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84869344951
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LH (R=n-C6H13, 1HNMR (270 MHz, CDCl3, δ 8.71 (ddd, J=4.9, 1.6, 0.8Hz, 1H, 8.63 (s, 1H, 8.20 (ddd, J=8.1, 1.1, 0.8Hz, 1H, 7.80 (ddd, J=8.1, 7.6, 1.6Hz, 1H, 7.35 (ddd, J=7.6, 4.9, 1.1 Hz, 1H, 7.25-7.22 (m, 4H, 2.63 (t, J=7.6 Hz, 2H, 1.63 (quint, J=7.6Hz, 2H, 1.32 (brs, 6H, 0.89 (t, J=6.2 Hz, 3H, 13CNMR (68 MHz, CDCl3, δ 159.61, 154.78, 149.64, 148.43, 141.89, 136.60, 129.18, 124.93, 121.75, 121.10, 35.54, 31.70, 31.42, 29.96, 22.58, 14.07. L H (R=n-C16H33, Mp 45-46°C. 1HNMR (270MHz, CDC13, δ 8.72 (ddd, J=4.9, 1.6, 0.8Hz, 1H, 8.63 (s, 1H, 8.21 (ddd, J=8.4, 1.1, 0.8Hz, 1H, 7.81 (ddd, J=8.4, 7.6, 1.6Hz, 1H, 7.35 (ddd, J=7.6, 4.9, 1.1 Hz, 1H, 7.25-7.23 (m, 4H, 2.63 (t, J=7.6Hz, 2H, 1.59 quint, J=7.6Hz, 2H, 1
-
3) : δ 159.61, 154.79, 149.65, 148.44, 141.90, 136.60, 129.18, 124.93, 121.76, 121.10, 35.55, 31.91, 31.47, 29.68 (3C), 29.64 (2C), 29.62 (2C), 29.59, 29.51, 29.35, 29.31, 22.67, 14.11.
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23
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84869344944
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-1. 3 (after-annealing) : Anal. Found: C. 70.72; H. 8.34; N. 8.32; S. 6.70%.
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-1. 3 (after-annealing) : Anal. Found: C. 70.72; H. 8.34; N. 8.32; S. 6.70%.
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