SCOPUS 정보 검색 플랫폼

Inorganic Chemistry

Volumn 47, Issue 23, 2008, Pages 10804-10806

Facile synthesis of monoazidotitanium isopropoxides

(3) Shekar, Sukesh a Twamley, Brendan b Wehmschulte, Rudolf J a

a Florida Institute of Technology ^* (United States)

b UNIVERSITY OF IDAHO (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 57949101935 PISSN: 00201669 EISSN: None Source Type: Journal
DOI: 10.1021/ic8012415 Document Type: Article

Times cited : (10)

References (30)

1
- 14544287681
- Tanemura, S.; Miao, L.; Wunderlich, W.; Tanemura, M.; Mori, Y.; Toh, S.; Kaneko, K. Sci. Technol. Adv. Mater. 2005, 6, 11-17.
- (2005) Sci. Technol. Adv. Mater , vol.6 , pp. 11-17
- Tanemura, S.¹ Miao, L.² Wunderlich, W.³ Tanemura, M.⁴ Mori, Y.⁵ Toh, S.⁶ Kaneko, K.⁷

2
- 0342458068
- 5th ed, Kroschwitz, J. I, Ed, Wiley-Interscience: Hoboken, NJ
- In Kirk - Othmer Encyclopedia of Chemical Technology, 5th ed.; Kroschwitz, J. I., Ed.; Wiley-Interscience: Hoboken, NJ, 2004-2005.
- (2004) Kirk - Othmer Encyclopedia of Chemical Technology

3
- 0035854541
- Asahi, R.; Morikawa, T.; Ohwaki, T.; Aoki, K.; Taga, Y. Science 2001, 293, 269-271.
- (2001) Science , vol.293 , pp. 269-271
- Asahi, R.¹ Morikawa, T.² Ohwaki, T.³ Aoki, K.⁴ Taga, Y.⁵

4
- 2542499528
- Diwald, O.; Thompson, T. L.; Zubkov, T.; Goralski, E. G.; Walck, S. D.; Yates, J. T., Jr. J. Phys. Chem. B 2004, 108, 6004-6008.
- (2004) J. Phys. Chem. B , vol.108 , pp. 6004-6008
- Diwald, O.¹ Thompson, T.L.² Zubkov, T.³ Goralski, E.G.⁴ Walck, S.D.⁵ Yates Jr., J.T.⁶

5
- 19544388234
- 085116/1-085116/4
- Di Valentin, C.; Pacchioni, G.; Selloni, A. Phys. Rev. B 2004, 70, 085116/1-085116/4.
- (2004) Phys. Rev. B , vol.70
- Di Valentin, C.¹ Pacchioni, G.² Selloni, A.³

6
- 0442326618
- Gole, J. L.; Stout, J. D.; Burda, C.; Lou, Y.; Chen, X. J. Phys. Chem. B 2004, 108, 1230-1240.
- (2004) J. Phys. Chem. B , vol.108 , pp. 1230-1240
- Gole, J.L.¹ Stout, J.D.² Burda, C.³ Lou, Y.⁴ Chen, X.⁵

7
- 33751239787
- Thompson, T. L.; Yates, J. T., Jr. Chem. Rev. 2006, 106, 4428-4453.
- (2006) Chem. Rev , vol.106 , pp. 4428-4453
- Thompson, T.L.¹ Yates Jr., J.T.²

8
- 34748835348
- Di Valentin, C.; Finazzi, E.; Pacchioni, G.; Selloni, A.; Livraghi, S.; Paganini, M. C.; Giamello, E. Chem. Phys. 2007, 339, 44-56.
- (2007) Chem. Phys , vol.339 , pp. 44-56
- Di Valentin, C.¹ Finazzi, E.² Pacchioni, G.³ Selloni, A.⁴ Livraghi, S.⁵ Paganini, M.C.⁶ Giamello, E.⁷

9
- 42149147896
- Chen, X.; Burda, C. J. Am. Chem. Soc. 2008, 130, 5018-5019.
- (2008) J. Am. Chem. Soc , vol.130 , pp. 5018-5019
- Chen, X.¹ Burda, C.²

10
- 0037962151
- Liu, S.; Fooken, U.; Burba, C. M.; Eastman, M. A.; Wehmschulte, R. J. Chem. Mater. 2003, 15, 2803-2808.
- (2003) Chem. Mater , vol.15 , pp. 2803-2808
- Liu, S.¹ Fooken, U.² Burba, C.M.³ Eastman, M.A.⁴ Wehmschulte, R.J.⁵

