Stepwise effects of the BCR sequential chemical extraction procedure on dissolution and metal release from common ferromagnesian clay minerals: A combined solution chemistry and X-ray powder diffraction study

Science of the Total Environment

Volumn 407, Issue 1, 2008, Pages 603-614

  Ryan, P C ^a   Hillier, S ^b   Wall, A J ^c  

^a MIDDLEBURY COLLEGE   (United States)

^b SCOTTISH CROP RESEARCH INSTITUTE   (United Kingdom)

^c PENNSYLVANIA STATE UNIVERSITY   (United States)

Author keywords

Chlorite; Sediments; Sequential chemical extraction; Smectite; Soils; Trace metal speciation

Indexed keywords

AMINES; CHEMICAL SPECIATION; CLAY MINERALS; DIFFRACTION; DISSOLUTION; HYDROGEN; HYDROGEN BONDS; HYDROGEN PEROXIDE; IRON COMPOUNDS; METAL RECOVERY; METALS; MINERALOGY; MINING; ORGANIC COMPOUNDS; OXIDATION; POWDER METALS; POWDERS; REACTION KINETICS; SEDIMENTATION; SEDIMENTOLOGY; SEDIMENTS; SILICA; SILICATE MINERALS; SOILS; STRUCTURAL METALS; TRACE ANALYSIS; TRACE ELEMENTS; X RAY ANALYSIS; X RAY DIFFRACTION ANALYSIS;

AQUA REGIA; CHLORITE; COMBINED SOLUTIONS; HYDROXYLAMINE HYDROCHLORIDES; METAL RELEASES; MINERAL DISSOLUTIONS; MINERAL MASSES; NONTRONITE; ORGANIC MATTERS; OXIDATION OF FE; PHYLLOSILICATE CLAYS; POWDER DIFFRACTIONS; REFERENCE CLAYS; SEQUENTIAL CHEMICAL EXTRACTION; SEQUENTIAL CHEMICAL EXTRACTIONS; SEQUENTIAL EXTRACTION PROCEDURES; SMECTITE; SOLID PHASIS; TRACE METAL SPECIATION; TRACE METALS; X-RAY DIFFRACTIONS;

MINERALS;

CARBONIC ACID; CHLORIDE; FERROMAGNESIAN; FERROUS ION; HYDROGEN PEROXIDE; HYDROXIDE; HYDROXYLAMINE; MANGANESE; MINERAL; ORGANIC MATTER; OXYGEN; PHYLLOSILICATE; SILICATE; SILICON DIOXIDE; SODIUM CHLORITE; SULFIDE; TRACE ELEMENT; TRACE METAL; UNCLASSIFIED DRUG;

CLAY MINERAL; DISSOLUTION; EXTRACTION METHOD; HYDROGEN PEROXIDE; HYDROLYSIS; SPECIATION (CHEMISTRY); STOICHIOMETRY; TRACE ELEMENT; X-RAY DIFFRACTION;

ARTICLE; CHEMICAL COMPOSITION; CHEMICAL STRUCTURE; CLAY; DISSOLUTION; OXIDATION; PRIORITY JOURNAL; STOICHIOMETRY; X RAY POWDER DIFFRACTION;

ALUMINUM SILICATES; CHEMISTRY, ANALYTICAL; CHLORIDES; IRON; MAGNESIUM; METALS; SILICATES; SOLUTIONS; TRACE ELEMENTS; X-RAY DIFFRACTION;

EID: 56249134921     PISSN: 00489697     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.scitotenv.2008.09.019     Document Type: Article

References (47)

