Deposition mechanism and microstructure of pyrocarbon prepared by chemical vapor infiltration with kerosene as precursor

Carbon

Volumn 47, Issue 6, 2009, Pages 1429-1435

  Wu, Xiaowen ^a   Luo, Ruiying ^a   Zhang, Jincao ^a   Xiang, Qiao ^a   Ni, Yongfeng ^a  

^a BEIHANG UNIVERSITY   (China)

Author keywords

[No Author keywords available]

Indexed keywords

ACTIVATION ENERGY; BENDING STRENGTH; CARBON CARBON COMPOSITES; KEROSENE; MICROSTRUCTURE; SCANNING ELECTRON MICROSCOPY; SEEPAGE; VAPORS;

APPARENT ACTIVATION ENERGIES; DEPOSITION MECHANISMS; INFILTRATION KINETICS; INFILTRATION RATES; ISOTROPIC STRUCTURES; LARGE SIZES; MATRIXES; MEDIUM TEMPERATURES; POLARIZED LIGHT MICROSCOPIES; PYROCARBON; ROUGH LAMINAR; SMOOTH LAMINAR; TEMPERATURE RANGES;

SOIL MECHANICS;

EID: 62949124517     PISSN: 00086223     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.carbon.2009.01.035     Document Type: Article

References (24)

1. Bruneton E., Narcy B., and Oberlin A. Carbon-carbon composites prepared by a rapid densification process I: synthesis and physico-chemical data. Carbon 35 10-11 (1997) 1593-1598
2. Delhaes P., Trinquecoste M., Lines J.F., Cosculluela A., Goyheneche J.M., and Couzi M. Chemical vapor infiltration of C/C composites: fast densification processes and matrix characterizations. Carbon 43 4 (2005) 681-691
3. Rovillain D., Trinquecoste M., Bruneton E., Derre A., David P., and Delhaes P. Film boiling chemical vapor infiltration: an experimental study on carbon/carbon composite materials. Carbon 39 9 (2001) 1355-1365
4. Jiang M.X., Lackey W.J., and More K. Liquid reagent CVD of carbon. I. Processing and microstructure. Carbon 42 10 (2004) 1895-1900
5. Sun W.C., Li H.J., Han H.M., Zhang S.Y., and Li K.Z. Microstructure of the pyrocarbon matrix prepared by the CLVI process. Mat Sci Eng A 369 1-2 (2004) 245-249
6. Wang J.P., Qian J.M., Qiao G.J., and Jin Z.H. Improvement of film boiling chemical vapor infiltration process for fabrication of large size C/C composite. Mater Lett 60 9-10 (2006) 1269-1272
7. Okuno H., Trinquecoste M., Derre A., Monthioux M., and Delhaes P. Catalytic effects on carbon/carbon composites fabricated by a film boiling chemical vapor infiltration process. J Mater Res 17 8 (2002) 1904-1913
8. Farhan S., Li K.Z., and Guo L.J. A novel thermal gradient chemical vapor infiltration process for carbon-carbon composites. New Carbon Mater 22 3 (2007) 247-252
9. Benzinger W., Becker A., and Huttinger K.J. Chemistry and kinetics of chemical vapour deposition of pyrocarbon: I. Fundamentals of kinetics and chemical reaction engineering. Carbon 34 8 (1996) 957-966
10. Benzinger W., and Huttinger K.J. Chemical vapour infiltration of pyrocarbon: I. Some kinetic considerations. Carbon 34 12 (1996) 1465-1471
11. Feron O., Langlais F., Naslain R., and Thebault J. On kinetic and microstructural transitions in the CVD of pyrocarbon from propane. Carbon 37 9 (1999) 1343-1353
12. Ji A.L., Huo X.X., and Ma B.X. Study on the procedure of densifying C/C composites with CLVD process. J Sol Roc Tech 24 3 (2001) 68-70
13. Luo R.Y., Yang C.L., and Cheng J.W. Effect of preform architecture on the mechanical properties of 2D C/C composites prepared using rapid directional diffused CVI processes. Carbon 40 12 (2002) 2221-2228
14. Huttinger K.J. CVD in hot wall reactors - the interaction between homogeneous gas-phase and heterogeneous surface reactions. Adv Mater-CVD 4 4 (1998) 151-158
15. Zhang W.G., and Huttinger K.J. Densification of a 2D carbon fiber perform by isothermal, isobaric CVI: kinetics and carbon microstructure. Carbon 41 12 (2003) 2325-2337
16. Hu Z.J., and Huttinger K.J. Chemistry and kinetics of chemical vapor deposition of pyrocarbon VIII. Carbon deposition from methane at low pressures. Carbon 39 3 (2001) 433-441
17. Oberlin A. Pyrocarbons. Carbon 40 1 (2002) 7-24
18. Lieberman M.L., and Pierson H.O. Effect of gas phase conditions on resultant matrix pyrocarbons in carbon/carbon composites. Carbon 12 3 (1974) 233-241
19. Pierson H.O., and Lieberman M.L. The chemical vapor deposition of carbon on carbon fibers. Carbon 13 3 (1975) 159-166
20. Reznik B., and Huttinger K.J. On the terminology for pyrolytic carbon. Carbon 40 4 (2002) 621-624
21. Delhaes P. Chemical vapor deposition and infiltration processes of carbon materials. Carbon 40 5 (2002) 641-657
22. Hu Z.J., Zhang W.G., Huttinger K.J., Reznik B., and Gerthsen D. Influence of pressure, temperature and surface area/volume ratio on the texture of pyrolytic carbon deposited from methane. Carbon 41 4 (2003) 749-758
23. Dong G.L., and Huttinger K.J. Consideration of reaction mechanisms leading to pyrolytic carbon of different textures. Carbon 40 14 (2002) 2515-2528
24. Zhang W.G., Hu Z.J., and Huttinger K.J. Chemical vapor infiltration of carbon fiber felt: optimization of densification and carbon microstructure. Carbon 40 14 (2002) 2529-2545