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Volumn 47, Issue 39, 2008, Pages 7547-7550

Multilateral solid-state metathesis reactions for the preparation of materials with heteroanions: The [Si(CN2)4]4- ion

Author keywords

Lanthanoids; Metathesis; Silicates; Solid state reactions; Structure elucidation

Indexed keywords


EID: 54749139586     PISSN: 14337851     EISSN: None     Source Type: Journal    
DOI: 10.1002/anie.200801784     Document Type: Article
Times cited : (28)

References (52)
  • 6
    • 0037119723 scopus 로고    scopus 로고
    • Angew. Chem. Int. Ed. 2002, 41, 3322-3336.
    • (2002) Angew. Chem. Int. Ed , vol.41 , pp. 3322-3336
  • 39
    • 54749092590 scopus 로고    scopus 로고
    • Crystal -structure data for KLa[Si(CN2)4, Mr, 732.44, orthorhombic, space group P2 1221, a, 7.601(1, b, 6.854 (1, c, 9.486(2) Å, Z, 2, F(000, 340, ρcalcd, 2.46 gcm-3, μ, 4.84 mm-1, crystal dimensions: 0.17 × 0.04 × 0.04 mm3, θ, 3.43-25.89°, Mo Kα radiation (γ, 0.71073 Å, T, 293 K, 3740 reflections were collected (STOE-IPDS diffractometer, of which 908 were independent (Rint, 0.048, Data were corrected for Lorentz, polarization, and absorption effects (software: STOE IPDS I, The structure was solved by direct methods (SHELXS) and refined by the method of full matrix least squares against F2, data/parameter ratio 12.97, final R values: R1, 0.0287, wR2, 0.0612 for all data, GOF, 1.030. b) Crysta
    • 4]).


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.