1. Aspandiar M.F., and Eggleton R.A. Weathering of chlorite: I. Reactions and products in microsystems controlled by the primary mineral. Clays Clay Miner 50 (2002) 685-698
2. Bacon J.R., and Davidson C.M. Is there a future for sequential chemical extraction?. Analyst 133 (2008) 25-46
3. Bain D.C. The weathering of chloritic minerals in some Scottish soils. J Soil Sci 28 (1977) 144-164
4. Bain D.C., and Duthie D.M.L. The effect of weathering in the silt fractions on the apparent stability of chlorite in Scottish soil clays. Geoderma 34 (1984) 221-227
5. Borggaard O.K., Lindgreen H.B., and Mørup S. Oxidation and reduction of structural iron in chlorite at 480 °C. Clays Clay Miner 30 (1982) 353-364
6. Brindley G.W., and Maksimovic Z. The nature and nomenclature of hydrous nickel-containing silicates. Clay Miner 10 (1974) 271-277
7. Brandt F., Bosbach D., Krawczyk-Bärsch E., Arnold T., and Bernhard G. Chlorite dissolution in the acid pH-range: a combined microscopic and macroscopic approach. Geochim Cosmochim Acta 67 (2003) 1451-1461
8. Brigatti M.F., Lugli C., Poppi L., and Venturelli G. Iron-rich saponite: dissolution reactions and Cr uptake. Clays Clay Miner 34 (1999) 637-645
9. Brookins D.G. Eh-pH diagrams for geochemistry (1988), Springer-Verlag, Berlin 176 pp.
10. Clark M.W., Davies-McConchie F., McConchie D., and Birch G.F. Selective chemical extraction and grainsize normalisation for environmental assessment of anoxic sediments: validation of an integrated procedure. Sci Total Environ 258 (2000) 149-170
11. Clark R.N., King T.V.V., Klejwa M., Swayze G., and Vergo N. High spectral resolution reflectance spectroscopy of minerals. J Geophys Res 95 (1990) 12653-12680
12. Dähn R., Scheidegger A.M., Manceau A., Schlegel M.L., Baeyens B., Bradbury M.H., et al. Neoformation of Ni phyllosilicate upon Ni uptake on montmorillonite: a kinetics study by powder and polarized extended X-ray absorption fine structure spectroscopy. Geochim Cosmochim Acta 66 (2002) 2335-2347
13. Gates W.P., Wilkinson H.T., and Stucki J.W. Swelling properties of microbially reduced ferruginous smectite. Clays Clay Miner 41 (1993) 360-364
14. Gaudin A., Petit S., Rose J., Martin F., Decarreau A., Noack Y., et al. Accurate crystal chemistry of ferric smectites from the lateritic nickel ore of Murrin Murrin (Western Australia); I, XRD and multi-scale chemical approaches. Clay Miner 39 (2004) 301-315
15. Hamer M., Graham R.C., Amrhein C., and Bozhilov K.N. Dissolution of ripidolite (Mg, Fe-chlorite) in organic and inorganic acid solutions. Soil Sci Soc Am J 67 (2003) 654-661
16. Hillier S. Use of an air-brush to spray dry specimens for X-ray powder diffraction. Clay Miner 34 (1999) 127-135
17. Jaisi D.P., Kukkadapu R.K., Eberl D.D., and Dong H. Control of Fe(III) site occupancy on the rate and extent of microbial reduction of Fe(III) in nontronite. Geochim Cosmochim Acta 69 (2005) 5429-5440
18. Jaisi D.P., Dong H., and Liu C. Influence of biogenic Fe(II) on the extent of microbial reduction of Fe(III) in clay minerals nontronite, illite, and chlorite. Geochim Cosmochim Acta 71 (2007) 1145-1158
19. Kohut C.K., and Warren J.C. Chlorites. In: Ammonette, J.E., Bleam, W.F., Schulze, D.G., Dixon, and J.B. (Eds). Soil mineralogy with environmental applications (2002) 531-554 Soil Science Society of America Book Series No.7.
20. Komadel P., Madejova J., and Stucki J.W. Reduction and reoxidation of nontronite: questions of reversibility. Clays Clay Miner 43 (1995) 105-110
21. Köster H.M., Ehrlicher U., Gilg H.A., Jordan R., Murad E., and Onnich K. Mineralogical and chemical characteristics of five nontronites and Fe-rich smectites. Clay Miner 34 (1999) 579-599
22. Krawczyk-Bärsch E., Arnold T., Reuther H., Brandt F., Bosbach D., and Bernhard G. Formation of secondary Fe-oxyhydroxide phases during the dissolution of chlorite-effects on uranium sorption. Appl Geochem 19 (2004) 1403-1412
23. Langmuir D. Aqueous environmental geochemistry (1997), Prentice-Hall, Upper Saddle River, New Jersey 600 pp.
24. Lynn W.C., and Whittig L.D. Alteration and formation of clay minerals during cat clay development. Clays Clay Miner 14 (1966) 241-248
25. McBride M.B. Environmental chemistry of soils (1997), Oxford Univ Press, New York 406 pp.
