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Tetrameric 1 was synthesized according to Higuchi et al. (Hayashi, N.; Naoe, A.; Miyabayashi, K.; Yamada, M.; Miyake, M.; Higuchi, H. Tetrahedron Lett. 2004, 45, 8215), and its purity was documented by various spectroscopic data and elemental analysis (see the Supporting Information).
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Tetrameric 1 was synthesized according to Higuchi et al. (Hayashi, N.; Naoe, A.; Miyabayashi, K.; Yamada, M.; Miyake, M.; Higuchi, H. Tetrahedron Lett. 2004, 45, 8215), and its purity was documented by various spectroscopic data and elemental analysis (see the Supporting Information).
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1H MNR spectra (see the Supporting Information).
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1H MNR spectra (see the Supporting Information).
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32
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Chiral solvents 5-9 were purchased from Aldrich Chemical Co. and Fluka Chemica AG and used as received.
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Chiral solvents 5-9 were purchased from Aldrich Chemical Co. and Fluka Chemica AG and used as received.
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