Direct determination of the enantiomeric purity or enantiomeric composition of methylpropionates using a single capacitive microsensor

Analytical Chemistry

Volumn 81, Issue 5, 2009, Pages 1969-1975

  Kurzawski, Petra ^a   Bogdanski, Anja ^b   Schurig, Volker ^b   Wimmer, Reinhard ^c   Hierlemann, Andreas ^a  

^a ETH ZURICH   (Switzerland)

^b UNIVERSITY OF TÜBINGEN   (Germany)

^c AALBORG UNIVERSITY   (Denmark)

Author keywords

[No Author keywords available]

Indexed keywords

ANALYTE; ANTIPODAL SIGNALS; CAPACITIVE TYPES; COATING MATERIALS; DESORPTION KINETICS; DIRECT DETERMINATIONS; ENANTIOMERIC COMPOSITIONS; ENANTIOMERIC PURITIES; ENANTIOSELECTIVE; IMPURITIES IN; MATRIXES; METHYL LACTATES; MICRO SENSORS; SENSOR SIGNALS; SENSOR TECHNIQUES;

CHIRALITY; DESORPTION; ENANTIOMERS;

SENSORS;

GAMMA CYCLODEXTRIN; METHYL 2 CHLOROPROPIONATE; PROPIONIC ACID DERIVATIVE; RECEPTOR; UNCLASSIFIED DRUG;

ACCURACY; ARTICLE; CHIRAL CHROMATOGRAPHY; DESORPTION; ENANTIOMER; ENANTIOSELECTIVITY; MEASUREMENT; METHODOLOGY; PURIFICATION; QUALITATIVE ANALYSIS; QUANTITATIVE ANALYSIS; SENSOR; SIGNAL TRANSDUCTION; TECHNIQUE;

GAMMA-CYCLODEXTRINS; LACTATES; MODELS, CHEMICAL; MOLECULAR STRUCTURE; PROPIONIC ACIDS; STEREOISOMERISM;

EID: 64749111075     PISSN: 00032700     EISSN: None     Source Type: Journal    
DOI: 10.1021/ac802455c     Document Type: Article

References (55)

