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Volumn 37, Issue 8, 2008, Pages 826-827

Substitution effects of Cp ring benzyl groups on photoisomerization of a rhodium dithionite complex in the crystalline state

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EID: 51149110068 PISSN: 03667022 EISSN: None Source Type: Journal
DOI: 10.1246/cl.2008.826 Document Type: Article

Times cited : (10)

References (14)

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- J. P. Blaha, M. S. Wrighton, J. Am. Chem. Soc. 1985, 107, 2694. Although the preparation of the benzyl derivative ligand precursor was reported in this paper, the most convenient preparation of this derivative is the method used for the preparation of the phenyl derivative. 6
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9
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- M. Björgvinsson, S. Halldorsson, I. Arnason, J. Magull, D. Fenske, J. Organomet. Chem. 1997, 544, 207.
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- See Supporting Information. It is available electronically on the CSJ-Journal web site; http://www.csj.jp/journals/chem-lett/.
- See Supporting Information. It is available electronically on the CSJ-Journal web site; http://www.csj.jp/journals/chem-lett/.

11
- 51149100498
- Crystal data for 1 at 123 K: Crystal size 0.32 × 0.18 × 0.17 mm3, C34H42O4Rh 2S2: fw 784.63, Space group P21/c, a, 9.0227(17, b, 13.993(2, c, 25.049(5)Å, β, 96.2991(14)°, V, 3143.6(10)Å3, Z, 4, D calcd, 1.658 g/cm3, Number of reflections 7123, R 1 (I > 2σ(I, 0.0275, wR2 (all data) 0.0794, CCDC-686764
- 2 (all data) 0.0794, CCDC-686764.

12
- 51149109738
- Crystal data for 2 at 123 K: Crystal size 0.24 × 0.22 × 0.19 mm3, C34H42O4Rh 2S2: fw 784.63, Space group P21/c, a, 9.1916(13, b, 14.2278(18, c, 24.323(4) Å, β, 95.7350(11)°, V, 3165.0(8)Å3, Z, 4, Dcalcd, 1.647 g/cm3, Number of reflections 6980, R1 (I > 2σ(I, 0.0709, wR 2 (all data) 0.1629, CCDC-686763
- 2 (all data) 0.1629, CCDC-686763.

13
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14
- 51149116240
- In the case of the Cp* derivative, only one stereoisomer was formed at the final stage of the photoreaction.2
- 2

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