Multiresidue determination of tetracyclines, sulphonamides and chloramphenicol in bovine milk using HPLC-DAD

Food Chemistry

Volumn 117, Issue 3, 2009, Pages 545-552

  Vargas Mamani, Mónica Cecilia ^a   Reyes Reyes, Felix Guillermo ^a   Rath, Susanne ^a  

^a UNIVERSITY OF CAMPINAS   (Brazil)

Author keywords

Antimicrobials; Chloramphenicol; HPLC; Milk; Sulphonamides; Tetracyclines

Indexed keywords

ANTIBIOTIC AGENT; CHLORAMPHENICOL; CHLORTETRACYCLINE; ENROFLOXACIN; MINOCYCLINE; OXYTETRACYCLINE; SULFADIMIDINE; SULFAMETHOXAZOLE; SULFAQUINOXALINE; SULFONAMIDE; TETRACYCLINE;

ARTICLE; BRAZIL; CATTLE; DRUG DETERMINATION; DRUG STRUCTURE; FOOD ANALYSIS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MILK; NONHUMAN; SOLID PHASE EXTRACTION;

BOVINAE;

EID: 67349112852     PISSN: 03088146     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.foodchem.2009.04.032     Document Type: Article

References (27)

1. Abete M.C., Genta E., and Squadrone S. Tetracicline nel latte: Determinazione mediante HPLC/DAD. Industrie Alimentari 360 (1997) 753-755
2. Andersen W.C., Roybal J.E., Gonzales S.A., Turnipseed S.B., Pfenning A.P., and Kuck L.R. Determination of tetracycline residues in shrimp and whole milk using liquid chromatography with ultraviolet detection and residue confirmation by mass spectrometry. Analytica Chimica Acta 529 (2005) 145-150
3. ANVISA (2006). Programa de análise de resíduos de medicamentos veterinários em alimentos de origem animal - PAMVet - Relatório 2004/2005 - monitoramento de resíduos em leite exposto ao consumo. Accessed 10.07.08.
4. Bogialli S., Curini R., di Corcia A., Laganá A., Mele M., and Nazzari M. Simple confirmatory assay for analyzing residues of aminoglycoside antibiotics in bovine mild: Hot water extraction followed by liquid chromatography-tandem mass spectrometry. Journal of Chromatography A 1067 (2005) 93-100
5. Brandsteterova E., Kubalec P., Bovanová L., Simko P., Bednarikova A., and Machácková L. SPE and MSPD as pre-separation techniques for HPLC of tetracycline in meat, milk and cheese. Zeitschrift für Lebensmittel Untersuchung und Forschung A 205 (1997) 311-315
6. European Commission, Regulation 2002/657/EC, 12 August (2002). Implementing council directive 96/23/EC concerning the performance of analytical methods and the interpretation of results. Official Journal of European Communities, L 221/8-L221/36
7. Ekuttan C.E., Kang'ethe E.K., Kimani V.N., and Randolph T.F. Investigation on the prevalence of antimicrobial residues in milk obtained from urban smallholder dairy and non-dairy farming households in Dagoretti Division, Nairobi, Kenya. East African Medical Journal 84 (2007) 87-91
8. EMEA, 2007. The European agency for the evaluation of medicinal products. EMEA/MRL026/95. Committee for medicinal products. Sulfonamides. Accessed July, 2008.
9. Fletouris D.J., Psomas J.E., and Botsoglou N.A. Trace analysis of oxytetracycline and tetracycline in milk by high-performance liquid chromatography. Journal of Agricultural and Food Chemistry 38 (1990) 1913-1917
10. Furusawa N. Rapid liquid chromatographic determination of oxytetracycline in milk. Journal of Chromatography A 839 (1999) 247-251
11. Furusawa N. Simplified determining procedure for routine monitoring of sulphamethazine and sulphadimethoxine in milk. Journal of Chromatography A 898 (2000) 185-191
12. Furusawa N. Isolation of tetracyclines in milk using a solid-phase extracting column and water eluent. Talanta 59 1 (2003) 155-159
13. Helena D., Zdenka D.D., Ksenija S.G., Andrej K., and Vesna C.F. Residues of certain veterinary drugs in raw milk in Slovenia in the 2000-2002 period. International Journal of Environment and Pollution 31 (2007) 155-166
14. Houglum J.E., and Larson R.D. Assay of chlortetracycline in animal feeds by liquid chromatography with fluorescence detection. Journal of the Association Official Analytical Chemists International 80 (1997) 961-965
15. Husam A., Hani A.M., Sameer A.Z., Tareq A.A., Jamla A.O., Maha A.B., et al. Prevalence of antimicrobial residues in milk and dairy products in the state of Kuwait. Journal of Food Quality 30 (2007) 745-763
16. JECFA (1998). Joint FAO/WHO expert committee on food additives. WHO technical report series no. 888 fifty meeting of JECFA. Accessed 29.04.2009.
17. JECFA (2004). Joint FAO/WHO expert committee on food additives. WHO technical report series no. 925 sixty two meeting of JECFA, page 49. Accessed 10.07.08.
18. Koesukwiwat U., Jayanta S., and Leepipatpiboon N.J. Solid-phase extraction for multiresidue determination of sulfonamides, tetracyclines, and pyrimethamine in bovine's milk. Journal of Chromatography A 1149 (2007) 102-111
19. Long A.R., Hsieh L.C., Bello A.C., Malbrough M.S., Short C.R., and Barker S.A. Method for the isolation and liquid chromatography determination of chloramphenicol in milk. Journal of Agriculture Food Chemistry 38 (1999) 427-429
20. Moats W.A., and Harik-Kahn R. Rapid HPLC determination of tetracyclines antibiotics in milk. Journal of Agriculture Food Chemistry 43 (1995) 931-934
21. Oka H., Ito Y., and Matsumoto H. Chromatographic analysis of tetracycline antibiotics in foods. Journal of Chromatography A 882 (2000) 109-133
22. Pena A.L.S., Lino C.M., and Silveira M.I.N. Determination of tetracycline antibiotics in salmon muscle by liquid chromatography using postcolumn derivatization with fluorescence detection. Journal of the Association Official Analytical Chemists International 82 (1999) 55-60
23. Perez N., Guiterrez R., Noa M., Diaz G., Luna H., Escobar I., et al. Liquid chromatographic determination of multiple sulfonamides, nitrofurans, and chloramphenicol residues in pasteurized milk. Journal of the Association Official Analytical Chemists International 85 (2002) 20-24
24. Samanidou V., and Nisyriou S. Multi-residue methods for confirmatory determination of antibiotics in milk. Journal of Separation Science 31 (2008) 2068-2090
25. Schenk F.J., and Callery P.S. Chromatographic methods of analysis of antibiotics in milk. Journal of Chromatography A 812 (1998) 99-109
26. Van Rhijn J.A., Lasaroms J.J.P., Berendsen B.J.A., and Brinkman U.A.Th. Liquid chromatographic-tandem mass spectrometric determination of selected sulfonamides in milk. Journal of Chromatography A 960 (2002) 121-133
27. Zhao F., Zhang X., and Gan Y. Determination of tetracyclines in ovine milk by high-performance liquid chromatography with a coulometric electrode array system. Journal of Chromatography A 1055 (2004) 109-114