11
- 33750419751
- Tewari, B. B.; Shekar, S.; Huang, L.; Gorrell, C. E.; Murphy, T. P.; Warren, K.; Nesnas, N.; Wehmschulte, R. J. Inorg. Chem. 2006, 45, 8807-8811.
- (2006) Inorg. Chem , vol.45 , pp. 8807-8811
- Tewari, B.B.¹ Shekar, S.² Huang, L.³ Gorrell, C.E.⁴ Murphy, T.P.⁵ Warren, K.⁶ Nesnas, N.⁷ Wehmschulte, R.J.⁸

12
- 0001504825
- Fischer, R. A.; Miehhr, A.; Herdtweck, E.; Mattner, M. R.; Ambacher, O.; Metzger, T.; Born, E.; Weinkauf, S.; Pulham, C. R.; Parsons, S. Chem. - Eur. J. 1996, 2, 1353-1358.
- (1996) Chem. - Eur. J , vol.2 , pp. 1353-1358
- Fischer, R.A.¹ Miehhr, A.² Herdtweck, E.³ Mattner, M.R.⁴ Ambacher, O.⁵ Metzger, T.⁶ Born, E.⁷ Weinkauf, S.⁸ Pulham, C.R.⁹ Parsons, S.¹⁰

13
- 0000497157
- Carmalt, C. J.; Cowley, A. H.; Culp, R. D.; Jones, R. A.; Sun, Y. M.; Fitts, B.; Whaley, S.; Roesky, H. W. Inorg. Chem. 1997, 36, 3108-3112.
- (1997) Inorg. Chem , vol.36 , pp. 3108-3112
- Carmalt, C.J.¹ Cowley, A.H.² Culp, R.D.³ Jones, R.A.⁴ Sun, Y.M.⁵ Fitts, B.⁶ Whaley, S.⁷ Roesky, H.W.⁸

14
- 0034500326
- Gillan, E. G. Chem. Mater. 2000, 12, 3906-3912.
- (2000) Chem. Mater , vol.12 , pp. 3906-3912
- Gillan, E.G.¹

15
- 0001147742
- Gillan, E. G.; Kaner, R. B. Inorg. Chem. 1994, 33, 5693-5700.
- (1994) Inorg. Chem , vol.33 , pp. 5693-5700
- Gillan, E.G.¹ Kaner, R.B.²

16
- 0000383046
- Hector, A. L.; Parkin, I. P. Polyhedron 1995, 14, 913-917.
- (1995) Polyhedron , vol.14 , pp. 913-917
- Hector, A.L.¹ Parkin, I.P.²

17
- 37049109369
- Choukroun, R.; Gervais, D. J. Chem. Soc., Dalton Trans. 1980, 1800-1802.
- (1980) J. Chem. Soc., Dalton Trans , pp. 1800-1802
- Choukroun, R.¹ Gervais, D.²

18
- 57949113331
- A mixture of 1 (6.8 g, 27 mmol) and Ti(OiPr)4 (8.3 mL, 28 mmol) was heated at 140°C for 1.5 h. The resulting yellow liquid solidified upon cooling to room temperature and was extracted twice with hexanes (70 mL each, Cooling at -20°C for 2 days afforded colorless crystals of 2. Yield: 11.4 g, 79, Mp: 74-76°C. 1H NMR (400.13 MHz, C6D6, δ 5.09 (s, broad, w 1/2 ≈ 73 Hz, OCH(CH3)2, 1H, 4.69 (s, broad, w1/2 ≈ 32 Hz, OCH(CH3) 2, 3H, 1.38 (d, broad, w1/2 ≈ 30 Hz, W, 6.0 Hz, OCH(CH3)2,6H, 1.30 (d, broad, w1/2 ≈ 13 Hz, J, 4.2 Hz, OCH(CH 3)2, 18H, 13C{1H} NMR (100.61, MHz, C6D6, δ 75.96 (broad, w1/2 ≈ 93 Hz, OCHCH
- 3Ti: C, 40.46; H, 7.92. Found: C, 40.04; H, 7.24.

19
- 57949097573
- Crystal data for 2: triclinic, space group P1, a, 10.4433(9) Å, b, 11.9712(10) Å, c, 13.2598(11) Å, α, 66.767(1)°, β, 72.717(2)°, γ, 69.662(1)°, V, 1403.5(2) Å3, Z, 1, μ(Mo Kα, 0.608 mm-1, Dc, 1.264 Mg/m 3, F000, 568, GOF on F2, 1.046, R1, 0.0586, wR2, 0.1194, F2, all data, data/restraints/ parameters 5078/7/293
- 2, all data), data/restraints/ parameters 5078/7/293.

