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58149315951
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This paper is dedicated to the memory of late Professor Yoshihiko Ito, Emeritus Professor of Kyoto University
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This paper is dedicated to the memory of late Professor Yoshihiko Ito, Emeritus Professor of Kyoto University.
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58149282590
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FeIIIEtio(CF3)4Pc}2(μ-O, 1, μ-Oxo-bis{2,7,12,17tetraethy1-3,6,13,16- tetrakis(trifluoromethyl)porphycenatoiron(III, FeIIIClEtio(CF 3)4Pc, 2-Cl)=Chloro-2,7,12,17-tetraethyl-3,6,13, 16-tetrakis(trifluoromethyl)porphycenatoiron(III, FeIIIEtio(CF 3)4-Pc(py)2, 2-Py2, Bispyridine-2,7,12,17-tetraethyl-3,6,13,16-tetrakis(trifluoromethyl) porphycenatoiron(III, FeIIIEtio(CH3) 4-Pc}2(μ-O, 3, μ-Oxo-bis{2,7,12,17- tetraethyl-3,6,13,16-tetra-methylporphycenatoiron(III, Fe IIIClEtio(CH3)4Pc, 4-Cl, Chloro-2,7,12,17- tetraethyl-3,6,13,16-tetramethylporphycenatoiron(III, Fe IIIEtio(CH3)4Pc(py)2, 4-Py 2, Bispyridine-2,7,12,17-tetraethyl-3,6,13,16- tetramethylporphycenatoironII
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2(μ-O)] (9) = //-Oxo-bis|l,3,5,7-tetramethyl-2,4,6,8- tetraethylporphyrinatoiron(III)}.
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SAINT Software Package, Version 6.45, Bruker AXS, Inc., Madison, WI 53711-5373, USA, 2001.
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58149299098
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Although the refinement of the crystal structure of 7 has never been completed, the Fe-Npyridyl and Fe-Npyrroic bond distances were preliminary determined as 2.02 and 2.00 A, respectively
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c bond distances were preliminary determined as 2.02 and 2.00 A, respectively.
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58149304542
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2 at 25 °C.
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2 at 25 °C.
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0001020094
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58149299099
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It was confirmed that the reaction was completed after 28 h
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It was confirmed that the reaction was completed after 28 h.
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58149318540
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28
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0037041608
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