1. Stinson, S. C. Chem. Eng. News 2000, 78, 55ff.
2. Stinson, S. C. Chem. Eng. News 2001, 79, 79ff.
3. Stinson, S. C. Chem. Eng. News 2001, 79, 45ff.
4. de Camp, W. H. Chirality 1989, 1, 2-6.
5. Izake, E. L. J. Pharm. Sci. 2007, 96, 1659-1676.
6. Mei, X. F.; Wolf, C. J. Am. Chem. Soc. 2006, 128, 13326-13327.
7. Schurig, V. J. Chromatogr., A 2002, 965, 315-356.
8. Shahgaldian, P.; Pieles, U. Sensors 2006, 6, 593-615.
9. Ward, T. J.; Hamburg, D. M. Anal. Chem. 2004, 76, 4635-4644.
10. Diamond, D.; Nolan, K. Anal. Chem. 2001, 73, 22A-29A.
11. Szejtli, J. Chem. Rev. 1998, 98, 1743-1753.
12. Belder, D.; Ludwig, M. Electrophoresis 2003, 24, 2422-2430.
13. Schreier, P.; Bernreuther, A.; Huffer, M. Analysis of Chiral Organic Molecules; Walter de Gruyter & Co., Berlin, New York, 1995.
14. Subramanian, G., Ed. A Practical Approach to Chiral Separations by Liquid Chromatography; Verlag Chemie, VCH: Weinheim, Germany, 1994.
15. Gübitz, G.; Schmid, M. G. Mol. Biotechnol. 2006, 32, 159-179.
16. Hillberg, A. L.; Brain, K. R.; Allender, C. J. Adv. Drug Delivery Rev. 2005, 57, 1875-1889.
17. Kieser, B.; Fietzek, C.; Schmidt, R.; Belge, G.; Weimar, U.; Schurig, V.; Gauglitz, G. Anal. Chem. 2002, 74, 3005-3012.
18. Köhler, J. E. H.; Hohla, M.; Richters, M.; König, W. A. Angew. Chem. 1992, 31, 319-320.
19. König, W. A.; Krebber, R.; Mischnick, P. J. High Resolut. Chromatogr. 1989, 12, 732-738.
20. Li, W.; Li, S. J. In Oligomers Polymer Composites Molecular Imprinting, Springer, Berlin, Heidelberg, 2007; Vol. 206, pp 191-210.
21. König, W. A.; Hochmuth, D. H. J. Chromatogr. Sci. 2004, 42, 423-439.
22. Roussel, C.; Del Rio, A.; Pierrot-Sanders, J.; Piras, P.; Vanthuyne, N. J. Chromatogr., A 2004, 1037, 311-328.
23. Bodenhöfer, K.; Hierlemann, A.; Juza, N.; Schurig, V.; Göpel, W. Anal. Chem. 1997, 69, 4017-4031.
24. Szejtli, J. Pure Appl. Chem. 2004, 76, 1825-1845.
25. Ozoemena, K. I.; Stefan, R. I. Talanta 2005, 66, 501-504.
26. König, W. A. Gas Chromatographic Enantiomer Separation with Modified Cyclodextrins;Hüthig Buch-Verlag: Heidelberg, Germany, 1992.
27. Easton, C. J.; Lincoln, S. F. Chem. Soc. Rev. 1996, 25, 163 ff.
28. May, L. P.; Byfield, M. P.; Lindstrom, M.; Wunsche, L. F. Chirality 1997, 9, 225-232.
29. Bodenhöfer, K.; Hierlemann, A.; Göpel, W.; Juza, M.; Gross, B.; Schurig, V. Chim. Oggi 1998, 16, 56-58.
30. König, W. A. Chirality 1998, 10, 499-504.
31. Fietzek, C.; Hermle, T.; Rosenstiel, W.; Schurig, V. Fresenius' J. Anal. Chem. 2001, 371, 58-63.
32. Juvancz, Z.; Szejtli, J. TrAC, Trends Anal. Chem. 2002, 21, 379-388.
33. Schmitt, U.; Branch, S. K.; Holzgrabe, U. J. Sep. Sci. 2002, 25, 959-974.
34. Shahgaldian, P.; Hegner, M.; Pieles, U. J. Inclusion Phenom. Macrocyclic Chem. 2005, 53, 35-39.
35. Mahony, J. O.; Nolan, K.; Smyth, M. R.; Mizaikoff, B. Anal. Chim. Acta 2005, 534, 31-39.
36. Liu, F.; Liu, X.; Ng, S. C.; Chan, H. S. O. Sens. Actuators, B 2006, 113, 234-240.
37. Trojanowicz, M.; Wcislo, M. Anal. Lett. 2005, 38, 523-547.
38. Yin, X. L.; Ding, J. J.; Zhang, S.; Kong, J. L. Biosens. Bioelectron. 2006, 21, 2184-2187.
39. Aboul-Enein, H. Y.; Stefan, R. I. Crit. Rev. Anal. Chem. 1998, 28, 259-266.
40. Kurzawski, P.; Bogdanski, A.; Schurig, V.; Wimmer, R.; Hierlemann, A. Angew. Chem., Int. Ed. 2008, 47, 913-916.
41. Hagleitner, C.; Hierlemann, A.; Lange, D.; Kummer, A.; Kerness, N.; Brand, O.; Baltes, H. Nature 2001, 414, 293-296.
42. Kurzawski, P.; Hagleitner, C.; Hierlemann, A. Anal. Chem. 2006, 78, 6910-6920.
43. Kummer, A. M.; Hierlemann, A.; Baltes, H. Anal. Chem. 2004, 76, 2470-2477.
44. Hagleitner, C.; Hierlemann, A.; Baltes, H. In Sensors Update; Baltes, H., Fedder, G. K., Korvink, J. G., Eds.; Wiley VCH: Weinheim, Germany, 2003; Vol. 12, pp 51-120.
45. Kummer, A.; Hierlemann, A. IEEE Sens. J. 2006, 6, 3-10.
46. Hagleitner, C.; Hierlemann, A.; Brand, O.; Baltes, H. In Sensors Update; Baltes, H., Fedder, G. K., Korvink, J. G., Eds.; Wiley VCH: Weinheim, Germany, 2002; Vol. 11, pp 101-155.
47. Hagleitner, C.; Lange, D.; Hierlemann, A.; Brand, O.; Baltes, H. IEEE J. Solid-State Circuits 2002, 37, 1867-1878.
48. Kummer, A. Ph.D. Thesis, ETH Zurich, Zurich, Switzerland, 2004.
49. Steiner, F. P.; Hierlemann, A.; Cornila, C.; Noetzel, G.; Bachtold, M.; Korvink, J. G.; Göpel, W.; Baltes, H. Proceedings of the 8th International Conference on Solid State Sensors and Actuators, Stockholm, Sweden, 1995; pp 814-817.
50. Schurig, V. TrAC, Trends Anal. Chem. 2002, 21, 647-661.
51. Hagleitner, C. Ph.D. Thesis, ETH Zurich, Zurich, Switzerland, 2002.
52. Kummer, A. M.; Burg, T. P.; Hierlemann, A. Anal. Chem. 2006, 78, 279-290.
53. Bodenhöfer, K.; Hierlemann, A.; Schlunk, R.; Göpel, W. Sens. Actuators, B 1997, 45, 259-264.
54. Riddick, J. A.; Bunger, W. B.; Sakano, T. K. Organic Solvents, 4th ed.; Wiley Interscience: New York, 1986.
55. Kurganov, A. A.; Ponomareva, T. M.; Davankov, V. A. Dokl. Akad. Nauk SSSR 1987, 293, 623-626.