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Intensity data from a Bruker SMART-CCD diffractometer (MoKα, Crystallographic data for AC5-CF3; C28H16F 6S2, MW 530.53, monoclinic, P21/c, a=25.237 (8, b=7.472 (2, c=5.7989 (19) Å, β=94.186 (6) °, V=1090.6 (6) Å3, Z=2, Dcalcd=1.616gcm-3, T=183 K. 5324 reflections measured, 1917 unique reflections [R (int)=0.0652, R 1=0.0598 [I≥ 2.0σ (I, wR 2=0.1540 (all data, GOF=1.039 Crystallographic data reported in this manuscript have been deposited with Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-717649. Copies of the data can be obtained free of charge via or from the Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge, CB2 1EZ, UK; fax: +44 1223 3360
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2=0.1540 (all data), GOF=1.039 Crystallographic data reported in this manuscript have been deposited with Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-717649. Copies of the data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/retrieving.html (or from the Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge, CB2 1EZ, UK; fax: +44 1223 336033; or deposit@ccdc. cam.ac.uk).
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