Five- and four-coordinate 1,3-diaza-2-yttria- and 1,3-diaza-2-scandia-[3] ferrocenophanes

European Journal of Inorganic Chemistry

Volumn , Issue 21, 2008, Pages 3340-3347

  Wrackmeyer, Bernd ^a   Klimkina, Elena V ^a   Milius, Wolfgang ^a  

^a UNIVERSITY OF BAYREUTH   (Germany)

Author keywords

NMR spectroscopy; Scandium; X ray structural analysis; Yttrium; 3 Ferrocenophanes

Indexed keywords

ATOMS; CHLORINE COMPOUNDS; LIGANDS; PYRIDINE; SODIUM COMPOUNDS; SPECTROSCOPIC ANALYSIS; STRUCTURAL ANALYSIS; YTTRIUM; YTTRIUM COMPOUNDS;

ATE COMPLEX; DIAMIDO LIGANDS; DIAMINOFERROCENE; DIPYRIDINE; FERROCENOPHANES; NMR-SPECTROSCOPY; PYRIDINE LIGANDS; TRIMETHYLSILYL; X RAY STRUCTURAL ANALYSIS; [3]FERROCENOPHANE;

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

EID: 53349171653     PISSN: 14341948     EISSN: 10990682     Source Type: Journal    
DOI: 10.1002/ejic.200800399     Document Type: Article

References (66)

