A pyridine-stabilized alumoxane containing two 1,3,2-diazaalumina[3] ferrocenophane units

European Journal of Inorganic Chemistry

Volumn , Issue 2, 2008, Pages 306-311

  Wrackmeyer, Bernd ^a   Klimkina, Elena V ^a   Milius, Wolfgang ^a  

^a UNIVERSITY OF BAYREUTH   (Germany)

Author keywords

Aluminum; Alumoxanes; Amides; NMR spectroscopy

Indexed keywords

ALUMINUM COMPOUNDS; CHLORINE COMPOUNDS; COORDINATION REACTIONS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PYRIDINE; SYNTHESIS (CHEMICAL);

ALUMINUM ATOMS; ALUMOXANE; FERROCENOPHANES; HIGH YIELD SYNTHESIS; NMR-SPECTROSCOPY; SIDE PRODUCTS; TRIMETHYLSILYL; X RAY STRUCTURAL ANALYSIS;

CRYSTALLINE MATERIALS;

EID: 38449117021     PISSN: 14341948     EISSN: 10990682     Source Type: Journal    
DOI: 10.1002/ejic.200700869     Document Type: Article

References (57)

1. a) R. O. Colclough, K. Wilkinson, J. Polym. Sci. Polym. Symp. 1963, 4, 311-332;
2. b) T. Saegusa, Y. Fujii, H. Fujii, J. Furukawa, Makromol. Chem. 1962, 55, 232-235;
3. c) G. B. Sakharovskaya, N. N. Korneev, A. F. Popov, Yu. V. Kissin, S. M. Mezhikovskii, E. V. Kristal'nyi, Zh. Obshch. Khim. 1969, 39, 788-795;
4. d) H. Sinn, W. Kaminsky, H.-J. Vollmer, R. Woldt, Angew. Chem. 1980, 92, 396-402;
5. Angew. Chem. Int. Ed. Engl. 1980, 19, 390-392;
6. e) H. Sinn, W. Kaminsky, Adv. Organomet. Chem. 1980, 18, 99-149;
7. f) W. Kaminsky, Adv. Catal. 2001, 46, 89-159;
8. g) W. Kaminsky, Catal. Today 2000, 62, 23-34;
9. h) H. G. Alt, Dalton Trans. 2005, 3271-3276;
10. i) C. Janiak, Coord. Chem. Rev. 2006, 250, 66-94.
11. a) W. Uhl, M. Koch, W. Hiller, M. Heckel, Angew. Chem. 1995, 107, 1122-1124;
12. Angew. Chem. Int. Ed. Engl. 1995, 34, 989-990;
13. b) S. Pasynkiewicz, Polyhedron 1990, 9, 429-453;
14. c) M. R. Mason, J. M. Smith, S. G. Bott, A. R. Barron, J. Am. Chem. Soc. 1993, 115, 4971-4984;
15. d) J. Storre, C. Schnitter, H. W. Roesky, H.-G. Schmidt, M. Noltemeyer, R. Fleischer, D. Stalke, J. Am. Chem. Soc. 1997, 119, 7505-7513;
16. e) S. J. Obrey, A. R. Barron, J. Chem. Soc. Dalton Trans. 2001, 2456-2458;
17. f) J. L. Atwood, D. C. Hrncir, R. D. Priester, R. D. Rogers, Organometallics 1983, 2, 985-989;
18. g) K. Kacprzak, J. Serwatowski, Appl. Organomet. Chem. 2004, 18, 394-397;
19. h) N. Ueyama, T. Araki, H. Tani, Inorg. Chem. 1973, 12, 2218-2225.
20. a) J. Lewiński, W. Bury, I. Justyniak, J. Lipkowski, Angew. Chem. 2006, 118, 2938-2941;
21. Angew. Chem. Int. Ed. 2006, 45, 2872-2875;
22. b) L. G. van Poppel, S. G. Bott, A. R. Barron, J. Chem. Crystallogr. 2001, 31, 417-420;
23. c) H. W. Roesky, M. G. Walawalkar, R. Murugaval, Acc. Chem. Res. 2001, 34, 201-211;
24. d) C. N. McMahon, A. R. Barron, J. Chem. Soc. Dalton Trans. 1998, 3703-3704;
25. e) R. Kumar, H. Rahbarnoohi, M. J. Heeg, D. G. Dick, J. P. Oliver, Inorg. Chem. 1994, 33, 1103-1108;
26. f) A. Piotrowski, A. Kunicki, S. Pasynkiewicz, J. Organomet. Chem. 1980, 201, 105-112;
