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Leaving 3 to dry further in an attempt to remove excess acetonitrile results in the measured carbon and, nitrogen values becoming lower than calculated. This is likely due to the labile nature of the acetonitrile ligands on palladium. Due to the hygroscopic nature of 4 (gained, weight upon leaving in air) it was not possible to obtain an accurate elemental anlysis without the presence of water molecules.
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Leaving 3 to dry further in an attempt to remove excess acetonitrile results in the measured carbon and, nitrogen values becoming lower than calculated. This is likely due to the labile nature of the acetonitrile ligands on palladium. Due to the hygroscopic nature of 4 (gained, weight upon leaving in air) it was not possible to obtain an accurate elemental anlysis without the presence of water molecules.
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