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Organometallics

Volumn 28, Issue 14, 2009, Pages 3970-3972

C-H and Si-N bond oxygenations of a divalent ytterbium amide of the pyrrolyl-cyclopentadienyl ligand

(3) Hao, Jingjun a Song, Haibin a Cui, Chunming a

a NANKAI UNIVERSITY (China)

Author keywords

[No Author keywords available]

Indexed keywords

CYCLOPENTADIENYL LIGANDS; DINUCLEAR; DIOXYGEN; LANTHANIDE AMIDES; PYRROLYL; SI-N BONDS;

AMIDES; COORDINATION REACTIONS; OXYGENATION; OXYGENATORS;

YTTERBIUM;

EID: 67651055375 PISSN: 02767333 EISSN: None Source Type: Journal
DOI: 10.1021/om9004127 Document Type: Article

Times cited : (17)

References (43)

1
- 0000516840
- For reviews, see: a
- For reviews, see: (a) Evans, W. J. Polyhedron 1987, 6, 803.
- (1987) Polyhedron , vol.6 , pp. 803
- Evans, W.J.¹

2
- 0033807999
- (b) Evans, W. J. Coord. Chem. Rev. 2000, 206, 263.
- (2000) Coord. Chem. Rev , vol.206 , pp. 263
- Evans, W.J.¹

3
- 0037087003
- (c) Evans, W. J. J. Organomet. Chem. 2002, 647, 2.
- (2002) J. Organomet. Chem , vol.647 , pp. 2
- Evans, W.J.¹

4
- 0036625395
- (d) Evans, W. J.; Davis, B. L. Chem. Rev. 2002, 102, 2119.
- (2002) Chem. Rev , vol.102 , pp. 2119
- Evans, W.J.¹ Davis, B.L.²

5
- 0037127083
- (e) Evans, W. J.; Allen, N. T.; Ziller, J. W. Angew. Chem., Int. Ed. 2002, 41, 359.
- (2002) Angew. Chem., Int. Ed , vol.41 , pp. 359
- Evans, W.J.¹ Allen, N.T.² Ziller, J.W.³

6
- 50249171894
- (f) Meyer, G. Angew. Chem., Int. Ed. 2008, 47, 4962.
- (2008) Angew. Chem., Int. Ed , vol.47 , pp. 4962
- Meyer, G.¹

7
- 0036625218
- (a) Arndt, S.; Okuda, J. Chem. Rev. 2002, 102, 1953.
- (2002) Chem. Rev , vol.102 , pp. 1953
- Arndt, S.¹ Okuda, J.²

8
- 0037087011
- (b) Hou, Z.; Wakatsuki, Y. J. Organomet. Chem. 2002, 647, 61.
- (2002) J. Organomet. Chem , vol.647 , pp. 61
- Hou, Z.¹ Wakatsuki, Y.²

9
- 33845377486
- (c) Evans, W. J.; Grate, J. W.; Choi, H. W.; Bloom, I.; Hunter, W. E.; Atwood, J. L. J. Am. Chem. Soc. 1985, 107, 941.
- (1985) J. Am. Chem. Soc , vol.107 , pp. 941
- Evans, W.J.¹ Grate, J.W.² Choi, H.W.³ Bloom, I.⁴ Hunter, W.E.⁵ Atwood, J.L.⁶

10
- 0000546864
- (d) Hou, Z.; Zhang, Y.; Yoshimura, T.; Wakatsuki, Y. Organometallics 1997, 16, 2963.
- (1997) Organometallics , vol.16 , pp. 2963
- Hou, Z.¹ Zhang, Y.² Yoshimura, T.³ Wakatsuki, Y.⁴

11
- 0034299147
- (e) Evans, W. J.; Johnston, M. A.; Fujimoto, C. H.; Greaves, J. Organometallics 2000, 19, 4258.
- (2000) Organometallics , vol.19 , pp. 4258
- Evans, W.J.¹ Johnston, M.A.² Fujimoto, C.H.³ Greaves, J.⁴

12
- 0000134423
- (f) Xie, Z.; Wang, S.; Yang, Q.; Mak, T. C. W. Organometallics 1999, 18, 2420.
- (1999) Organometallics , vol.18 , pp. 2420
- Xie, Z.¹ Wang, S.² Yang, Q.³ Mak, T.C.W.⁴

