Development of extraction procedures for the determination of imidacloprid: Application to residue analysis and dynamics of two formulations in Chinese cabbage

Biomedical Chromatography

Volumn 22, Issue 6, 2008, Pages 581-589

  Khay, Sathya ^a   Abd El Aty, A M ^b,c   Cho, Soon Kil ^d   Choi, Jeong Heui ^a   Mamun, M I R ^a   Goudah, Ayman ^c   Shin, Ho Chul ^b   Shim, Jae Han ^a  

^a Chonnam National University   (South Korea)

^b Konkuk University   (South Korea)

^c Cairo University   (Egypt)

^d Ministry of Agriculture and Forestry Korea   (South Korea)

Author keywords

Commercial formulations; Degradation dynamic; Imidacloprid; Residues

Indexed keywords

HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; INSECTICIDES; MASS SPECTROMETRY;

ADDITIONAL COLUMNS; CHINESE CABBAGE; COMMERCIAL FORMULATION; DEGRADATION DYNAMICS; EXTRACTION PROCEDURE; IMIDACLOPRIDS; RESIDUE; RESIDUE ANALYSIS; RESIDUE LEVEL; WETTABLE POWDERS;

DEGRADATION;

IMIDACLOPRID;

ARTICLE; CHEMICAL ANALYSIS; CHEMICAL COMPOSITION; CHINESE CABBAGE; CONCENTRATION (PARAMETERS); GREENHOUSE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ION MONITORING; MASS SPECTROMETRY; QUANTITATIVE ANALYSIS; RADIATION DETECTION; RESIDUE ANALYSIS; SEPARATION TECHNIQUE; STANDARDIZATION; ULTRAVIOLET RADIATION;

BRASSICA RAPA SUBSP. PEKINENSIS;

EID: 46949109004     PISSN: 02693879     EISSN: 10990801     Source Type: Journal    
DOI: 10.1002/bmc.972     Document Type: Article

References (49)

