bruker AXS Inc.: Madison, WI
    • SAINT+ version 6.22a; Bruker AXS Inc.: Madison, WI, 2001.
    • (2001) SAINT+ Version , vol.6
  • 39
    • 0004150157 scopus 로고    scopus 로고
    • Bruker AXS Inc.: Madison, WI
    • SHELXTL version 6.14; Bruker AXS Inc.: Madison, WI, 2000.
    • (2000) SHELXTL Version 6. , vol.14


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.