1. M. F. Lappert, P. P. Power, A. R. Sanger, R. C. Srivastava, Metal and Metalloid Amides: Synthesis Structure, and Physical and Chemical Properties, Ellis Horwood, Chichester, 1980, p. 847.
2. a) M. F. Lappert, J. Organomet. Chem. 2000, 600, 144-158;
3. b) R. Kempe, Angew. Chem. 2000, 112, 478-504;
4. Angew. Chem. Int. Ed. 2000, 39, 468-493;
5. c) R. Kempe, H. Noss, T. Irrgang, J. Organomet. Chem. 2002, 647, 12-20;
6. d) L. H. Gade, Acc. Chem. Res. 2002, 35, 575-582;
7. e) O. Belda, C. Moberg, Coord. Chem. Rev. 2005, 249, 727-740.
8. A. Shafir, M. P. Power, G. D. Whitener, J. Arnold, Organometallics 2001, 20, 1365-1369.
9. M. J. Monreal, C. T. Carver, P. L. Diaconescu, Inorg. Chem. 2007, 46, 7226-7228.
10. a) A. Shafir, J. Arnold, J. Am. Chem. Soc. 2001, 123, 9212-9213;
11. b) M. Herberhold, Angew. Chem. 2002, 114, 998-1000;
12. Angew. Chem. Int. Ed. 2002, 41, 956-958.
13. A. Shafir, J. Arnold, Organometallics 2003, 22, 567-575.
14. I. Westmoreland, J. Arnold, Acta Crystallogr., Sect. E: Struct. Rep. Online 2006, 62, m2272-m2273.
15. a) I. Westmoreland, J. Arnold, Acta Crystallogr., Sect. E: Struct. Rep. Online 2006, 62, m2303-m2304;
16. b) M. J. Monreal, P. L. Diaconescu, Organometallics 2008, 27, 1702-1706.
17. C. T. Carver, M. J. Monreal, P. L. Diaconescu, Organometallics 2008, 27, 363-370.
18. a) A. Shafir, D. Fiedler, J. Arnold, Chem. Commun. 2003, 2598-2599;
19. b) A. Shafir, D. Fiedler, J. Arnold, J. Chem. Soc., Dalton Trans. 2002, 555-560;
20. c) P. D. Beer, Z. Chen, M. G. B. Drew, A. O. M. Johnson, D. K. Smith, P. Spencer, Inorg. Chim. Acta 1996, 246, 143-150.
21. a) J. Eppinger, K. R. Nikolaides, M. Zhang-Presse, F. A. Riederer, G. W. Rabe, A. L. Rheingold, Organometallics 2008, 27, 736-740;
22. b) U. Siemeling, T.-C. Auch, S. Tomm, H. Fink, C. Bruhn, B. Neumann, H.-G. Stammler, Organometallics 2007, 26, 1112-1115;
23. c) A. Shafir, J. Arnold, Inorg. Chim. Acta 2003, 345, 216-220;
24. d) V. C. Gibson, N. J. Long, E. L. Marshall, P. J. Oxford, A. J. P. White, D. J. Williams, J. Chem. Soc., Dalton Trans. 2001, 1162-1164;
25. e) U. Siemeling, O. Kuhnert, B. Neumann, A. Stammler, H.-G. Stammler, B. Bildstein, M. Malaun, P. Zanello, Eur. J. Inorg. Chem. 2001, 913-916.
26. a) B. Wrackmeyer, E. V. Klimkina, W. Milius, O. L. Tok, M. Herberhold, Inorg. Chim. Acta 2005, 358, 1420-1428;
27. b) B. Wrackmeyer, E. V. Klimkina, H. E. Maisel, W. Milius, M. Herberhold, Inorg. Chim. Acta 2004, 357, 1703-1710.
28. a) B. Wrackmeyer, E. V. Klimkina, W. Milius, Eur. J. Inorg. Chem. 2008, 306-311;
29. b) B. Wrackmeyer, E. V. Klimkina, W. Milius, Z. Naturforsch. 2007, 62b, 1259-1266;
30. c) B. Wrackmeyer, E. V. Klimkina, W. Milius, Z. Anorg. Allg. Chem. 2007, 633, 1964-1972;
31. d) B. Wrackmeyer, E. V. Klimkina, W. Milius, Polyhedron 2007, 26, 3496-3504;
32. e) B. Wrackmeyer, E. V. Klimkina, W. Milius, Inorg. Chem. Commun. 2006, 9, 716-721.
33. a) B. Wrackmeyer, E. V. Klimkina, W. Milius, Z. Anorg. Allg. Chem. 2008, 634, 311-316;
34. b) B. Wrackmeyer, E. V. Klimkina, W. Milius, Z. Anorg. Allg. Chem. 2006, 632, 2331-2340;
35. c) B. Wrackmeyer, E. V. Klimkina, W. Milius, Inorg. Chem. Commun. 2004, 7, 884-888;
36. d) B. Wrackmeyer, E. V. Klimkina, W. Milius, Inorg. Chem. Commun. 2004, 7, 412-416;
37. e) B. Wrackmeyer, E. V. Klimkina, W. Milius, Struct. Chem. 2004, 15, 333-337;
38. f) B. Wrackmeyer, W. Milius, H. E. Maisel, H. Vollrath, M. Herberhold, Z. Anorg. Allg. Chem. 2003, 629,1169-1174;
39. g) B. Wrackmeyer, H. E. Maisel, W. Milius, M. Herberhold, J. Organomet. Chem. 2003, 680, 271-280.
40. K. Stott, J. Keeler, Q. N. Van, A. J. Shaka, J. Magn. Reson. 1997, 125, 302-324.
41. A. E. Derome, Modern NMR Techniques for Chemistry Research, Pergamon, Oxford, 1987, pp. 188-190.
42. a) D. Riegert, J. Collin, J.-C. Daran, T. Fillebeen, E. Schulz, D. Lyubov, G. Fukin, A. Trifonov, Eur. J. Inorg. Chem. 2007, 1159-1168;
43. b) S. T. Liddle, P. L. Arnold, Dalton Trans. 2007, 3305-3313;
44. c) Y. Yao, X. Lu, Q. Shen, K. Yu, J. Chem. Chrystallogr. 2004, 34, 275-279;
45. d) A. G. Avent, F. G. N. Cloke, B. R. Elvidge, P. B. Hitchcock, Dalton Trans. 2004, 1083-1096;
46. e) T. G. Wetzel, S. Dehnen, P. W. Roesky, Angew. Chem. 1999, 111, 1155-1158;
47. Angew. Chem. Int. Ed. 1999, 38, 1086-1088;
48. f) A. Spannenberg, P. Arndt, R. Kempe, Angew. Chem. 1998, 110, 824-827;
49. Angew. Chem. Int. Ed. 1998, 37, 832-835;
50. g) H. C. Aspinall, M. R. Tillotson, Polyhedron 1994, 13, 3229-3234.
51. T. Parella, J. Magn. Reson. 2004, 167, 266-272.
52. a) R. E. White, T. P. Hanusa, Organometallics 2006, 25, 5621-5630;
53. b) D. Gudat, Ann. Rep. NMR Spectrosc. 2003, 51, 59-103;
54. c) C. J. Schaverien, Organometallics 1994, 13, 69-82;
55. d) J. Eppinger, M. Spiegler, W. Hieringer, W. A. Herrmann, R. Anwander, J. Am. Chem. Soc. 2000, 122, 3080-3096.
56. a) J. Kronenbitter, A. Schwenk, J. Magn. Reson. 1977, 25, 147-165;
57. b) G. C. Levy, P. L. Rinaldi, J. T. Bailey, J. Magn. Reson. 1980, 40, 167-173.
58. M. Herberhold, Angew. Chem. 1995, 107, 1985-1987;
59. Angew. Chem. Int. Ed. Engl. 1995, 34, 1837-1839.
60. a) T. I. Gountchev, T. D. Tilley, Organometallics 1999, 18, 2896-2905;
61. b) H. Noss, M. Oberthuer, C. Fischer, W. P. Kretschmer, R. Kempe, Eur. J. Inorg. Chem. 1999, 2283-2288.
62. P. W. Roesky, Organometallics 2002, 21, 4756-4761.
63. a) G. A. Morris, R. Freeman, J. Am. Chem. Soc. 1979, 101, 760-762;
64. b) G. A. Morris, J. Am. Chem. Soc. 1980, 102, 428-429;
65. c) J. Schraml in The Chemistry of Organic Silicon Compounds (Eds.: Z. Rappoport, Y. Apeloig), Wiley, Chichester, 2001, vol. 3, pp. 223-339.
66. CCDC-681432 (3 at 133 K), -681431 (5 at 293 K) and -681433 (6a at 173 K) contain the supplementary crystallographic data. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.