13
- 0034300930
- (g) Fedushkin, I. L.; Dechert, S.; Schumann, H. Organometallics 2000, 19, 4066.
- (2000) Organometallics , vol.19 , pp. 4066
- Fedushkin, I.L.¹ Dechert, S.² Schumann, H.³

14
- 1842533892
- (h) Nishiura, M.; Hou, Z.; Wakatsuki, Y. Organometallics 2004, 23, 1359.
- (2004) Organometallics , vol.23 , pp. 1359
- Nishiura, M.¹ Hou, Z.² Wakatsuki, Y.³

15
- 0000678931
- (a) Molander, G.; Schumann, H.; Rosenthal, E. C. E.; Demtschuk, J. Organometallics 1996, 15, 3817.
- (1996) Organometallics , vol.15 , pp. 3817
- Molander, G.¹ Schumann, H.² Rosenthal, E.C.E.³ Demtschuk, J.⁴

16
- 0000115018
- (b) Schumann, H.; Rosenthal, E. C. E.; Demtschuk, J. Organometallics 1998, 17, 5324.
- (1998) Organometallics , vol.17 , pp. 5324
- Schumann, H.¹ Rosenthal, E.C.E.² Demtschuk, J.³

17
- 85045781231
- (c) Schumann, H.; Erbstein, F.; Fedushkin, I. L.; Demtschuk, J. Z. Anorg. Allg. Chem. 1999, 625, 781.
- (1999) Anorg. Allg. Chem , vol.625 , pp. 781
- Schumann, H.¹ Erbstein, F.² Fedushkin, I.L.³ Demtschuk, J.Z.⁴

18
- 0038007040
- (d) Giesbrecht, G. R.; Cui, C.; Shafir, A.; Schmidt, J. A. R.; Arnold, J. Organometallics 2002, 21, 3841.
- (2002) Organometallics , vol.21 , pp. 3841
- Giesbrecht, G.R.¹ Cui, C.² Shafir, A.³ Schmidt, J.A.R.⁴ Arnold, J.⁵

19
- 0037450888
- (a) Walker, D. A.; Woodman, T. J.; Schormann, M.; Hughes, D. L.; Bochmann, M. Organometallics 2003, 22, 797.
- (2003) Organometallics , vol.22 , pp. 797
- Walker, D.A.¹ Woodman, T.J.² Schormann, M.³ Hughes, D.L.⁴ Bochmann, M.⁵

20
- 0003072364
- (b) Sassmannshausen, J.; Powell, A. K.; Anson, C. E.; Wocadlo, S.; Bochmann, M. J. Organomet. Chem. 1999, 592, 84-94.
- (1999) J. Organomet. Chem , vol.592 , pp. 84-94
- Sassmannshausen, J.¹ Powell, A.K.² Anson, C.E.³ Wocadlo, S.⁴ Bochmann, M.⁵

21
- 0035796650
- (c) Deckers, P. J. W.; Hessen, B.; Teuben, J. H. Angew. Chem., Int. Ed. 2001, 40, 2516-2519.
- (2001) Angew. Chem., Int. Ed , vol.40 , pp. 2516-2519
- Deckers, P.J.W.¹ Hessen, B.² Teuben, J.H.³

22
- 0343889802
- For leading reviews on ansa-metallocenes, see: a
- For leading reviews on ansa-metallocenes, see: (a) Alt, H. G.; Köppl, A. Chem. Rev. 2000, 100, 1205.
- (2000) Chem. Rev , vol.100 , pp. 1205
- Alt, H.G.¹ Köppl, A.²

23
- 4644336643
- (b) Hong, S.; Marks, T. J. Acc. Chem. Res. 2004, 37, 673.
- (2004) Acc. Chem. Res , vol.37 , pp. 673
- Hong, S.¹ Marks, T.J.²

24
- 67651016730
- (c) Müller, T. E.; Hutzsch, K. C.; Yus, M.; Foubelo, F.; Tada, M. Chem. Rev. 2008, 108, 3796.
- (2008) Chem. Rev , vol.108 , pp. 3796
- Müller, T.E.¹ Hutzsch, K.C.² Yus, M.³ Foubelo, F.⁴ Tada, M.⁵

