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Volumn 11, Issue 10, 2008, Pages 1132-1135

Assembly of a new Wells-Dawson polyoxometalate-templated compound based on Fe-btb complex

Author keywords

Bis(triazole) ligand; Flexible ligand; Hydrothermal synthesis; Wells Dawson polyoxometalate

Indexed keywords


EID: 52949153562     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2008.06.014     Document Type: Article
Times cited : (19)

References (45)
  • 32
    • 52949111009 scopus 로고    scopus 로고
    • note
    • 18 (5262.84): C 7.3, H 1.12, N 6.38. Found: C 7.25, H 1.15, N 6.34.
  • 33
    • 52949117745 scopus 로고    scopus 로고
    • note
    • 2 by full-matrix least squares methods using SHELXTL 97.
  • 40
    • 52949137411 scopus 로고    scopus 로고
    • note
    • Electrochemical measurements were performed with a CHI 660b electrochemical workstation. A conventional three-electrode system was used. Ag/AgCl (3 M KCl) electrode was used as a reference electrode, and a Pt wire as a counter electrode. Chemically bulk-modified carbon-paste electrode (CPE) were used as the working electrode, which was prepared as the following process: 90 mg of graphite powder and 8 mg of 1, were mixed and ground together by an agate mortar and pestle to achieve a uniform mixture, and then was added 0.1 mL of Nujol with stirring. The homogenized mixture was packed into a glass tube with a 1.5 mm inner diameter, and the tube surface was wiped with paper. Electrical contact was established with a copper rod through the back of the electrode.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.