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note
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Under ambient condition it takes approximately 5 h for 50% conversion of a 1-R complex to the corresponding 2-R complex.
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76
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51249116337
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note
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The evolved hydrogen could not be detected experimentally.
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78
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51249086127
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note
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2 group.
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79
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51249100078
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note
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A little dichloromethane was necessary to take the complex into solution. Addition of large excess of acetonitrile was necessary to record the redox responses in proper shape.
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83
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51249124744
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note
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Chemical shifts are given in ppm and multiplicity of the signals along with the associated coupling constants (J in Hz) are given in parentheses. Overlapping signals are marked with an asterisk.
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84
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51249119731
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G.M. Sheldrick, shelxs-97 and shelxl-97, Fortran programs for crystal structure solution and refinement, University of Gottingen, Gottingen, Germany, 1997.
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G.M. Sheldrick, shelxs-97 and shelxl-97, Fortran programs for crystal structure solution and refinement, University of Gottingen, Gottingen, Germany, 1997.
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