Construction of three-dimensional honeycomb-like supramolecular host network with dicationic metallotecton CU[(2-C4H3N 2)2C(OH)2]22+ through cooperative hydrogen-bonding and anion-π interactions

Crystal Growth and Design

Volumn 8, Issue 11, 2008, Pages 3897-3901

  Wan, Chong Qing ^a   Li, Gui Sheng ^a   Chen, Xu Dong ^a   Mak, Thomas C W ^a  

^a CHINESE UNIVERSITY OF HONG KONG   (Hong Kong)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 61649116001     PISSN: 15287483     EISSN: 15287505     Source Type: Journal    
DOI: 10.1021/cg800476a     Document Type: Article

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55. Finely ground fresh samples were used for powder X-ray diffraction. Dehydrated samples were obtained by heating the powder at 100 °C under vacuum for 2 h. Powder patterns were recorded on a Bruker D8 Advance Powder X-ray diffractometer (Cu Kα, λ = 1.5418 Å) operating at 40 kV and 40 mA, with a graphite reflected beam monochromator and variable divergence slits.