1. Akelah A. Novel utilisation of conventional agrochemicals by controlled release formulations. Materials Science and Engineering 1996; 83-98.
2. Bai D, Lummis SCR, Leicht W, Breer H and Sattelle DB. Actions of imidacloprid and a related nitromethylene on cholinergic receptors of an identified insect motor neuron. Pesticide Science 1991; 33: 197-204.
3. Baskaran S, Kookana RS and Naidu R. Determination of the insecticide imidacloprid in water and soil using high-performance liquid chromatography. Journal of Chromatography 1997; 787: 271-275.
4. Blasco C, Fernández M, Picó Y, Font G and Mañes J. Simultaneous determination of imidacloprid, carbendazim, methiocarb and hexythiazox in peaches and nectarines by liquid chromatography-mass spectrometry. Analytica Chimica Acta 2002; 461: 109-116.
5. Buckingham SD, Lapied B, Le Corrone H, Grolleau F and Sattelle DB. Imidacloprid action on insect neuronal acetylcholine receptors. The Journal of Experimental Biology 1997; 200: 2685-2692.
6. Cabras P, Meloni M, Manca MR, Pirisi FM, Cabitza F and Cubeddu M. Pesticide residues in lettuce. 1. Influence of the cultivar. Journal of Agricultural and Food Chemistry 1998; 36: 92-95.
7. Cryer SA and Laskowski DA. Chlorpyrifos release rate from clay granules: experimental observations and simple algorithm development for use in computer-based exposure assessments. Journal of Agricultural and Food Chemistry 1998; 46: 3810-3816.
8. Daraghmeh A, Shraim A, Abulhaj S, Sansour R and Ng JC. Imidacloprid residues in fruits, vegetables and water samples from Palestine. Environmental Geochemistry and Health 2007; 29: 45-50.
9. Déglise P, Grünewald B and Gauthier M. The insecticide imidacloprid is a partial agonist of the nicotinic receptor of honeybee Kenyon cells. Neuroscience Letters 2002; 321: 13-16.
10. Dejonckheere W, Verstraeten R, Steurbaut W, Melkebeke G and Kips RH. Permethrin and deltamethrin residues on lettuce. Pesticide Science 1982; 13: 351-356.
11. Di Muccio A, Fidente P, Barbini DA, Dommarco R, Seccia S and Morrica P. Application of solid-phase extraction and liquid chromatography-mass spectrometry to the determination of neonicotinoid pesticide residues in fruit and vegetables. Journal of Chromatography A 2006; 1108: 1-6.
12. Du F, Zhu Q and Liu J. Evolution and control measures of vegetable pests and diseases. Yangtze Veg 2002; 3: 28-29.
13. Escriche B, Gonzalez-Cabrera J, Herrero S and Ferré J. Insecticidal effects of Bacillus thurigiensis crystal proteins. Potency differences depending on the tested strain. Phytoma 2001; 129: 40-45.
14. Eskilsson CS, Hartonen K, Mathiasson L and Riekkola ML. Pressurized hot water extraction of insecticides from process dust - comparison with supercritical fluid extraction. Journal of Separation Science 2004; 27: 59-64.
15. European Commission (SANCO/3103/2000). Quality control procedures for pesticide residues analysis. Guidelines for Residues Monitoring in the European Union, 2nd edn, 1999/2000.
16. Fernandez-Alba AR, Valverde A, Agüera A, Contreras M and Chirom S. Determination of imidacloprid in vegetables by high-performance liquid chromatography with diode-array detection. Journal of Chromatography A 1996; 721: 97-105.
17. Francotte E, Davatz A and Richert P. Development and validation of chiral high-performance liquid chromatographic methods for the quantitation of valsartan and of the tosylate of valinebenzyl ester. Journal of Chromatography B 1996: 686: 77-80.
18. Gajbhiye VT, Gupta S and Gupta RK. Persistence of imidacloprid in/on cabbage and cauliflower. Bulletin of Environmental Contamination and Toxicology 2004; 72: 283-288.
19. Garrido Frenich A, Egea González FJ, Martínez Vidal JL, Parilla Vázquez P and Media Sánchez M. Determination of imidacloprid and its metabolite 6-chloronicotinic acid in greenhouse air by high-performance liquid chromatography with diode-array detection. Journal of Chromatography A 2000; 869: 497-504.
20. Gonzalex-Pradas E, Urena-Amate MD, Flores-Cespedes F, Fernandez-Perez M, Garratt J and Wilkins R. Leaching of Imidacloprid and Procymidone in a Greenhouse of Southeast of Spain. Soil Science Society of America Journal 2002; 66:1821-1828.
21. Gunther FA, Iwata I, Carman GE and Smith CA. The citrus re-entry problem: research on its causes and effects, and approaches to its minimization. Residue Reviews 1977; 67: 1-139.
22. Kagabu S, Yokoyama K, Iwaya K and Tanaka M. Imidacloprid and related compounds: structure and water solubility of N-alkyl derivatives of imidacloprid. Bioscience, Biotechnology, and Biochemistry 1998; 62: 1216-1224.
23. Kanrar B, Ghosh T, Pramanik SK, Dutta S, Bhattacharyya A and Dhuri A. Degradation dynamics and persistence of imidacloprid in a rice ecosystem under West Bengal climatic conditions. Bulletin of Environmental Contamination and Toxicology 2006; 77: 631-637.
24. Khay S, Abd El-Aty AM, Choi JH, Choi JT, Lim KT and Shim JH. Methomyl residue on Chinese cabbage grown under greenhouse conditions. Bulletin of Environmental Contamination and Toxicology 2006; 77: 516-520.
25. Kissel J and Fenske R. Improved estimation of dermal pesticide dose to agricultural workers upon reentry. Applied Occupational and Environmental Hygiene 2000; 15: 284-290.
