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Although this seems the most likely assignment, an alternative molecular structure featuring a macrocyclic dinuclear complex arising from coordination of two bidentate ligands to two palladium atoms cannot be totally ruled out; furthermore, the configuration at the double bond was not determined
-
Although this seems the most likely assignment, an alternative molecular structure featuring a macrocyclic dinuclear complex arising from coordination of two bidentate ligands to two palladium atoms cannot be totally ruled out; furthermore, the configuration at the double bond was not determined.
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The use of other phosphorus containing compounds than tertiary phosphines as isomerization catalysts has been reported in case of the partial isomerization (25% conversion) of maleic to fumaric dimethyl ester in the presence of an iron diphosphenyl complex and was explained by a similar mechanism as proposed in this work. Weber, L, Frebel, M, Boese, R. Chem. Ber. 1990, 123, 733
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The use of other phosphorus containing compounds than tertiary phosphines as isomerization catalysts has been reported in case of the partial isomerization (25% conversion) of maleic to fumaric dimethyl ester in the presence of an iron diphosphenyl complex and was explained by a similar mechanism as proposed in this work. Weber, L.; Frebel, M.; Boese, R. Chem. Ber. 1990, 123, 733.
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64549154176
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It was not established if the observation of a mixture of the isomers 10/10 owes to incomplete equilibration, or represents actually the composition of the equilibrium mixture.
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It was not established if the observation of a mixture of the isomers 10/10 owes to incomplete equilibration, or represents actually the composition of the equilibrium mixture.
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