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17
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49149099838
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2: C, 71.68; H, 7.96; N, 9.83; S, 5.63%. Found: C, 71.84; H, 8.16; N, 9.99; S, 5.34%.
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2: C, 71.68; H, 7.96; N, 9.83; S, 5.63%. Found: C, 71.84; H, 8.16; N, 9.99; S, 5.34%.
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18
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49149087912
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Selected crystallographic data of 1. At 100 K: monoclinic, C2/c, a, 13.681(3, b, 11.360(3, c, 21.345(5)Å, β, 93.5819(17)°, V, 3310.9(14)Å3. At 400 K: monoclinic, C2/c, a, 13.62(4, b, 11.644(18, c, 22.25(3) Å, β, 92.617(10)°, V, 3525(13) Å3. For details, see CCDC 684391 and 684392
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3. For details, see CCDC 684391 and 684392.
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20
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49149100861
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molT jump. An error within ±5 K was estimated.
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molT jump. An error within ±5 K was estimated.
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22
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49149099056
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14 derivative, see Supporting Information, being available electronically on the CSJ-Journal Web site, http://www.csj.jp/ jounals/chem-lett/index.html.
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14 derivative, see Supporting Information, being available electronically on the CSJ-Journal Web site, http://www.csj.jp/ jounals/chem-lett/index.html.
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