Determination of organic acids in urine by solid-phase microextraction and gas chromatography-ion trap tandem mass spectrometry previous 'in sample' derivatization with trimethyloxonium tetrafluoroborate

Biomedical Chromatography

Volumn 22, Issue 10, 2008, Pages 1155-1163

  Pacenti, Marco ^a,c   Dugheri, Stefano ^a   Villanelli, Fabio ^a   Bartolucci, Gianluca ^a   Calamai, Luca ^a   Boccalon, Pierpaolo ^a   Arcangeli, Giulio ^a   Vecchione, Febe ^b   Alessi, Paolo ^b   Kikic, Ireneo ^b   Cupelli, Vincenzo ^a  

^a UNIVERSITY OF FLORENCE   (Italy)

^b UNIVERSITY OF TRIESTE   (Italy)

^c CAREGGI UNIVERSITY HOSPITAL   (Italy)

Author keywords

Gas chromatography ion trap mass spectrometry; Occupational exposure; Solid phase microextraction; Trimethyloxonium tetrafluoroborate; Urinary metabolites

Indexed keywords

BODY FLUIDS; DRUG PRODUCTS; EXTRACTION; ION CHROMATOGRAPHY; IONIZATION OF GASES; IONS; MASS SPECTROMETRY; ORGANIC ACIDS;

DIRECT IMMERSION SOLID-PHASE MICROEXTRACTION; DIRECT IMMERSION-SOLID-PHASE MICROEXTRACTION; GAS CHROMATOGRAPHY-ION TRAP MASS SPECTROMETRIES; HEADSPACES; OCCUPATIONAL EXPOSURE; SOLID-PHASE MICROEXTRACTION; TANDEM-MASS SPECTROMETRY; TETRAFLUOROBORATES; TRIMETHYLOXONIA TETRAFLUOROBORATE; URINARY METABOLITES;

GAS CHROMATOGRAPHY;

2 FUROIC ACID; BORIC ACID; CARBOXYLIC ACID; HIPPURIC ACID; MANDELIC ACID; MUCONIC ACID; PHENYLGLYOXYLIC ACID; TRIMETHYLOXONIUM TETRAFLUOROBORATE; UNCLASSIFIED DRUG; TRIMETHYLOXONIUM TETRAFLUOROBORATE(1 ); TRIMETHYLOXONIUM TETRAFLUOROBORATE(1-);

ANALYTIC METHOD; ARTICLE; AUTOMATION; CONTROLLED STUDY; DERIVATIZATION; ENVIRONMENTAL EXPOSURE; GAS CHROMATOGRAPHY; IMMERSION; ION TRAP MASS SPECTROMETRY; ION TRAP TANDEM MASS SPECTROMETRY; REPRODUCIBILITY; SENSITIVITY AND SPECIFICITY; SOLID PHASE MICROEXTRACTION; TANDEM MASS SPECTROMETRY; URINALYSIS; CHEMISTRY; HUMAN; MASS FRAGMENTOGRAPHY; METHODOLOGY; URINE;

BORATES; CARBOXYLIC ACIDS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HUMANS; REPRODUCIBILITY OF RESULTS; SOLID PHASE MICROEXTRACTION; TANDEM MASS SPECTROMETRY;

EID: 58149163491     PISSN: 02693879     EISSN: 10990801     Source Type: Journal    
DOI: 10.1002/bmc.1039     Document Type: Article

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