25
- 0036625260
- Bochkarev, M. N. Chem. Rev. 2002, 102, 2089.
- (2002) Chem. Rev , vol.102 , pp. 2089
- Bochkarev, M.N.¹

26
- 0035804395
- For examples, see: a
- For examples, see: (a) Ganesan, M.; Gambarotta, S.; Yap, G. P. A. Angew. Chem., Int. Ed. 2001, 40, 766.
- (2001) Angew. Chem., Int. Ed , vol.40 , pp. 766
- Ganesan, M.¹ Gambarotta, S.² Yap, G.P.A.³

27
- 0041823180
- (b) Christian, D.; Yazdanbakhsh, M.; Gambarotta, S.; Yap, G. P. A. Organometallic 2003, 22, 3742.
- (2003) Organometallic , vol.22 , pp. 3742
- Christian, D.¹ Yazdanbakhsh, M.² Gambarotta, S.³ Yap, G.P.A.⁴

28
- 7744235051
- (c) Evans, W. J.; Lee, D.; Rego, D. B.; Perotti, J. M.; Kozimor, S. A.; Moore, E. K.; Ziller, J. W. J. Am. Chem. Soc. 2004, 126, 14574.
- (2004) J. Am. Chem. Soc , vol.126 , pp. 14574
- Evans, W.J.¹ Lee, D.² Rego, D.B.³ Perotti, J.M.⁴ Kozimor, S.A.⁵ Moore, E.K.⁶ Ziller, J.W.⁷

29
- 0036625332
- (d) Edelmann, F. T.; Freckmann, D. M. M.; Swchumann, H. Chem. Rev. 2002, 102, 1851.
- (2002) Chem. Rev , vol.102 , pp. 1851
- Edelmann, F.T.¹ Freckmann, D.M.M.² Swchumann, H.³

30
- 14844303470
- Wang, J.; Gardiner, M. G.; Skelton, B. W.; White, A. H. Organometallics 2005, 24, 815.
- (2005) Organometallics , vol.24 , pp. 815
- Wang, J.¹ Gardiner, M.G.² Skelton, B.W.³ White, A.H.⁴

31
- 0038002448
- Ganesan, M.; Bérabé, C. D.; Gambarotta, S.; Yap, G. P. A. Organometallics 2002, 21, 1707.
- (2002) Organometallics , vol.21 , pp. 1707
- Ganesan, M.¹ Bérabé, C.D.² Gambarotta, S.³ Yap, G.P.A.⁴

32
- 33749110499
- Boncella, J. M.; Anderson, R. A. Organometallics 1985, 4, 205.
- (1985) Organometallics , vol.4 , pp. 205
- Boncella, J.M.¹ Anderson, R.A.²

33
- 67651057327
- 1: Mp: 37-39 °C. 1H NMR (CDCl3, δ 0.29 (s, 6H, SiMe2, 1.65 (s, 6H, Cp-Me2, 1.81 (s, 6H, Cp-Me2, 3.12 (m, 1H, Cp-CH, 6.33 (s, 2H, pyrrole-H, 6.81 (s, 2H, pyrrole-H, 13C NMR (CDCl 3, δ -3.78, 11.14, 13.00, 55.18, 110.68, 123.25, 131.63, 137.09. Anal. Calcd for C15H23NSi (245.44, C, 73.40; H, 9.45; N, 5.71. Found: C, 73.18; H, 9.25; N, 5.59.2: A mixture of 1 (0.74 g, 3.00 mmol) and Yb[N(SiMe3)2]2(THF)2 (1.92 g, 3.00 mmol) in toluene (50 mL) was stirred at room temperature for 5 h and then at 60 °C for 2 d. The solution was concentrated (ca. 15 mL) and stored at 40 °C overnight to give dark green crystals of 2 (1.13 g, 65.2, Mp: 235-237 °C. 1H NMR (C6D6, δ 0.19 (s, 18H, SiMe3, 0.48 s, 6H, SiMe2, 2
- 2 (1027.26): C, 42.13; H, 5.99; N, 4.09. Found: C, 41.64; H, 6.18; N, 3.75.

