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1
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0001034345
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For reviews on catalytic hydrothiolations, see: a
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For reviews on catalytic hydrothiolations, see: a) T. Beletskaya, C. Moberg, Chem. Rev. 1999, 99, 3435.
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Chem. Rev
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Beletskaya, T.1
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6
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29344438415
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C. Cao, L. R. Fraser, J. A. Love, J. Am. Chem. Soc. 2005, 127, 17614.
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J. Am. Chem. Soc
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Cao, C.1
Fraser, L.R.2
Love, J.A.3
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7
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85047285903
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a) A. Ogawa, J. Kawakami, M. Mihara, T. Ikeda, N. Sonoda, T. Hirao, J. Am. Chem. Soc. 1997, 119, 12380.
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Ogawa, A.1
Kawakami, J.2
Mihara, M.3
Ikeda, T.4
Sonoda, N.5
Hirao, T.6
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8
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0001449823
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b) A. Ogawa, N. Kawabe, J. Kawakami, M. Mihara, T. Hirao, N. Sonoda, Organometallics 1998, 17, 3111.
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Organometallics
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Ogawa, A.1
Kawabe, N.2
Kawakami, J.3
Mihara, M.4
Hirao, T.5
Sonoda, N.6
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9
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0037420860
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c) J. Kawakami, M. Mihara, I. Kamiya, M. Takeba, A. Ogawa, N. Sonoda, Tetrahedron 2003, 59, 3521.
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Tetrahedron
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Kawakami, J.1
Mihara, M.2
Kamiya, I.3
Takeba, M.4
Ogawa, A.5
Sonoda, N.6
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10
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0001907047
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R. Ugo, G. L. Manica, S. Cenini, A. Segre, F. Conti, J. Chem. Soc. A 1971, 522.
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J. Chem. Soc. A
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Ugo, R.1
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Segre, A.4
Conti, F.5
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53549092263
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A. Ishii, N. Nakata, R. Uchiumi, K. Murakami, Angew. Chem., Int. Ed. 2008, 47, 2661.
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Angew. Chem., Int. Ed
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Ishii, A.1
Nakata, N.2
Uchiumi, R.3
Murakami, K.4
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12
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33644505454
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T. Kitagawa, Y. Idomoto, H. Matsubara, D. Hobara, T. Kakiuchi, T. Okazaki, K. Komatsu, J. Org. Chem. 2006, 71, 1362.
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J. Org. Chem
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Kitagawa, T.1
Idomoto, Y.2
Matsubara, H.3
Hobara, D.4
Kakiuchi, T.5
Okazaki, T.6
Komatsu, K.7
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13
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34248176293
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H. Petzold, H. Gorls, W. Weigand, J. Organomet. Chem. 2007, 692, 2736.
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J. Organomet. Chem
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Petzold, H.1
Gorls, H.2
Weigand, W.3
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14
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84869358703
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3: mp 148°C, 1HNMR (C6D6, 400MHz, δ, 1.70 (br s, 24H, 2.00 (br s, 6H, 3,25-3.33 (m, 4H, 6.88-7.00 (m, 18H, 7.58-7.60 (m, 12H, 31P{1H}NMR (C 6D6, 162MHz, δ, 27.0 s, 1J Pt-P, 2827Hz, Anal. Calcd for C58H64P 2PtS2: C, 64.37; H, 5,96, Found: C, 63.68; H, 6.06
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2: C, 64.37; H, 5,96%. Found: C, 63.68; H, 6.06%.
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15
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67650349046
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Crystallographic data have been deposited with Cambridge Crystallo-graphic Data Centre as supplementary publication nos. CCDC-721303 for 3 and CCDC-721304 for 5
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Crystallographic data have been deposited with Cambridge Crystallo-graphic Data Centre as supplementary publication nos. CCDC-721303 for 3 and CCDC-721304 for 5.
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16
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34250334152
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A. Ishii, S. Kashiura, Y. Hayashi, W. Weigand, Chem. - Eur. J. 2007, 13, 4326.
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(2007)
Chem. - Eur. J
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, pp. 4326
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Ishii, A.1
Kashiura, S.2
Hayashi, Y.3
Weigand, W.4
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17
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84869347974
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5: mp 136-138°C, 1HNMR (CDC13, 400MHz, δ, 5.96 (dd, 2JP-H, 189, 18 Hz, 1JPt-H= 947 Hz, 1H, 5.28 (s, 1H, 6.91-7.04 (m, 12H, 7.13-7.35 (m, 24H, 7.60-7.64 (m, 6H, 31P{1H)NMR (CDCl3, 162MHz, δ, 23.1 (d, 2JP-P =15 Hz, 1JPt-P, 3189Hz, 32.4 (d. 2JP-P, 15Hz, 2JPt-P, 1963Hz, IR (KBr, v, cm-1, 2100. Anal. Calcd for C 56H44P2PtS·CH2C 12, C, 59.24; H, 4.11, Found: C, 59.29; H, 3.99
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12): C, 59.24; H, 4.11%. Found: C, 59.29; H, 3.99%,
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18
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1842684032
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S. M. Aucott, H. L. Milton, S. D. Robertson, A. M. Z. Slawin, G. D. Walker, J. D. Woollins, Chem. - Eur. J. 2004, 10, 1666.
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(2004)
Chem. - Eur. J
, vol.10
, pp. 1666
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Aucott, S.M.1
Milton, H.L.2
Robertson, S.D.3
Slawin, A.M.Z.4
Walker, G.D.5
Woollins, J.D.6
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19
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84869358695
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6: mp 253-254°C, 1HNMR (CDCl3, 400 MHz, δ, 5.24 (s, 1H, 5.92 (dt, J, 8.1 Hz, 1H, 6.52 (t, J, 8 Hz, 1H, 6.73 (d, J, 7 Hz, 1H, 6.88-6.98 (m, 12H, 7.12-7.40 (m, 18H, 7.62-7.69 (m, 6H, 7.89 (d. J, 8Hz, 2H, 31P{1H}NMR (CDCl3, 162 MHz, δ, 24.5 (d, 2J P-P, 21 Hz, 1JPt-P, 1852 Hz, 26.2 d, 2JP-P, 21 Hz, 1JPt-P, 3183 Hz, Anal, Calcd for C56H42P2PtS: C, 66.99; H, 4.22. Found: C, 66.68;H. 4.11
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2PtS: C, 66.99; H, 4.22. Found: C, 66.68;H. 4.11.
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22
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0000253338
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c) C. A. Dullaghan, X. Zhang, D. L. Greene, G. B. Carpenter, D. A. Sweigart, C. Camiletti, E. Rajaseelan, Organometallics 1998, 17, 3316.
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(1998)
Organometallics
, vol.17
, pp. 3316
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Dullaghan, C.A.1
Zhang, X.2
Greene, D.L.3
Carpenter, G.B.4
Sweigart, D.A.5
Camiletti, C.6
Rajaseelan, E.7
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23
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0001237667
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d) H. Li, G. B. Carpenter, D. A. Sweigart, Organometallics 2000, 19, 1823.
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(2000)
Organometallics
, vol.19
, pp. 1823
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Li, H.1
Carpenter, G.B.2
Sweigart, D.A.3
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24
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0344584847
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e) G. Picazo, A. Arevalo, S. Bernes, J. J. Garcia, Organometallics 2003, 22, 4734.
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(2003)
Organometallics
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Picazo, G.1
Arevalo, A.2
Bernes, S.3
Garcia, J.J.4
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