20
- 84982077851
- Wellern, H. O.; Mueller, U. Chem. Ber. 1976, 109, 3039-3046.
- (1976) Chem. Ber , vol.109 , pp. 3039-3046
- Wellern, H.O.¹ Mueller, U.²

21
- 25544450640
- Kirschbaum, K.; Giolando, D. M. Acta Crystallogr., Sect. C 1992, C48, 1837-1839.
- (1992) Acta Crystallogr., Sect. C , vol.C48 , pp. 1837-1839
- Kirschbaum, K.¹ Giolando, D.M.²

22
- 57949112998
- Fric, H.; Puchberger, M.; Schubert, U. Eur. J. Inorg. Chem. 2007, 37, 6-383.
- (2007) Eur. J. Inorg. Chem , vol.37 , pp. 6-383
- Fric, H.¹ Puchberger, M.² Schubert, U.³

23
- 0000235715
- Wu, Y.-T.; Ho, Y.-C.; Lin, C.-C.; Gau, H.-M. Inorg. Chem. 1996, 35, 5948-5952.
- (1996) Inorg. Chem , vol.35 , pp. 5948-5952
- Wu, Y.-T.¹ Ho, Y.-C.² Lin, C.-C.³ Gau, H.-M.⁴

24
- 13244291567
- Fric, H.; Schubert, U. New J. Chem. 2005, 29, 232-236.
- (2005) New J. Chem , vol.29 , pp. 232-236
- Fric, H.¹ Schubert, U.²

25
- 57949085152
- 2, all data), data/restraints/parameters 9157/1/537.
- 2, all data), data/restraints/parameters 9157/1/537.

26
- 0000674993
- Boyle, T. J.; Alam, T. M.; Tafoya, C. J.; Scott, B. L. Inorg. Chem. 1998, 37, 5588-5594.
- (1998) Inorg. Chem , vol.37 , pp. 5588-5594
- Boyle, T.J.¹ Alam, T.M.² Tafoya, C.J.³ Scott, B.L.⁴

27
- 0142062476
- Ghosh, R.; Nethaji, M.; Samuelson Ashoka, G. Chem. Commun. 2003, 2556-2557.
- (2003) Chem. Commun , pp. 2556-2557
- Ghosh, R.¹ Nethaji, M.² Samuelson Ashoka, G.³

28
- 0037416316
- Nolte, J.-O.; Schneider, M.; Neumann, B.; Stammler, H.-G.; Jutzi, P. Organometallics 2003, 22, 1010-1017.
- (2003) Organometallics , vol.22 , pp. 1010-1017
- Nolte, J.-O.¹ Schneider, M.² Neumann, B.³ Stammler, H.-G.⁴ Jutzi, P.⁵

29
- 0039435705
- Zank, G. A.; Jones, C. A.; Rauchfuss, T. B.; Rheingold, A. L. Inorg. Chem. 1986, 25, 1886-1891.
- (1986) Inorg. Chem , vol.25 , pp. 1886-1891
- Zank, G.A.¹ Jones, C.A.² Rauchfuss, T.B.³ Rheingold, A.L.⁴

30
- 57949084601
- Water (38 mg, 2.1 mmol, 38 μL) was added in two portions via syringe to a solution of 2 (2.30 g, 2.1 mmol) in hexanes (60 mL) with cooling in an ice bath. The water droplets appeared to solidify upon contact with the cooled solution. A small amount of a fine colorless precipitate formed after ca. 15 min. The reaction mixture was slowly warmed to room temperature and stirred overnight. Filtration, concentration of the pale-yellow filtrate to ca. 5 mL, and redissolution of the precipitate by brief gentle heating afforded large (>3 mm) yellow crystals of 3 after 1 h (0.49 g) at room temperature. A second crop was obtained after cooling of the concentrated mother liquor at -20°C for 2 days. Yield: 0.94 g, 54, Mp: 105-107°C. 1H NMR (400.13 MHz, C6D6, δ 5.19 (sept, J, 6.0 Hz, OCH(CH3)2, 5H, 5.10 (s, broad, w 1/2 ≈ 67 Hz, OCH(CH3)2, 2H
- 4: C, 37.28; H, 7.30; N, 17.39. Found: C, 34.44; H, 6.74; N, 15.50.

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.