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X-ray crystal data for 3: C68H162Cl 2Li6O29P4Ti4, Mr, 1748.15, monoclinic, space group C 2/c, a, 30.5054(7) Å, b, 17.9005(5) Å, c, 21.8176(4) Å, α, 90°, β, 114.4919(14)°, γ, 90°, V, 10841.8 Å3, Z, 4, F(000, 3768,p, 1.071 kg m-3, μ, 0.453 mm-1, crystal dimensions, 0.10 X 0.22 X 0.32 mm, T, 193 K, radiation Mo-K α (λ, 0.71073 Å, scan type ω/Θ, Θmax, 27.47°, number of measured reflections: 44530, number of independent reflections: 21946, number of reflections in refinement: 13193, I > 3.00σI, number of parameters: 529, R, 0.0682, Rw, 0.0359, weighting scheme ω·[1, δF/6σF
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[8] Scattering factors have been taken from the International Tables, vol. IV, Table 2.2B. CCDC-204453 contains the supplementary crystallographic data for compound 3. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.
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