26. Korea Food and Drug Administration. MRLs for Pesticides in Foods. Seoul, Korea, 2005.
27. Lambin M, Armengaud C, Raymond S and Gauthier M. Imidacloprid-induced facilitation of the proboscis extension reflex habituation in the honeybee. Archives of Insect Biochemistry and Physiology 2005; 48: 129-134.
28. Libman GN and MacIntosh SC. Registration of biopesticides. In Entomopathogenic Bacteria: from Laboratory to Field Application, Charles J, Delecluse A and Nielsen-Le Roux C (eds). Kluwer Academic: Dordrecht, 2000; 333-336.
29. Liu H, Song J, Zhang S, Qu L, Zhao Y, Wu Y and Liu H. Analysis of residues of imidacloprid in tobacco by high-performance liquid chromatography with liquid-liquid partition cleanup. Pest Management Science 2005; 61: 511-514.
30. 3H] imidacloprid binding site in house fly head acetylcholine receptor to insecticidal activity of 2-nitromethylene- and 2-nitroimino-imidazolidines. Pesticide Biochemistry and Physiology 1993; 46: 40-46.
31. Lodevico RG and Li QX. Determination of total imidacloprid residues in coffee by gas chromatography-mass spectrometry. Analytical Letters 2002; 35: 315-326.
32. Luo Y, Zang Y, Zhong Y and Kong Z. Toxicological study of two novel pesticides on earthworm Eisenia foetida. Chemosphere 1999; 39: 2347-2356.
33. MacDonald LM and Meyer TR. Determination of imidacloprid and triadimefon in white pine by gas chromatography/mass spectrometry. Journal of Agricultural and Food Chemistry 1998; 46: 3133-3138.
34. Martínez Galera M, Garrido Frenich A, Martínez Vidal JL and Parrilla Vázquez P. Resolution of imidacloprid pesticide and its metabolite 6-chloronicotinic acid using cross-sections of spectrochromatograms obtained by high-performance liquid chromatography with diode-array detection. Journal of Chromatography A 1998: 799: 149-154.
35. Matsuda K, Shimomura M, Kondo Y, Ihara M, Hashigami K, Yoshida N, Raymond V, Mongan NP, Freeman JC, Komai K and Sattelle DB. Role of loop D of the α7 nicotinic acetylcholine receptor in its interaction with the insecticide imidacloprid and related neonicotinoids. British Journal of Pharmacology 2000; 130: 981-986.
36. Matsuda K, Buckingham SD, Kleier D, Rauh JJ, Grauso M and Sattelle DB. Neonicotinoids: insecticides acting on insect nicotinic acetylcholine receptors. Trends in Pharmacological Sciences 2001; 22: 573-580.
37. Moriya K, Shibuya K, Hattori J, Tsuboi S, Shiokawa K and Kagabu S. 1-(6-Chloronicotinyl)-2-nitroimino-imidazolines and related compounds as potential new insecticides. Bioscience, Biotechnology, and Biochemistry 1992; 56: 364-365.
38. Obana H, Okihashi M, Akutsu K, Kitagawa Y and Hori S. Determination of acetamiprid, imidacloprid, and nitenpyram residues in vegetables and fruits by high-performance liquid chromatography with diode-array detection. Journal of Agricultural and Food Chemistry 2002; 50: 4464-4467.
39. Sances FV, Toscano NC and Gaston LK. Minimization of pesticide residue on head lettuce: within-head residue distribution of selected insecticides. Journal of Eonomic Entomology 1992; 85: 203-207.
40. Sannino A, Bolzoni L and Bandini M. Application of liquid chromatography with electrospray tandem mass spectrometry to the determination of a new generation of pesticides in processed fruits and vegetables. Journal of Chromatography A 2004; 1036: 161-169.
41. Spencer JR, Hernandez BZ, Schneider FA, Gonzales M, Begum S and Krieger RI. Seasonal mevinphos degradation on row crops in Monterey County. Chemosphere 1992; 24: 773-777.
42. Suchail S, Guez D and Belzunces LP. Discrepancy between acute and chronic toxicity induced by imidacloprid and its metabolites in Apis mellifera. Environmental Toxicology and Chemistry 2001; 20: 2482-2486.
43. Tharp GI, Johnson GD and Onsager JA. Laboratory and field evaluations of imidacloprid against Melanoplus sanguinipes (Orthoptera: Acrididae) on small grains. Journal of Economic Entomology 2000; 93: 293-299.
44. Timme G, Frehse H and Laska V. Statistical interpretation and graphic representation of the degradation behavior of pesticides residues. I. Pflanzenschutz-Nachrichten Bayer 1980; 33: 47-60.
45. Timme G, Frehse H and Laska V. Statistical interpretation and graphic representation of the degradation behavior of pesticides residues. II. Pflanzenschutz-Nachrichten Bayer 1986; 39: 187-203.
46. Tomizawa M and Casida JE. Imidacloprid, thiacloprid, and their imine derivatives up-regulate the α4β2 nicotinic acetylcholine receptor in M10 cells. Toxicology and Applied Pharmacology 2000; 169: 114-120.
47. Tomizawa M, Cowan A and Casida JE. Analgesic and toxic effects of neonicotinoid insecticides in mice. Toxicology and Applied Pharmacology 2001; 177: 77.
48. Yamamoto I, Yabuta G, Tomizawa M, Salto T, Miyamoto T and Kagabu S. Molecular mechanism for selective toxicity of nicotinoids and neonicotinoids. Journal of Pesticide Science 1995; 20: 33-40.
49. Xu T, Jacobsen CM, Cho IK, Hara AH and Li QX. Application of an enzyme-linked immunosorbent assay for the analysis of imidacloprid in wiliwili tree, Erythrina sandwicensis O. Deg, for control of the wasp Quadrastichus erythrinae. Journal of Agricultural and Food Chemistry 2006; 54: 8444-8449.