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Volumn 48, Issue 8, 2009, Pages 3505-3507

Synthesis and crystallization of infinite indium and gallium acetate 1d chain structures and concomitant ethyl acetate hydrolysis

Author keywords

[No Author keywords available]

Indexed keywords

ACETIC ACID DERIVATIVE; ACETIC ACID ETHYL ESTER; GALLIUM; INDIUM; ORGANOMETALLIC COMPOUND;

EID: 65349178272     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic9000945     Document Type: Article
Times cited : (23)

References (39)
  • 29
    • 65349168177 scopus 로고    scopus 로고
    • The nitroso compound is vital to the formation of the M13 complexes that we have reported, which is why it was present in these reactions.
    • The nitroso compound is vital to the formation of the M13 complexes that we have reported, which is why it was present in these reactions.
  • 30
    • 65349164973 scopus 로고    scopus 로고
    • HPLC-grade methanol was obtained from J. T. Baker and used without further purification (water content ?0.1%). No attempt was made to keep the methanol anhydrous. Hydrated metal nitrate salts were also used, so all of the water available for incorporation as hydroxide bridges came from these salts, water in the solvent, and other adventitious water.
    • HPLC-grade methanol was obtained from J. T. Baker and used without further purification (water content ?0.1%). No attempt was made to keep the methanol anhydrous. Hydrated metal nitrate salts were also used, so all of the water available for incorporation as hydroxide bridges came from these salts, water in the solvent, and other adventitious water.
  • 31
    • 37348999176 scopus 로고    scopus 로고
    • The iron complex most similar to 1 and 2 that we have found is a linear trimer produced by Lippard and co-workers (Reisner, E.; Telser, J.; Lippard, S. J. Inorg. Chem. 2007, 46, 10754-10770).
    • The iron complex most similar to 1 and 2 that we have found is a linear trimer produced by Lippard and co-workers (Reisner, E.; Telser, J.; Lippard, S. J. Inorg. Chem. 2007, 46, 10754-10770).
  • 33
    • 84868916458 scopus 로고    scopus 로고
    • Crystal data for 1: C4H7InO5, Mr, 249.92, colorless block, 0.34 × 0.18 × 0.09 mm, orthorhombic, space group Cmcm, T, 173 K, Mo Kα (0.717 03 Å, a, 14.570(5) Å, b, 6.831(2) Å, c, 7.269(2) Å, V, 723.5(4) Å3, Z, 4, ρcalcd, 2.294 g/cm3, μ, 3.23 mm-1, F=000, 480, 2max, 56.5°, 1962 reflections collected, 481unique [Rint, 0.011, R indices [I > 2σI, R1, 0.0167, wR2, 0.0475, GOF, 1.131
    • int = 0.011]. R indices [I > 2σ(I)]: R1 = 0.0167, wR2 = 0.0475, GOF = 1.131.
  • 34
    • 84868927650 scopus 로고    scopus 로고
    • int = 0.024]. R indices [I > 2σ(I)]: R1 = 0.0304, wR2 = 0.0782, GOF = 1.106.
    • int = 0.024]. R indices [I > 2σ(I)]: R1 = 0.0304, wR2 = 0.0782, GOF = 1.106.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.