A novel 1D chain compound constructed from alternating wells-dawson polyanions and mixed-valence hexacopper phosphate cations

Crystal Growth and Design

Volumn 8, Issue 8, 2008, Pages 2623-2625

  Yang, Hongxun ^a,b   Lin, Jingxiang ^a,b   Chen, Jiutong ^a,b   Zhu, Xiandong ^a,b   Gao, Shuiying ^a,b   Cao, Rong ^a,b  

^a FUJIAN INSTITUTE OF RESEARCH ON THE STRUCTURE OF MATTER   (China)

^b UNIVERSITY OF CHINESE ACADEMY OF SCIENCES   (China)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 61549112482     PISSN: 15287483     EISSN: 15287505     Source Type: Journal    
DOI: 10.1021/cg800471x     Document Type: Article

References (43)

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29. -1 region is indicative of the organic ligand 2,2′-bpy (see the Supporting Information, Figure S4).
30. 2 = 0.1401 (all data), GOF = 1.131. The data were collected on a Mercury CCD (2 × 2 bin mode) diffractometer with graphite monochromated Mo-Kα radiation (λ = 0.71073 A) at 20 °C. Empirical from equivalents were made from ψ-scan data using the program SHELXTL 97. The structure of compound 1 was solved by the direct methods (Wingx32, SIR-92), and successive Fourier difference syntheses. All the atoms were refined with anisotropic thermal parameters except the atoms of the disorder 2,2′-bpy and all hydrogen atoms. The 2,2′-bipyridine molecule coordinated with the Cu1 is disordered over a center of inversion and was refined as a rigid hexagon having 1.39 A (see the Supporting Information, Figure S1). CCDC-680366 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge at www.ccdc.cam.ac.uk/ conts/retrieving.html.
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