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Crystal Growth and Design

Volumn 8, Issue 11, 2008, Pages 3924-3926

Trinuclear copper(II) endomacrocyclic complex with a new nonaazamacrocyclic ligand showing a trapped perchlorate anion

(5) Fernández Fernández, M Del Carmen a Bastida, Rufina b Macías, Alejandro b Pérez Lourido, Paulo a Valencia, Laura a

a UNIVERSITY OF VIGO (Spain)

b UNIVERSITY OF SANTIAGO DE COMPOSTELA (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 61549116501 PISSN: 15287483 EISSN: 15287505 Source Type: Journal
DOI: 10.1021/cg800758d Document Type: Article

Times cited : (3)

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- Data collection was performed at 293 K on a FR591-KappaCCD2000 Bruker Nonius diffractometer (Cu Kα, λ, 1.54184 Å, Reflections were corrected for Lorentz and polarization effects and for absorption by an empirical method.19 The structure was solved by direct methods and refined with the full-matrix least-squares technique (SHELXL-97)20 to give a final R1 value of 0.0636 for 979 parameters and 13972 unique reflections with I ≥ 2σ(I) and wR 2 of 0.1781 for all 157 426 reflections. Molecular graphics: ORTEP-3.21 X-ray crystal data for [CU3L(CH 3CN)5(H2O)2](ClO4) 6·CH3CN.H2O: C57H 81Cl6N15O27 Cu3 (M, 1811.69, orthorhombic, Pbca, a, 30.238(5, b, 12.8652(12) c, 39.247(3) Å
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* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.