The First Crystalline Solids in the Ternary Si-C-N System

Angewandte Chemie (International Edition in English)

Volumn 36, Issue 6, 1997, Pages 603-606

  Riedel, Ralf ^a   Greiner, Axel ^a   Miehe, Gerhard ^a   Dressler, Wolfgang ^a   Fuess, Hartmut ^a   Bill, Joachim ^b   Aldinger, Fritz ^b  

^a DARMSTADT UNIVERSITY OF TECHNOLOGY   (Germany)

^b MAX PLANCK INSTITUTE FOR INTELLIGENT SYSTEMS   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0030997290     PISSN: 05700833     EISSN: None     Source Type: Journal    
DOI: 10.1002/anie.199706031     Document Type: Article

References (37)

1. K. Komeya, M. Matsui in Materials Science and Technology Vol. 11 (Eds.: R. W. Cahn, P. Haasen, E. J. Kramer), VCH, Weinheim, 1994, p. 517-565.
2. a) A. Y. Liu, M. L. Cohen, Science 1989, 245, 841-842;
3. b) C. Niu, Y. Z. Lu, C. M. Lieber, ibid. 1993, 261, 334-337;
4. c) P. H. Fang, J. Mater. Sci. Lett. 1995, 14, 536-538.
5. F. Wakai, Y. Kodama, S. Sakaguchi, N. Murayama, K. Izaki, K. Niihara, Nature 1990, 344, 421-423.
6. K. Niihara, J. Ceram. Soc. Jpn. 1991, 99, 974-982.
7. R. Riedel, H.-J. Kleebe, H. Schönfelder, F. Aldinger, Nature 1995, 374, 526-528.
8. a) R. Riedel, Nicht-oxidische Keramiken aus anorganischen Vorstufen, Materialkundlich-Technische Reihe 12, Gebrüder Bornträger, Berlin, Stuttgart. 1993;
9. b) R. Riedel, G. Passing, H. Schönfelder, R. J. Brook, Nature 1992, 355, 714-717.
10. D. Seyferth, G. H. Wiseman, J. Am. Ceram. Soc. 1984, 67, C132-C133.
11. a) T. Kawamura, Mineral, J. 1965, 4, 333-355;
12. b) W. Schnick, Angew. Chem. 1993, 105, 846-858; Angew. Chem. Int. Ed. Engl. 1993, 32, 806.
13. b) W. Schnick, Angew. Chem. 1993, 105, 846-858; Angew. Chem. Int. Ed. Engl. 1993, 32, 806.
14. A. Kienzle, A. Obermeyer, R. Riedel, F. Aldinger, A. Simon, Chem. Ber. 1993, 126, 2569-2571.
15. A. Obermeyer, A. Kienzle, J. Weidlein, R. Riedel, A. Simon, Z. Anorg. Allg. Chem. 1994, 620, 1357-1363.
16. (Bragg) = 0.0178. Further details of the crystal structure investigation may be obtained from the Fachinformationszentrum Karlsruhe, D-76344 Eggenstein-Leopoldshafen (Germany), on quoting the depository number CSD-59342.
17. M. J. Zawarotko, Chem. Soc. Rev. 1994, 283-288.
18. Rietveld refinement program LHPM 7: a) D. B. Wiles, R. A. Young, J. Appl. Crystallogr. 1981, 14, 149; b) C. J. Howard, R. J. Hill, Aust, A. E. C. Res. Establ. Rep. AAEC M112 1986.
19. Rietveld refinement program LHPM 7: a) D. B. Wiles, R. A. Young, J. Appl. Crystallogr. 1981, 14, 149; b) C. J. Howard, R. J. Hill, Aust, A. E. C. Res. Establ. Rep. AAEC M112 1986.
20. H.-D. Schädler, L. Jäger, I. Senf, Z. Anorg. Allg. Chem. 1993, 619, 1115-1120.
21. K. R. Carduner, C. S. Blackwell, W. B. Hammond, F. Reidinger, G. R. Hatfield, J. Am. Chem. Soc. 1990, 112, 4676-4679.
22. 4 is strong evidence for the existence of the carbodiimide rather than cyanamide structure (see also ref. [24]).
23. (Bragg) = 0.067. Further details of the crystal structure investigation may be obtained from the Fachinformationszentrum Karlsruhe, D-76344 Eggenstein-Leopoldshafen (Germany), on quoting the depository number CSD-59342.
24. J. Sjoeberg, G. Helgesson, I. Idrestedt, Acta Crystallogr. Sect. C 1991, 47, 2438-2441.
25. M. G. Down, M. J. Haley, P. Hubberstey, R. J. Pulham, A. E. Thunder, J. Chem. Soc. Dalton Trans. 1978, 1407-1411.
26. A. Harper, P. Hubberstey, J. Chem. Res. Synop. 1989, 194-195.
27. M. J. Sole, A. D. Yoffe, Proc. R. Soc. A 1964, 227, 498-522.
28. K. M. Adams, M. J. Cooper, M. J. Sole, Acta Crystallogr. 1964, 17, 1449-1451.
29. R. Dronskowski, Z. Naturforsch. B 1995, 50, 1245-1251.
30. U. Berger, W. Schnick, J. Alloys Comp. 1994, 206, 179-184.
31. N.-G. Vannerberg, Acta Chem. Scand. 1962, 16, 2263-2266.
32. A. Kienzle, K. Wurm, J. Bill, F. Aldinger, R. Riedel in Organosilicon Chemistry II, (Eds.: N. Auner, J. Weis), VCH, Weinheim, 1996, pp. 725-731.
33. a) J. Bill, A. Kienzle, F. Aldinger, R. Riedel, DE 44 47 534 A1, 1996;
34. b) D. Seyferth, C. Strohmann, A. J. Perotta, J. P. Gardner, Mater. Res. Soc. Symp. Proc. 1994, 327, 191-199.
35. A Netzsch STA429 coupled with a Balzers QMG420 was used for simultaneous thermal analysis and MS measurements. TEM was performed with a Philips CM20 microscope equipped with a HP Ge-detector (NORAN, System Voyager at 200 kV. IR spectra were recorded on a Perkin Elmer 1750 FT-IR, and MAS-NMR spectra on a Varian Unity+400 and a Bruker MSL 300 equipped with a standard probe. Elemental analyses were conducted at Mikro-analytisches Labor Pascher (53424 Remagen-Bandorf, Germany) or with a LECO TC 436 N/O-Analyser for N and O and a LECO CS 244 Analyser for C and ICP-AES for Si (Instruments SA, JY 70 +).
36. I. A. Vostokov, Y. I. Dergunov, A. S. Gordetsov, Zh. Obshch. Khim. 1977, 47, 1769-1771.
37. J. Weiss, H. L. Lukas, J. Lorenz, G. Petzow, H. Krieg, CALPHAD Comp. Coupling Phase Diagrams Thermochem 1981, 5, 125-140.