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4644339701
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19
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0036402093
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Uchida, F.10
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20
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62649086229
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note
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2sdp (125 mg, 0.5 mmol), and phen (90 mg, 0.5 mmol) was refluxed for 3 h. The solution was filtered out and was stood for a few days. The crystals obtained were collected by filtration.
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21
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62649134871
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note
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-1, reflections collected 16,729, unique reflections 7217, param refined 613, R = 0.0840, wR = 0.1239, GOF = 1.302.
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23
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4644234801
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Kondo M., Irie Y., Shimizu Y., Miyazawa M., Kawaguchi H., Nakamura A., Naito T., Maeda K., and Uchida F. Inorg. Chem. 43 (2004) 6139
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Kondo, M.1
Irie, Y.2
Shimizu, Y.3
Miyazawa, M.4
Kawaguchi, H.5
Nakamura, A.6
Naito, T.7
Maeda, K.8
Uchida, F.9
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24
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62649096374
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Kondo M., Irie Y., Miyazawa M., Kawaguchi H., Yasue S., Maeda K., and Uchida F. J. Organomet. Chem. 692 (2007) 1991
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(2007)
J. Organomet. Chem.
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Kondo, M.1
Irie, Y.2
Miyazawa, M.3
Kawaguchi, H.4
Yasue, S.5
Maeda, K.6
Uchida, F.7
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25
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62649088584
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note
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The solid-state cyclic voltammogram (CV) measurements were carried out by immobilization of the sample at the working electrode surface according to the literature [26]. The glassy carbon electrode was gently rubbed over the crystalline sample (1-3 mg) for each compound in order to immobilize their compounds at the electrode surface. SCE and platinum wire were used as reference and counter electrodes, respectively as similar to the solution-state measurements. The three electrodes were immersed in an acetonitrile solution containing tetra-n-buylammonium hexafluorophosphate (100 mM) as an electrite. The acetonitrile solution was degassed with nitrogen for a few minutes prior to the measurements. After each measurement, the working electrode surface was cleaned with a razor blade.
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