Determination of spiramycin and neospiramycin antibiotic residues in raw milk using LC/ESI-MS/MS and solid-phase extraction

Journal of Separation Science

Volumn 32, Issue 4, 2009, Pages 681-688

  Wang, Jian ^a   Leung, Daniel ^a  

^a CANADIAN FOOD INSPECTION AGENCY   (Canada)

Author keywords

LC ESI MS MS; Measurement uncertainty; Metabolite; Neospiramycin; Raw milk

Indexed keywords

ACCURACY AND PRECISION; ANTIBIOTIC RESIDUES; ELECTROSPRAY; LC/ESI-MS/MS; MACROLIDE; MATRIX; MEASUREMENT UNCERTAINTY; MULTIPLE REACTION MONITORING; NEOSPIRAMYCIN; POSITIVE ION MODE; PROTONATED; PSEUDOMOLECULAR IONS; RAW MILK; SOLID-PHASE EXTRACTION; SPIRAMYCIN; STANDARD CALIBRATION;

ANTIBIOTICS; BIOMOLECULES; EXTRACTION; METABOLISM; METABOLITES;

UNCERTAINTY ANALYSIS;

ANTIBIOTIC AGENT; DRUG METABOLITE; MACROLIDE; NEOSPIRAMYCIN; SPIRAMYCIN; UNCLASSIFIED DRUG; ANTIINFECTIVE AGENT; DRUG DERIVATIVE;

ACCURACY; ARTICLE; CONTROLLED STUDY; DRUG DETERMINATION; DRUG MILK LEVEL; DRUG STRUCTURE; ELECTROSPRAY MASS SPECTROMETRY; LIQUID CHROMATOGRAPHY; MILK; PRIORITY JOURNAL; SOLID PHASE EXTRACTION; UNCERTAINTY; VALIDATION PROCESS; ANIMAL; CHEMICAL STRUCTURE; CHEMISTRY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ISOLATION AND PURIFICATION; METHODOLOGY; TANDEM MASS SPECTROMETRY; TEMPERATURE;

ANIMALS; ANTI-BACTERIAL AGENTS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; MILK; MOLECULAR STRUCTURE; SOLID PHASE EXTRACTION; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; SPIRAMYCIN; TANDEM MASS SPECTROMETRY; TEMPERATURE;

EID: 64149102868     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.200800599     Document Type: Article

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