Nuclear magnetic resonance and liquid chromatography-mass spectrometry combined with an incompleted separation strategy for identifying the natural products in crude extract

Analytica Chimica Acta

Volumn 632, Issue 2, 2009, Pages 221-228

  Dai, Dongmei ^a   He, Jiuming ^a   Sun, Ruixiang ^b   Zhang, Ruiping ^a   Aisa, Haji Akber ^c   Abliz, Zeper ^a  

^a BEIJING UNIVERSITY OF POSTS AND TELECOMMUNICATIONS   (China)

^b INSTITUTE OF COMPUTING TECHNOLOGY   (China)

^c XINJIANG TECHNICAL INSTITUTE OF PHYSICS AND CHEMISTRY   (China)

Author keywords

Crude extract; Incompleted separation strategy; Natural products; Nuclear magnetic resonance liquid chromatography mass spectrometry parallel dynamic spectroscopy; Off line analytical method

Indexed keywords

CHROMATOGRAPHIC ANALYSIS; CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ISOMERS; LIQUID CHROMATOGRAPHY; MAGNETIC RESONANCE; MASS SPECTROMETERS; MASS SPECTROMETRY; NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PRECIPITATION (CHEMICAL); SEPARATION; SOLVENT EXTRACTION; SPECTROMETERS; SPECTROMETRY; SPECTRUM ANALYSIS; STRUCTURE (COMPOSITION); SUGARS;

CRUDE EXTRACT; INCOMPLETED SEPARATION STRATEGY; NATURAL PRODUCTS; NUCLEAR MAGNETIC RESONANCE/LIQUID CHROMATOGRAPHY-MASS SPECTROMETRY PARALLEL DYNAMIC SPECTROSCOPY; OFF-LINE ANALYTICAL METHOD;

COLUMN CHROMATOGRAPHY;

4' METHOXYLQUERCETIN 3' GLUCOSIDE; 8 METHOXYLKAEMPFEROL 7 RHAMNOSIDE; ASTRAGALIN; CHRYSIN; FLAVONOID GLYCOSIDE; HERBACEOUS AGENT; HYPERIN; ISOQUERCETRIN; ISORHAMNETIN; KAEMPFEROL; KAEMPFEROL 3 (6'' PARA COUMAROYL)GLUCOSIDE; KAEMPFEROL 3 GALACTOSIDE; KAEMPFEROL 7 O GLUCOSIDE; KAEMPFEROL DERIVATIVE; LUTEOLIN; NATURAL PRODUCT; QUERCETIN; QUERCETIN 3' GLUCOSIDE; QUERCETIN DERIVATIVE; QUERCIMERITRIN; UNCLASSIFIED DRUG; WOGONIN;

ARTICLE; COLUMN CHROMATOGRAPHY; COTTON; DRUG DETERMINATION; GOSSYPIUM HERBACEAM; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; PRIORITY JOURNAL; PROTON NUCLEAR MAGNETIC RESONANCE; STRUCTURE ANALYSIS;

BIOLOGICAL PRODUCTS; CHROMATOGRAPHY, LIQUID; COMPLEX MIXTURES; GOSSYPIUM; MAGNETIC RESONANCE SPECTROSCOPY; MASS SPECTROMETRY; PLANT EXTRACTS; TIME FACTORS;

EID: 57849113438     PISSN: 00032670     EISSN: 18734324     Source Type: Journal    
DOI: 10.1016/j.aca.2008.11.002     Document Type: Article

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