34
- 67651066581
- Crystallographic data for 2: C2|H40N 2Si3Yb, M=577.85, monoclinic, space group P2(1)/n,a, 9.0936(18) Å, b, 28.185(6) Å, c= 10.081 (2) Å, α, 90.00°, β, 97.94(3)°, y, 90.00°, V= 2559.0(9) Å3, Z= 4, Dc, 1.497 g · cm-3, F(000, 1164, 20 616 reflections measured (6050 unique, Rl [I> 2σ(I, 0.0280, wR2 (all data, 0.0661. Crystallographic data for 3: C36H 6|N3O2Si4Yb2, M= 1027.26, monoclinic, space group P2(1, n, a= 12.099(2) Å, b, 26.325(5) Å2. c, 13.147(3) Å, α, 90.00°, β, 98.66 (3)°, y, 90.00°, V, 4139.7(14) Å3, Z, 4, Dc= 1.647 g-cm-3, F000, 2040, 28 176 reflections
- 20

35
- 0038002448
- Ganesan, M.; Bérabé, C. D.; Gambarotta, S.; Yap, G. P. A. Organometallics 2002, 21, 1707.
- (2002) Organometallics , vol.21 , pp. 1707
- Ganesan, M.¹ Bérabé, C.D.² Gambarotta, S.³ Yap, G.P.A.⁴

36
- 0040567837
- Tilley, T. D.; Andersen, R. A.; Zalkin, A. Inorg. Chem. 1984, 23, 2271.
- (1984) Inorg. Chem , vol.23 , pp. 2271
- Tilley, T.D.¹ Andersen, R.A.² Zalkin, A.³

37
- 47249146563
- Boyle, T. J.; Ottley, L. A. M. Chem. Rev. 2008, 108, 1896.
- (2008) Chem. Rev , vol.108 , pp. 1896
- Boyle, T.J.¹ Ottley, L.A.M.²

38
- 0001380032
- Karl, M.; Seybert, G.; Massa, W.; Harms, K.; Agarwal, S.; Maleika, R.; Stelter, W.; Greiner, A.; Heitz, W.; Neumuller, B; Dehnicke, K. Z. Anorg. Allg. Chem. 1999, 625, 1301.
- (1999) Anorg. Allg. Chem , vol.625 , pp. 1301
- Karl, M.¹ Seybert, G.² Massa, W.³ Harms, K.⁴ Agarwal, S.⁵ Maleika, R.⁶ Stelter, W.⁷ Greiner, A.⁸ Heitz, W.⁹ Neumuller, B.¹⁰ Dehnicke, K.Z.¹¹

39
- 11044233455
- Zhang,X. W.; Loppnow, G. R.; McDonald, R.; Takats, J. J. Am. Chem. Soc. 1995, 117, 7828-7829.
- (1995) J. Am. Chem. Soc , vol.117 , pp. 7828-7829
- Zhang, X.W.¹ Loppnow, G.R.² McDonald, R.³ Takats, J.⁴

40
- 0036049591
- (a) Niemeyer, M. Z. Anorg. Allg. Chem. 2002, 628, 647.
- (2002) Anorg. Allg. Chem , vol.628 , pp. 647
- Niemeyer, M.Z.¹

41
- 0036569093
- (b) Cui, D.; Tang, T.; Cheng, J.; Hu, N.; Chen, W.; Huang, B. J. Organomet. Chem. 2002, 650, 84.
- (2002) J. Organomet. Chem , vol.650 , pp. 84
- Cui, D.¹ Tang, T.² Cheng, J.³ Hu, N.⁴ Chen, W.⁵ Huang, B.⁶

42
- 84943920736
- SHELXS-90/96, Program for Structure Solution
- Sheldrick, G. M. SHELXS-90/96, Program for Structure Solution. Acta Crystallogr., Sect. A 1990, 46, 467.
- (1990) Acta Crystallogr., Sect. A , vol.46 , pp. 467
- Sheldrick, G.M.¹

43
- 0004150157
- Program for Crystal structure Refinement; University of Goettingen: Geottingen, Germany
- Sheldrick, G. M. SHELXL 97, Program for Crystal structure Refinement; University of Goettingen: Geottingen, Germany, 1997.
- (1997) SHELXL 97
- Sheldrick, G.M.¹

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