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(h) Suh, Y. G.; Jung, J.-K.; Seo, S.-Y.; Min, K.-H.; Shin, D.-Y.; Lee, Y.-S.; Kim, S.-H.; Park, H.-J. J. Org. Chem. 2002, 67, 4127.
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Park, H.-J.8
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13
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0002339617
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See also the following pioneering works on brefeldin A synthesis
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See also the following pioneering works on brefeldin A synthesis: (k) Corey, E. J.; Wollenberg, R. H. Tetrahedron Lett. 1976, 4705.
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Tetrahedron Lett.
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Wollenberg, R.H.2
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(m) Baudouy, R.; Crabbé, P.; Greene, A. E.; Le Drian, C.; Orr, A. F. Tetrahedron Lett. 1977, 2973.
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Crabbé, P.2
Greene, A.E.3
Le Drian, C.4
Orr, A.F.5
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17
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1842483218
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For recent reviews on olefin metathesis, see
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For recent reviews on olefin metathesis, see: (a) Diver, S. T.; Giessert, A. J. Chem. Rev. 2004, 104, 1317.
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Chem. Rev.
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Giessert, A.J.2
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(b) Nicolaou, K. C.; Bulger, P. G.; Sarlah, D. Angew. Chem. Int. Ed. 2005, 44, 4490.
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Bulger, P.G.2
Sarlah, D.3
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(b) Lee, J.; Jung, Y.-H.; Tae, J. Bull. Korean Chem. Soc. 2007, 28, 513.
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Lee, J.1
Jung, Y.-H.2
Tae, J.3
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(c) Jung, Y.-H.; Lee, J.; Tae, J. Chem. Asian J. 2007, 2, 656.
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Lee, J.2
Tae, J.3
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23
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54749129382
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For an asymmetric desymmetrization method, see
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For an asymmetric desymmetrization method, see: Li, Z.; Zhanh, W.; Yamamoto, H. Angew. Chem. Int. Ed. 2008, 47, 7520.
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Angew. Chem. Int. Ed.
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24
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(a) Tokunaga, M.; Larrow, J. F.; Kakiuchi, F.; Jacobsen, E. N. Science 1997, 277, 936.
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(c) Taylor, R. E.; Engelhardt, C. E.; Schmitt, M. J.; Yuan, H. J. Am. Chem. Soc. 2001, 123, 2964.
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(b) Procter, G.; Russell, A. T.; Murphy, P. J.; Tan, T. S.; Mather, A. N. Tetrahedron 1988, 44, 3953.
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Mather, A.N.5
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32
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0001856640
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For the synthesis of BFA by intramolecular cyclization reactions using allylsilanes, see: Epoxide opening
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For the synthesis of BFA by intramolecular cyclization reactions using allylsilanes, see: (a) Epoxide opening: Hatakeyama, S.; Sugawara, K.; Kawamura, M.; Takano, S. Synlett 1990, 691.
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Synlett
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Takano, S.4
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33
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67649423569
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β-Lactone opening: ref 3j
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(b) β-Lactone opening: ref 3j
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34
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34250803824
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(a) Jastrzebska, I.; Scaglione, J. B.; DeKoster, G. T.; Rath, N. P.; Covey, D. F. J. Org. Chem. 2007, 72, 4837.
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Scaglione, J.B.2
Dekoster, G.T.3
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Covey, D.F.5
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(b) Fürstner, A.; Thiel, O. R.; Ackermann, L. Org. Lett. 2001, 3, 449.
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(c) Takahata, H.; Yotsui, Y.; Momose, T. Tetrahedron 1998, 54, 13505.
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Tetrahedron
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14744297962
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(a) Rao, K. S.; Mukkanti, K.; Reddy, D. S.; Pla, M.; Iqbal, J. Tetrahedron Lett. 2005, 46, 2287.
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Tetrahedron Lett.
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Rao, K.S.1
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14744297962
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Rao, K. S.; Mukkanti, K.; Reddy, D. S.; Pal, M.; Iqbal, J. Tetrahedron Lett. 2005, 46, 2287.
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Rao, K.S.1
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Iqbal, J.5
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42
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67649454769
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note
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We were not able to isolate the minor Z-isomers. Only E-isomers were isolated after column chromatography.
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43
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note
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2O (4:1, 0.1 mL)
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