27. g) A. Sadownik, S. Pasynkiewicz, M. Boleslawski, H. Szachnowska, J. Organomet. Chem. 1978, 152, C49-C52;
28. h) S. Pasynkiewicz, M. Boleslawski, A. Sadownik, J. Organomet. Chem. 1976, 113, 303-309.
29. K. Knabel, I. Krossing, H. Nöth, H. Schwenk-Kircher, M. Schmidt-Amelunxen, T. Seifert, Eur. J. Inorg. Chem. 1998, 1095-1114.
30. M. Veith, J. Frères, P. König, O. Schütt, V. Huch, J. Blin, Eur. J. Inorg. Chem. 2005, 3699-3710.
31. a) W. Zheng, H. W. Roesky, M. Noltemeyer, Organometallics 2001, 20, 1033-1035;
32. b) N. Kuhn, S. Fuchs, E. Niquet, M. Richter, M. Steimann, Z. Anorg Allg. Chem. 2002, 628, 717-718;
33. c) G. Bai, H. W. Roesky, J. Li, M. Noltemeyer, H.-G. Schmidt, Angew. Chem. 2003, 115, 5660-5664;
34. Angew. Chem. Int. Ed. 2003, 42, 5502-5506;
35. d) G. Bai, S. Singh, H. W. Roesky, M. Noltemeyer, H.-G. Schmidt, J. Am. Chem. Soc. 2005, 127, 3449-3455;
36. e) S. González-Gallardo, V. Jancik, R. Cea-Olivares, R. A. Toscano, M. Moya-Cabrera, Angew. Chem. 2007, 119, 2953-2956;
37. Angew. Chem. Int. Ed. 2007, 46, 2895-2898.
38. G. Leggett, M. Motevalli, A. C. Sullivan, J. Organomet. Chem. 2000, 598, 36-41.
39. A. Shafir, M. P. Power, G. D. Whitener, J. Arnold, Organometallics 2000, 19, 3978-3982.
40. A. Shafir, M. P. Power, G. D. Whitener, J. Arnold, Organometallics 2001, 20, 1365-1369.
41. B. Wrackmeyer, E. V. Klimkina, W. Milius, Z. Anorg. Allg. Chem. 2007, in press.
42. B. Wrackmeyer, E. V. Klimkina, W. Milius, Polyhedron 2007, 26, 3496-3504.
43. B. Wrackmeyer, E. V. Klimkina, W. Milius, Inorg. Chem. Commun. 2006, 9, 716-721.
44. B. Wrackmeyer, E. V. Klimkina, W. Milius, Z. Anorg. Allg. Chem. 2007, 33, 1964-1972.
45. G. A. Razuvaev, Yu. A. Sangalov, Yu. Ya. Nel'kenbaum, K. S. Minsker, Izvest. Akad. Nauk SSSR, Ser. Khim. 1975, 2547-2553.
46. H. J. Koch, S. Schulz, H. W. Roesky, M. Noltemeyer, H.-G. Schmidt, A. Heine, R. Herbst-Irmer, D. Stalke, G. M. Sheldrick, Chem. Ber. 1992, 125, 1107-1109.
47. T. Parella, J. Magn. Reson. 2004, 167, 266-272.
48. M. Herberhold, Angew. Chem. 1995, 107, 1985-1987;
49. Angew. Chem. Int. Ed. Engl. 1995, 34, 1837-1839.
50. a) M. Linnolahti, T. N. P. Luhtanen, T. A. Pakkanen, Chem. Eur. J. 2004, 10, 5977-5987;
51. b) T. N. P. Luhtanen, M. Linnolahti, T. A. Pakkanen, J. Organomet. Chem. 2002, 648, 49-54;
52. c) R. J. Gillespie, S. A. Johnson, Inorg. Chem. 1997, 36, 3031-3039;
53. d) W. H. Fink, P. P. Power, T. L. Allen, Inorg. Chem. 1991, 36, 1431-1436.
54. a) G. A. Morris, R. Freeman, J. Am. Chem. Soc. 1979, 101, 760-762;
55. b) G. A. Morris, J. Am. Chem. Soc. 1980, 102, 428-429;
56. c) J. Schraml in The Chemistry of Organic Silicon Compounds (Eds.: Z. Rappoport, Y. Apeloig), Wiley, Chichester, 2001, vol. 3, pp. 223-339.
57. CCDC-656856 (for 6A at 293 K), -656857 (for 6A at 173 K), and -656855 (for 6B) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.