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note
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It was found in the reaction between piperonal and benzylamine that it is not really necessary to heat the ionic liquid under vacuum to recover its activity. It was still active even after 3 runs only by removing the solvent under vacuum.
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5644300566
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note
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2O (3 × 5 mL) by simple decantation. The combined organic phases were concentrated at reduced pressure to furnish the crude product. The recovered ionic liquid containing molecular sieves was dried at 60-70 °C under vacuum (0.1 mm Hg) for 0.5 h.
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note
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All the compounds gave satisfactory spectroscopic data.
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