26. Manceau A., Marcus M.A., Tamura N., Proux O., Geoffroy N., and Lanson B. Natural speciation of Zn at the micrometer scale in a clayey soil using X-ray fluorescence, absorption, and diffraction. Geochim Cosmochim Acta 68 (2004) 2467-2483
27. Moore D.M., and Reynolds Jr. R.C. X-ray diffraction and the identification and analysis of clay minerals (1997), Oxford Univ. Press, New York New York, 378 pp.
28. Nagy K.L., Blum A.E., and Lasaga A.C. Dissolution and precipitation kinetics of kaolinite at 80 °C and pH 3: the dependence on solution saturation state. Am J Sci 291 (1991) 649-686
29. Newman A.C.D., and Brown G. The chemical constitution of clays. In: Newman, and A.C.D. (Ed). The chemistry of clays and clay minerals (1987), Mineralogical Society, London 1-128
30. Novák I., and Číčel B. Dissolution of smectites in hydrochloric acid: II. Dissolution rate as a function of crystallochemical composition. Clays Clay Miner 26 (1978) 341-344
31. Oze C., Fendorf S.E., Bird D.K., and Coleman R. Chromium geochemistry in serpentinized ultramafic rocks and serpentine soils in the Franciscan Complex of California. Am J Sci 304 (2004) 67-101
32. Post J.L. Saponite near Ballarat, California. Clays Clay Miner 32 (1984) 147-153
33. Post J.L., and Plummer C.C. The chlorite series of Flagstaff Hill area, California: a preliminary investigation. Clays Clay Miner 20 (1972) 271-283
34. Quevauviller P.h., van der Sloot H.A., Ure A., Muntau H., Gomez A., and Rauret G. Conclusions of the workshop: harmonization of leaching/extraction tests for environmental risk assessment. Sci Total Environ 178 (1996) 133-139
35. Rauret G., López-Sànchez J.F., Sahuquillo A., Rubio R., Ure A.M., Davidson C.M., et al. Improvement of the BCR three step sequential extraction procedure prior to the certification of new sediment and soil reference materials. J Environ Monit 1 (1999) 57-61
36. Rauret G., López-Sànchez J.F., Sahuquillo A., Ure A.M., Davidson C.M., Gomez A., et al. Application of a modified BCR sequential extraction (three-step) procedure for the determination of extractable trace metal contents in a sewage sludge amended soil reference material (CRM 483), complemented by a three-year stability study of acetic acid and EDTA extractable metal content. J Environ Monit 2 (2000) 228-233
37. Ross G.J. Acid dissolution of chlorites: Release of magnesium, iron and aluminum and mode of acid attack. Clays Clay Miner 17 (1969) 347-354
38. Ross G.J., and Kodama H. Experimental alteration of a chlorite into a regularly interstratified chlorite-vermiculite by chemical oxidation. Clays Clay Miner 24 (1976) 183-190
39. Ryan P.C., Wall A.J., Hillier S.J., and Clark L. Insights into sequential chemical extraction procedures from quantitative XRD: a study of trace metal partitioning in sediments related to frog malformities. Chem Geol 184 (2002) 337-357
40. Scheckel K.G., and Ryan J.A. Spectroscopic speciation and quantification of lead in phosphate-amended soils. J Environ Qual 33 (2004) 1288-1295
41. Senkayi A.L., Dixon J.B., and Hossner L.R. Transformation of chlorite to smectite through regularly interstratified intermediates. Soil Sci Soc Am J 45 (1981) 650-656
42. Stucki J.W., Golden D.C., and Roth C.B. Effects of reduction and reoxidation of structural iron on the surface charge and dissolution of dioctahedral smectites. Clays Clay Miner 32 (1984) 350-356
43. Suarez Barrios M., de Santiago Buey C., Garcia Romero E., and Martin Pozas J.M. Textural and structural modifications of saponite from Cerro del Aguila by acid treatment. Clay Miner 36 (2001) 483-488
44. Sulkowski M., and Hirner A.V. Element fractionation by sequential extraction in a soil with high carbonate content. Appl Geochem 21 (2006) 16-28
45. Tessier A., Campbell P.G.C., and Bisson M. Sequential extraction procedure for the speciation of particulate trace metals. Anal Chem 51 (1979) 844-851
46. Wieland E., Wehrli B., and Stumm W. The coordination chemistry of weathering. III. A generalization on the dissolution rates of minerals. Geochim Cosmochim Acta 52 (1988) 1969-1981
47. Young S.D., Zhang H., Tye A.M., Maxted A., Thums C., and Thornton I. Characterizing the availability of metals in contaminated soils. I. The solid phase: sequential extraction and isotopic dilution. Soil Use Manage 21 (2006) 450-458