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The synthetic methods typically lead to very small amounts of products the first crystals of suitable size are harvested, and their uniform morphology and color, sharp melting points indicate a structurally homogenous product. The amounts obtained were not enough to allow us to perform X-ray powder diffraction analysis, but for several compounds we determined the unit cell on multiple crystals and they were consistent with the structures reported herein
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The synthetic methods typically lead to very small amounts of products (the first crystals of suitable size are harvested), and their uniform morphology and color, sharp melting points indicate a structurally homogenous product. The amounts obtained were not enough to allow us to perform X-ray powder diffraction analysis, but for several compounds we determined the unit cell on multiple crystals and they were consistent with the structures reported herein.
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